JP7560452B2 - 骨格型mfiを有するゼオライト材料を含む成形品 - Google Patents

骨格型mfiを有するゼオライト材料を含む成形品 Download PDF

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Publication number
JP7560452B2
JP7560452B2 JP2021519721A JP2021519721A JP7560452B2 JP 7560452 B2 JP7560452 B2 JP 7560452B2 JP 2021519721 A JP2021519721 A JP 2021519721A JP 2021519721 A JP2021519721 A JP 2021519721A JP 7560452 B2 JP7560452 B2 JP 7560452B2
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Prior art keywords
range
molded article
zeolitic material
mfi
framework
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Japanese (ja)
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JP2022512656A5 (OSRAM
JP2022512656A (ja
Inventor
パルフレスク,アンドレイ-ニコラエ
リュッツェル,ハンス-ユルゲン
ミュラー,ウルリヒ
リーデル,ドミニク
ヘンリケ テレス,ジョアキム
ヴェーバー,マルクス
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BASF SE
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BASF SE
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22C—FOUNDRY MOULDING
    • B22C1/00—Compositions of refractory mould or core materials; Grain structures thereof; Chemical or physical features in the formation or manufacture of moulds
    • B22C1/16—Compositions of refractory mould or core materials; Grain structures thereof; Chemical or physical features in the formation or manufacture of moulds characterised by the use of binding agents; Mixtures of binding agents
    • B22C1/18—Compositions of refractory mould or core materials; Grain structures thereof; Chemical or physical features in the formation or manufacture of moulds characterised by the use of binding agents; Mixtures of binding agents of inorganic agents
    • B22C1/181—Cements, oxides or clays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/635—0.5-1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/63—Pore volume
    • B01J35/638—Pore volume more than 1.0 ml/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J6/00—Heat treatments such as Calcining; Fusing ; Pyrolysis
    • B01J6/001—Calcining
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/22—After treatment, characterised by the effect to be obtained to destroy the molecular sieve structure or part thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/42—Addition of matrix or binder particles

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2021519721A 2018-10-09 2019-10-09 骨格型mfiを有するゼオライト材料を含む成形品 Active JP7560452B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP18199428.6 2018-10-09
EP18199428 2018-10-09
PCT/EP2019/077372 WO2020074586A1 (en) 2018-10-09 2019-10-09 A molding comprising a zeolitic material having framework type mfi

Publications (3)

Publication Number Publication Date
JP2022512656A JP2022512656A (ja) 2022-02-07
JP2022512656A5 JP2022512656A5 (OSRAM) 2022-10-14
JP7560452B2 true JP7560452B2 (ja) 2024-10-02

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ID=63862001

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JP2021519721A Active JP7560452B2 (ja) 2018-10-09 2019-10-09 骨格型mfiを有するゼオライト材料を含む成形品

Country Status (9)

Country Link
US (1) US20210346942A1 (OSRAM)
EP (1) EP3864010A1 (OSRAM)
JP (1) JP7560452B2 (OSRAM)
KR (1) KR102863394B1 (OSRAM)
CN (1) CN112805272A (OSRAM)
MX (1) MX2021004084A (OSRAM)
SG (1) SG11202102455SA (OSRAM)
WO (1) WO2020074586A1 (OSRAM)
ZA (1) ZA202103028B (OSRAM)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2024543122A (ja) 2021-11-22 2024-11-19 ビーエーエスエフ ソシエタス・ヨーロピア エポキシ化触媒及びその調製方法
KR20240115875A (ko) 2021-11-29 2024-07-26 바스프 에스이 과산화수소 활성화를 위한 촉매
KR20250168655A (ko) 2023-04-06 2025-12-02 바스프 에스이 올레핀 산화물의 제조 공정을 위한 스타트업 방법
EP4719665A1 (en) 2023-05-31 2026-04-08 Basf Se Catalyst for epoxidation of propylene
EP4719664A1 (en) 2023-05-31 2026-04-08 Basf Se Catalyst molding for hydrogen peroxide activation

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1132699C (zh) 1999-12-24 2003-12-31 中国石油化工集团公司 一种钛硅分子筛及其制备方法
JP2016529190A (ja) 2013-07-05 2016-09-23 ダンマークス・テクニスケ・ユニヴェルシテット ゼオライト及びゼオ型を製造する方法
JP2016535718A (ja) 2013-10-23 2016-11-17 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 疎水性のゼオライト系材料についての成形物及びその製造方法
JP2017531691A (ja) 2014-09-29 2017-10-26 中国石油化工股▲ふん▼有限公司 オレフィン類の酸化方法、反応装置及び反応系

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19939416A1 (de) * 1999-08-20 2001-02-22 Basf Ag Verfahren zur Herstellung eines kristallinen, zeolithischen Feststoffs
JP5933445B2 (ja) * 2009-11-27 2016-06-08 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se チタンゼオライト触媒の製造方法
US8785670B2 (en) * 2010-12-07 2014-07-22 Basf Se Process for the production of propylene oxide
CN103708493A (zh) * 2013-11-26 2014-04-09 华东师范大学 具有mfi结构钛硅分子筛及其制备方法
CN108250161B (zh) * 2016-12-28 2022-01-04 中国石油化工股份有限公司 烯丙醇氧化方法
WO2018197470A1 (en) * 2017-04-24 2018-11-01 Basf Se A molding comprising a zeolitic material, phosphorous, one or more metals and a binder

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1132699C (zh) 1999-12-24 2003-12-31 中国石油化工集团公司 一种钛硅分子筛及其制备方法
JP2016529190A (ja) 2013-07-05 2016-09-23 ダンマークス・テクニスケ・ユニヴェルシテット ゼオライト及びゼオ型を製造する方法
JP2016535718A (ja) 2013-10-23 2016-11-17 ビーエーエスエフ ソシエタス・ヨーロピアBasf Se 疎水性のゼオライト系材料についての成形物及びその製造方法
JP2017531691A (ja) 2014-09-29 2017-10-26 中国石油化工股▲ふん▼有限公司 オレフィン類の酸化方法、反応装置及び反応系

Also Published As

Publication number Publication date
BR112021005279A2 (pt) 2021-06-15
ZA202103028B (en) 2025-09-25
MX2021004084A (es) 2021-06-04
CN112805272A (zh) 2021-05-14
EP3864010A1 (en) 2021-08-18
SG11202102455SA (en) 2021-04-29
US20210346942A1 (en) 2021-11-11
KR20210066913A (ko) 2021-06-07
KR102863394B1 (ko) 2025-09-22
JP2022512656A (ja) 2022-02-07
WO2020074586A1 (en) 2020-04-16

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