JPH0131443B2 - - Google Patents
Info
- Publication number
- JPH0131443B2 JPH0131443B2 JP57101754A JP10175482A JPH0131443B2 JP H0131443 B2 JPH0131443 B2 JP H0131443B2 JP 57101754 A JP57101754 A JP 57101754A JP 10175482 A JP10175482 A JP 10175482A JP H0131443 B2 JPH0131443 B2 JP H0131443B2
- Authority
- JP
- Japan
- Prior art keywords
- hollow
- microspheres
- materials
- solution
- metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000010304 firing Methods 0.000 claims description 12
- 150000002736 metal compounds Chemical class 0.000 claims description 11
- 229910044991 metal oxide Inorganic materials 0.000 claims description 8
- 150000004706 metal oxides Chemical class 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 6
- 239000004005 microsphere Substances 0.000 description 21
- 239000002245 particle Substances 0.000 description 14
- 238000000034 method Methods 0.000 description 13
- 239000000463 material Substances 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 239000002994 raw material Substances 0.000 description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 238000009826 distribution Methods 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 239000002131 composite material Substances 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 238000000635 electron micrograph Methods 0.000 description 3
- 239000003595 mist Substances 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 229910000859 α-Fe Inorganic materials 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 239000011358 absorbing material Substances 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 239000012159 carrier gas Substances 0.000 description 2
- 238000009841 combustion method Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- -1 melt Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 description 2
- 239000010936 titanium Substances 0.000 description 2
- 229910052719 titanium Inorganic materials 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical class CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 1
- 239000004604 Blowing Agent Substances 0.000 description 1
- FGQRHNWAVSBJHZ-UHFFFAOYSA-N CCCC[Zr] Chemical compound CCCC[Zr] FGQRHNWAVSBJHZ-UHFFFAOYSA-N 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- ISKQADXMHQSTHK-UHFFFAOYSA-N [4-(aminomethyl)phenyl]methanamine Chemical compound NCC1=CC=C(CN)C=C1 ISKQADXMHQSTHK-UHFFFAOYSA-N 0.000 description 1
- 150000001242 acetic acid derivatives Chemical class 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 229910052910 alkali metal silicate Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 150000004703 alkoxides Chemical class 0.000 description 1
- 229920000180 alkyd Polymers 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 229910052787 antimony Inorganic materials 0.000 description 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
- GVFOJDIFWSDNOY-UHFFFAOYSA-N antimony tin Chemical compound [Sn].[Sb] GVFOJDIFWSDNOY-UHFFFAOYSA-N 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- JRPBQTZRNDNNOP-UHFFFAOYSA-N barium titanate Chemical compound [Ba+2].[Ba+2].[O-][Ti]([O-])([O-])[O-] JRPBQTZRNDNNOP-UHFFFAOYSA-N 0.000 description 1
- 229910002113 barium titanate Inorganic materials 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 239000003989 dielectric material Substances 0.000 description 1
- 239000012776 electronic material Substances 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000010881 fly ash Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- FUKUFMFMCZIRNT-UHFFFAOYSA-N hydron;methanol;chloride Chemical compound Cl.OC FUKUFMFMCZIRNT-UHFFFAOYSA-N 0.000 description 1
- SKWCWFYBFZIXHE-UHFFFAOYSA-K indium acetylacetonate Chemical compound CC(=O)C=C(C)O[In](OC(C)=CC(C)=O)OC(C)=CC(C)=O SKWCWFYBFZIXHE-UHFFFAOYSA-K 0.000 description 1
- RHZWSUVWRRXEJF-UHFFFAOYSA-N indium tin Chemical compound [In].[Sn] RHZWSUVWRRXEJF-UHFFFAOYSA-N 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 150000003893 lactate salts Chemical class 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000696 magnetic material Substances 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 229910001562 pearlite Inorganic materials 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000002952 polymeric resin Substances 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000013268 sustained release Methods 0.000 description 1
- 239000012730 sustained-release form Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 239000011135 tin Substances 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
- C01B13/14—Methods for preparing oxides or hydroxides in general
- C01B13/34—Methods for preparing oxides or hydroxides in general by oxidation or hydrolysis of sprayed or atomised solutions
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Iron (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Silicon Compounds (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP57101754A JPS58223606A (ja) | 1982-06-14 | 1982-06-14 | 金属酸化物中空超微小球体の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP57101754A JPS58223606A (ja) | 1982-06-14 | 1982-06-14 | 金属酸化物中空超微小球体の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS58223606A JPS58223606A (ja) | 1983-12-26 |
| JPH0131443B2 true JPH0131443B2 (de) | 1989-06-26 |
Family
ID=14309018
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP57101754A Granted JPS58223606A (ja) | 1982-06-14 | 1982-06-14 | 金属酸化物中空超微小球体の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS58223606A (de) |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61168528A (ja) * | 1985-01-23 | 1986-07-30 | Shokubai Kasei Kogyo Kk | 酸化チタンからなる真球状微粒子粉末 |
| JPS61201604A (ja) * | 1985-03-05 | 1986-09-06 | Hiroyoshi Inoue | 球状金属酸化物超微粒子の製造方法 |
| JP2566805B2 (ja) * | 1988-01-28 | 1996-12-25 | 日鉄化工機株式会社 | 複合酸化物粉体の製造方法 |
| DE69317519T2 (de) * | 1992-12-11 | 1998-11-26 | Asahi Glass Co Ltd | Verfahren zur Herstellung von kristallinen Mikrohohlkugeln |
| WO1999011574A1 (fr) | 1997-09-02 | 1999-03-11 | Ishihara Sangyo Kaisha, Ltd. | Poudre fine creuse, poudre d'oxyde de titane fine et floconneuse, preparee par pulverisation de la poudre fine creuse et procede de preparation de ces deux poudres |
| JP4822576B2 (ja) * | 2000-05-30 | 2011-11-24 | 京セラ株式会社 | 無機質中空粉体とその製造方法 |
| JP4043805B2 (ja) * | 2001-09-13 | 2008-02-06 | 矢崎総業株式会社 | アルミナ中空粒子の製造方法及び製造装置 |
| JP4271045B2 (ja) * | 2003-04-17 | 2009-06-03 | 矢崎総業株式会社 | アルミナ中空粒子の製造方法 |
| JP4112540B2 (ja) * | 2004-08-26 | 2008-07-02 | 電気化学工業株式会社 | 球状無機質中空粉体の製造方法。 |
| US9278866B2 (en) * | 2005-08-10 | 2016-03-08 | The Procter & Gamble Company | Hollow silica particles, compositions comprising them, and methods for making same |
| WO2007102569A1 (ja) * | 2006-03-08 | 2007-09-13 | Denki Kagaku Kogyo Kabushiki Kaisha | 無機質中空粉体、その製造方法及び該無機質中空粉体を含有する組成物 |
| KR100692612B1 (ko) | 2006-04-21 | 2007-03-14 | 한국화학연구원 | 구형 실리콘 미립자의 제조 방법 |
| KR100917969B1 (ko) | 2007-03-23 | 2009-09-17 | 셀룬코리아(주) | 초음파분무법을 이용한 세라믹 중공구 제조방법 |
| JP5248054B2 (ja) * | 2007-07-23 | 2013-07-31 | 関西電力株式会社 | 球状アルミナ粒子の製造方法 |
| US8377555B2 (en) | 2008-02-22 | 2013-02-19 | Toyota Motor Engineering & Manufacturing North America, Inc. | Gas storage materials, including hydrogen storage materials |
| US7914846B2 (en) | 2008-04-17 | 2011-03-29 | Toyota Motor Engineering & Manufacturing North America, Inc. | Method for encapsulating reactive metal hydrides |
| JP2010208875A (ja) * | 2009-03-09 | 2010-09-24 | Tokyo Institute Of Technology | 磁性中空粒子およびその製造方法 |
| JP2011016718A (ja) * | 2010-09-06 | 2011-01-27 | Kyocera Corp | 無機質中空粉体およびその製造方法 |
| KR101326226B1 (ko) * | 2010-12-29 | 2013-11-05 | 한국세라믹기술원 | 분무 건조법을 이용한 실리카 중공입자 및 그 제조방법과 실리카-티타니아 복합 중공입자 및 그 제조방법 |
| JP6316153B2 (ja) * | 2013-09-19 | 2018-04-25 | 太平洋セメント株式会社 | 微小アルミナ中空粒子 |
| AU2018329173B2 (en) | 2017-09-11 | 2023-10-05 | Basf Se | Porous metal oxide microspheres |
| EP3681685A4 (de) | 2017-09-11 | 2021-06-16 | President And Fellows Of Harvard College | Mikrokugeln mit polydispersen polymernanokugeln und porösen metalloxidmikrokugeln |
-
1982
- 1982-06-14 JP JP57101754A patent/JPS58223606A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS58223606A (ja) | 1983-12-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPH0131443B2 (de) | ||
| US5439502A (en) | Method for making silver powder by aerosol decomposition | |
| US5429657A (en) | Method for making silver-palladium alloy powders by aerosol decomposition | |
| CN100391831C (zh) | 制备碳纳米笼的方法 | |
| JP2004290730A (ja) | 複合粒子の製造方法、球状複合粒子の製造方法 | |
| US5928405A (en) | Method of making metallic powders by aerosol thermolysis | |
| JPH04275927A (ja) | 中空ガラス球体小粒子の製造法 | |
| KR102241096B1 (ko) | 큐빅 구조를 가지는 가넷형 산화물 고체전해질의 제조방법 | |
| Do Kim et al. | Formation of spherical hollow silica particles from sodium silicate solution by ultrasonic spray pyrolysis method | |
| JP2002346377A (ja) | 熱プラズマによるセラミック又は金属の球状粉末の製造方法および装置 | |
| JPS59107904A (ja) | 金属酸化物微粒子の製造法 | |
| US8117867B2 (en) | Process for producing spherical inorganic particle | |
| JP6228782B2 (ja) | 発泡金属の製造方法 | |
| KR100917969B1 (ko) | 초음파분무법을 이용한 세라믹 중공구 제조방법 | |
| JP4400718B2 (ja) | 単結晶セラミックス粒子の製造方法 | |
| JPS63156017A (ja) | フェライト原料用粉末複合酸化物を製造する方法 | |
| KR100468050B1 (ko) | 구형 실리카 분말의 제조방법 | |
| EP0476050B1 (de) | Aluminiumoxidschäume und verfahren zur herstellung davon | |
| JP4596111B2 (ja) | 球状酸化物粉末の製造方法および球状粉末製造装置 | |
| KR20030071703A (ko) | 유리 중공구체의 제조 방법 및 장치 | |
| JPH05311212A (ja) | Ａｇ−Ｐｄ合金微粉末の製造方法 | |
| JP6228783B2 (ja) | 発泡金属からなる容器の製造方法 | |
| JPS62167206A (ja) | 球状金属酸化物粒子の製造法 | |
| JP2006247551A (ja) | 微細液滴の発生方法とそれを用いた微粒子の製造方法及び微粒子 | |
| KR102529239B1 (ko) | 미립 구상 방열 소재 및 이의 제조방법 |