JP7039051B2 - 大気圧での化学蒸着(ap-cvd)により銅基板にグラフェンを製造する改良方法および改良システム - Google Patents
大気圧での化学蒸着(ap-cvd)により銅基板にグラフェンを製造する改良方法および改良システム Download PDFInfo
- Publication number
- JP7039051B2 JP7039051B2 JP2019524490A JP2019524490A JP7039051B2 JP 7039051 B2 JP7039051 B2 JP 7039051B2 JP 2019524490 A JP2019524490 A JP 2019524490A JP 2019524490 A JP2019524490 A JP 2019524490A JP 7039051 B2 JP7039051 B2 JP 7039051B2
- Authority
- JP
- Japan
- Prior art keywords
- copper sheets
- copper
- cylindrical chamber
- producing graphene
- graphene according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/46—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for heating the substrate
- C23C16/463—Cooling of the substrate
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/22—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
- C23C16/26—Deposition of carbon only
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/184—Preparation
- C01B32/186—Preparation by chemical vapour deposition [CVD]
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/02—Pretreatment of the material to be coated
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/46—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for heating the substrate
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/54—Apparatus specially adapted for continuous coating
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/04—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
- H01L21/18—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic Table or AIIIBV compounds with or without impurities, e.g. doping materials
- H01L21/28—Manufacture of electrodes on semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/268
- H01L21/283—Deposition of conductive or insulating materials for electrodes conducting electric current
- H01L21/285—Deposition of conductive or insulating materials for electrodes conducting electric current from a gas or vapour, e.g. condensation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Nanotechnology (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Power Engineering (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Computer Hardware Design (AREA)
- Crystallography & Structural Chemistry (AREA)
- Composite Materials (AREA)
- Carbon And Carbon Compounds (AREA)
- Chemical Vapour Deposition (AREA)
- General Induction Heating (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CL2016001858A CL2016001858A1 (es) | 2016-07-21 | 2016-07-21 | Método y sistema para producir grafeno sobre un sustrato de cobre por deposición de vapores químicos (ap_cvd) modificado |
| CL1858-2016 | 2016-07-21 | ||
| PCT/CL2017/050032 WO2018014143A1 (es) | 2016-07-21 | 2017-07-18 | Método y sistema para producir grafeno sobre un substrato de cobre por deposición de vapores químicos (ap-cvd) modificado |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2019529323A JP2019529323A (ja) | 2019-10-17 |
| JP2019529323A5 JP2019529323A5 (cg-RX-API-DMAC7.html) | 2021-01-21 |
| JP7039051B2 true JP7039051B2 (ja) | 2022-03-22 |
Family
ID=59858379
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2019524490A Expired - Fee Related JP7039051B2 (ja) | 2016-07-21 | 2017-07-18 | 大気圧での化学蒸着(ap-cvd)により銅基板にグラフェンを製造する改良方法および改良システム |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US11624114B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP3489194A4 (cg-RX-API-DMAC7.html) |
| JP (1) | JP7039051B2 (cg-RX-API-DMAC7.html) |
| KR (1) | KR102408821B1 (cg-RX-API-DMAC7.html) |
| CL (1) | CL2016001858A1 (cg-RX-API-DMAC7.html) |
| WO (1) | WO2018014143A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CL2016001858A1 (es) | 2016-07-21 | 2017-02-17 | Univ Técnica Federico Santa Mar+Ia | Método y sistema para producir grafeno sobre un sustrato de cobre por deposición de vapores químicos (ap_cvd) modificado |
| KR20220070031A (ko) * | 2019-09-30 | 2022-05-27 | 램 리써치 코포레이션 | 리모트 플라즈마를 사용한 선택적인 그래핀 증착 |
| CN115380365A (zh) | 2020-02-13 | 2022-11-22 | 朗姆研究公司 | 具有无穷大选择性的高深宽比蚀刻 |
| JP2023514831A (ja) | 2020-02-19 | 2023-04-11 | ラム リサーチ コーポレーション | グラフェン集積化 |
| CN115433920B (zh) * | 2021-06-03 | 2024-05-14 | 上海新池能源科技有限公司 | 生长单层石墨烯的工艺方法 |
| CN113566044A (zh) * | 2021-07-30 | 2021-10-29 | 重庆大学 | 一种获取连续高温氯气的加热方法 |
| CN113699503B (zh) * | 2021-08-31 | 2022-09-09 | 上海交通大学 | 金属表面具有多相复合碳源的石墨烯制备方法及装置 |
| CN114459336A (zh) * | 2022-03-04 | 2022-05-10 | 广东粤港澳大湾区国家纳米科技创新研究院 | 石墨烯应变传感器及石墨烯应变传感器的制备方法 |
| CN115125524A (zh) * | 2022-07-05 | 2022-09-30 | 常州第六元素半导体有限公司 | 一种分段式卷对卷cvd石墨烯连续生长设备 |
| CN115744886B (zh) * | 2022-11-24 | 2024-04-19 | 广东墨睿科技有限公司 | 一种石墨烯生长支架及生长石墨烯的方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014038803A1 (en) | 2012-09-04 | 2014-03-13 | Samsung Techwin Co., Ltd | Catalyst metal film-supporting device and method and apparatus for synthesizing multiple graphene films |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4698354B2 (ja) * | 2005-09-15 | 2011-06-08 | 株式会社リコー | Cvd装置 |
| US20100301212A1 (en) * | 2009-05-18 | 2010-12-02 | The Regents Of The University Of California | Substrate-free gas-phase synthesis of graphene sheets |
| KR101912798B1 (ko) * | 2011-01-31 | 2018-10-30 | 한화에어로스페이스 주식회사 | 그래핀 합성장치 및 합성방법 |
| GB2516372B (en) * | 2012-01-06 | 2021-01-13 | Ut Battelle Llc | High quality large scale single and multilayer graphene production by chemical vapor deposition |
| GB201215579D0 (en) * | 2012-08-31 | 2012-10-17 | Univ Leiden | Thin film formation |
| US20150140211A1 (en) * | 2013-11-19 | 2015-05-21 | Cvd Equipment Corporation | Scalable 2D-Film CVD Synthesis |
| CL2016001858A1 (es) | 2016-07-21 | 2017-02-17 | Univ Técnica Federico Santa Mar+Ia | Método y sistema para producir grafeno sobre un sustrato de cobre por deposición de vapores químicos (ap_cvd) modificado |
-
2016
- 2016-07-21 CL CL2016001858A patent/CL2016001858A1/es unknown
-
2017
- 2017-07-18 JP JP2019524490A patent/JP7039051B2/ja not_active Expired - Fee Related
- 2017-07-18 EP EP17830164.4A patent/EP3489194A4/en not_active Withdrawn
- 2017-07-18 KR KR1020197002936A patent/KR102408821B1/ko active Active
- 2017-07-18 US US16/318,193 patent/US11624114B2/en active Active
- 2017-07-18 WO PCT/CL2017/050032 patent/WO2018014143A1/es not_active Ceased
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014038803A1 (en) | 2012-09-04 | 2014-03-13 | Samsung Techwin Co., Ltd | Catalyst metal film-supporting device and method and apparatus for synthesizing multiple graphene films |
Non-Patent Citations (1)
| Title |
|---|
| RYU, Jaechul et al.,Fast Synthesis of High-Performance Graphene Films by Hydrogen-Free Rapid Thermal Chemical Vapor Deposition,ACS NANO,英国,2014年,Vol.8/No.1,pp.950-956 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP3489194A1 (en) | 2019-05-29 |
| WO2018014143A1 (es) | 2018-01-25 |
| EP3489194A4 (en) | 2020-04-22 |
| KR20190032401A (ko) | 2019-03-27 |
| KR102408821B1 (ko) | 2022-06-14 |
| CL2016001858A1 (es) | 2017-02-17 |
| US20190233942A1 (en) | 2019-08-01 |
| US11624114B2 (en) | 2023-04-11 |
| JP2019529323A (ja) | 2019-10-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP7039051B2 (ja) | 大気圧での化学蒸着(ap-cvd)により銅基板にグラフェンを製造する改良方法および改良システム | |
| KR101828528B1 (ko) | 그래핀의 제조 장치 및 제조 방법 | |
| Capasso et al. | Nitrogen-doped graphene films from chemical vapor deposition of pyridine: influence of process parameters on the electrical and optical properties | |
| Lavin-Lopez et al. | Synthesis and characterization of graphene: influence of synthesis variables | |
| US11447391B2 (en) | Method of growing a graphene coating or carbon nanotubes on a catalytic substrate | |
| US8388924B2 (en) | Method for growth of high quality graphene films | |
| US20130011574A1 (en) | Graphene production method and graphene production apparatus | |
| KR101701369B1 (ko) | 탄소가 포함된 액체상의 전구체를 이용한 연속 롤투롤 방식의 고품질 그래핀 제조방법과 그 제조장치 | |
| TW201609341A (zh) | 連續式合成碳薄膜或無機材料薄膜之設備與方法 | |
| CN103352202B (zh) | 一种常压化学气相沉积大面积高质量双层石墨烯薄膜的可控制备方法 | |
| KR101760653B1 (ko) | 그래핀 제조장치 및 그래핀 제조방법 | |
| Lavin-Lopez et al. | Thickness control of graphene deposited over polycrystalline nickel | |
| CN105274500A (zh) | 等离子体增强化学气相沉积制备石墨烯的方法 | |
| US20140170317A1 (en) | Chemical vapor deposition of graphene using a solid carbon source | |
| Somekh et al. | Fully reproducible, low-temperature synthesis of high-quality, few-layer graphene on nickel via preheating of gas precursors using atmospheric pressure chemical vapor deposition | |
| WO2017064113A1 (en) | Metal free graphene synthesis on insulating or semiconducting substrates | |
| KR101154416B1 (ko) | 단결정 성장 방법 | |
| Rouessac et al. | Preparation of silica membranes inside macroporous alumina tubes by PECVD for hydrogen selectivity | |
| TWI535887B (zh) | 合成高品質碳薄膜或無機材料薄膜之設備與方法 | |
| US10337102B2 (en) | Process for producing a graphene film | |
| KR101562906B1 (ko) | 기체상의 금속 촉매를 이용한 전사 공정이 생략된 그래핀의 제조 방법 | |
| Deraman et al. | Optical properties of diamond-like carbon thin films deposited by DC-PECVD | |
| JP6944699B2 (ja) | 六方晶系窒化ホウ素膜の製造方法 | |
| Eres et al. | Ggraphene for metamaterials: Synthesis using do-it-yourself low-cost reactor | |
| WO2021149474A1 (ja) | ダイヤモンド |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20200716 |
|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20201201 |
|
| A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20210608 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20210706 |
|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20210930 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20220208 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20220302 |
|
| R150 | Certificate of patent or registration of utility model |
Ref document number: 7039051 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| LAPS | Cancellation because of no payment of annual fees |