JP7028457B2 - 過酸化物混合物の連続クエンチのためのフロースルー反応器およびそれを含む方法 - Google Patents

過酸化物混合物の連続クエンチのためのフロースルー反応器およびそれを含む方法 Download PDF

Info

Publication number
JP7028457B2
JP7028457B2 JP2018566851A JP2018566851A JP7028457B2 JP 7028457 B2 JP7028457 B2 JP 7028457B2 JP 2018566851 A JP2018566851 A JP 2018566851A JP 2018566851 A JP2018566851 A JP 2018566851A JP 7028457 B2 JP7028457 B2 JP 7028457B2
Authority
JP
Japan
Prior art keywords
reactor
peroxide
quench
flow
peroxide mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2018566851A
Other languages
English (en)
Japanese (ja)
Other versions
JP2019524661A (ja
JP2019524661A5 (enExample
Inventor
パトリック・フォリー
アレクサンドル・シャポー
アントニオ・ミリーチャ
イチリオ・アダミ
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
P2 Science Inc
Original Assignee
P2 Science Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by P2 Science Inc filed Critical P2 Science Inc
Publication of JP2019524661A publication Critical patent/JP2019524661A/ja
Publication of JP2019524661A5 publication Critical patent/JP2019524661A5/ja
Application granted granted Critical
Publication of JP7028457B2 publication Critical patent/JP7028457B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/007—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor in the presence of catalytically active bodies, e.g. porous plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/242—Tubular reactors in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/243—Tubular reactors spirally, concentrically or zigzag wound
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2455—Stationary reactors without moving elements inside provoking a loop type movement of the reactants
    • B01J19/2465—Stationary reactors without moving elements inside provoking a loop type movement of the reactants externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/40—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with ozone; by ozonolysis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/34—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with ozone; by hydrolysis of ozonides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
    • C07C51/373—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by introduction of functional groups containing oxygen only in doubly bound form
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D493/00—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system
    • C07D493/12—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system in which the condensed system contains three hetero rings
    • C07D493/18—Bridged systems
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00096—Plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00788—Three-dimensional assemblies, i.e. the reactor comprising a form other than a stack of plates
    • B01J2219/00792—One or more tube-shaped elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00788—Three-dimensional assemblies, i.e. the reactor comprising a form other than a stack of plates
    • B01J2219/00792—One or more tube-shaped elements
    • B01J2219/00795—Spiral-shaped
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00822—Metal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00835—Comprising catalytically active material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00858—Aspects relating to the size of the reactor
    • B01J2219/0086—Dimensions of the flow channels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00867—Microreactors placed in series, on the same or on different supports
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00873—Heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00889—Mixing

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
JP2018566851A 2016-06-21 2017-06-21 過酸化物混合物の連続クエンチのためのフロースルー反応器およびそれを含む方法 Active JP7028457B2 (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201662352926P 2016-06-21 2016-06-21
US62/352,926 2016-06-21
US201762504487P 2017-05-10 2017-05-10
US62/504,487 2017-05-10
PCT/US2017/038577 WO2017223220A1 (en) 2016-06-21 2017-06-21 Flow-through reactors for the continuous quenching of peroxide mixtures and methods comprising the same

Publications (3)

Publication Number Publication Date
JP2019524661A JP2019524661A (ja) 2019-09-05
JP2019524661A5 JP2019524661A5 (enExample) 2020-02-20
JP7028457B2 true JP7028457B2 (ja) 2022-03-02

Family

ID=60783379

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2018566851A Active JP7028457B2 (ja) 2016-06-21 2017-06-21 過酸化物混合物の連続クエンチのためのフロースルー反応器およびそれを含む方法

Country Status (5)

Country Link
US (1) US10668446B2 (enExample)
EP (1) EP3472124A4 (enExample)
JP (1) JP7028457B2 (enExample)
CA (1) CA3026192A1 (enExample)
WO (1) WO2017223220A1 (enExample)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9682914B2 (en) 2014-01-13 2017-06-20 P2 Science, Inc. Terpene-derived acids and esters and methods for preparing and using same
US10071944B2 (en) 2014-06-20 2018-09-11 P2 Science, Inc. Film ozonolysis in a tubular or multitubular reactor
WO2017223220A1 (en) 2016-06-21 2017-12-28 P2 Science, Inc. Flow-through reactors for the continuous quenching of peroxide mixtures and methods comprising the same
EP3512631B1 (en) 2016-09-16 2022-03-23 P2 Science, Inc. Uses of vanadium to oxidize aldehydes and ozonides
JP7546296B2 (ja) 2018-10-19 2024-09-06 ピー２・サイエンス・インコーポレイテッド オゾニドの不均化クエンチの新規方法
CN113578244A (zh) * 2021-08-09 2021-11-02 聊城鲁西甲胺化工有限公司 一种列管式反应装置及其应用
EP4605368A1 (en) 2022-11-22 2025-08-27 P2 Science, Inc. New method for the ozonolytic synthesis of high melting dicarboxylic acids and oxo-acids
WO2024167957A1 (en) * 2023-02-06 2024-08-15 P2 Science, Inc. New method for ozonolysis and reductive quenching of ozonides

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010095669A1 (ja) 2009-02-17 2010-08-26 国立大学法人宇都宮大学 含酸素化合物の製造方法
JP2015529647A (ja) 2012-07-19 2015-10-08 ピー２ サイエンス，インコーポレイティド 還元および／または酸化された生成物流を発生させるためのオゾン分解操作
WO2015196019A1 (en) 2014-06-20 2015-12-23 P2 Science, Inc. Film ozonolysis in a tubular or multitubular reactor

Family Cites Families (50)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2404666A (en) * 1944-11-08 1946-07-23 Thompson Prod Inc Shock absorbing device
US2813113A (en) 1953-05-07 1957-11-12 Emery Industries Inc Method of making azelaic acid
US3023244A (en) 1959-04-02 1962-02-27 Givaudan Corp Process for making pinonic aldehyde
CH493451A (de) 1967-09-15 1970-07-15 Givaudan & Cie Sa Verfahren zur Herstellung von Terpenderivaten
GB1555333A (en) 1975-05-29 1979-11-07 Bush Boake Allen Ltd Perfumery compositions comprising hydroxy- or alkoxy-substituted c9 alkanals alkanols and esters
IT1100096B (it) 1978-11-10 1985-09-28 Snia Viscosa Procedimento per la preparazione di acidi alfa,omega-dicarbossilici
US4296258A (en) * 1979-01-26 1981-10-20 Firmenich Sa Process for the preparation of macrocyclic ketones
IT1166068B (it) 1979-02-23 1987-04-29 Ballestra Chim Procedimento perfezionato per la solfonazione a film in un reattore multitubolare a reattore multitubolare atto a realizare detto procedimento
US4491537A (en) 1983-07-08 1985-01-01 International Flavors & Fragrances Inc. Tertiary hydroxyl carboxaldehydes and organoleptic use thereof
DE3722566A1 (de) 1987-07-08 1989-01-19 Henkel Kgaa Verfahren zur kontinuierlichen ozonisierung von ungesaettigten organischen verbindungen
EP0555472B1 (en) 1991-08-06 1995-11-29 Lion Corporation Process for ozonizing unsaturated fatty acid or lower alkyl ester thereof and oxidative decomposition of the resulting ozonide
JP3271785B2 (ja) 1992-02-20 2002-04-08 長谷川香料株式会社 ８−ヒドロキシ−８−メチルノナナールを含有する香料組成物
US5650536A (en) * 1992-12-17 1997-07-22 Exxon Chemical Patents Inc. Continuous process for production of functionalized olefins
DK0707566T3 (da) 1993-07-09 2000-09-04 Theramex Hidtil ukendte strukturelle analoger til vitamin D
US5543565A (en) 1995-01-20 1996-08-06 Henkel Corporation Method for forming two terminal carboxylic acid groups from an ozonide
DE19532886A1 (de) 1995-09-06 1997-03-13 Haarmann & Reimer Gmbh Offenkettige olefinisch ungesättigte Verbindungen, Verfahren zu ihrer Herstellung und ihre Verwendung als Riechstoffe
US6287431B1 (en) 1997-03-21 2001-09-11 Lynntech International, Ltd. Integrated ozone generator system
CN1268107A (zh) 1997-06-27 2000-09-27 普罗格特-甘布尔公司 直链缩醛和缩酮香料前体
DE19741645A1 (de) 1997-09-22 1999-03-25 Bayer Ag Verfahren und Vorrichtung zur Oxidation organischer Verbindungen in flüssiger Phase unter Verwendung peroxidischer Oxidationsmittel
EP1095700A1 (de) 1999-10-29 2001-05-02 Dr. Frische GmbH Verfahren zur Durchführung einer Mehrphasenreaktion nach dem Gegenstromprinzip einer flüssigen und gasförmigen Phase und Vorrichtung zur Durchführung des Verfahrens
DE10010770C5 (de) 2000-03-04 2007-02-22 Celanese Chemicals Europe Gmbh Nichtkatalytisches Verfahren zur Herstellung geradkettiger aliphatischer Carbonsäuren aus Aldehyden
DE10010771C1 (de) 2000-03-04 2001-05-03 Celanese Chem Europe Gmbh Verfahren zur Herstellung aliphatischer Carbonsäuren aus Aldehyden
DE60109058T2 (de) 2000-12-12 2006-03-02 Lynntech International, Ltd., College Station Elektrochemische vorrichtung mit ausfahrbarer elektrode
AT500421A1 (de) 2000-12-14 2005-12-15 Dsm Fine Chem Austria Gmbh Verbessertes verfahren zur reinigung von ketonen, erhalten aus den korrespondierenden terpenen durch ozonolyse und reduktion
WO2003011802A1 (de) 2001-07-09 2003-02-13 Symrise Gmbh & Co. Kg ISO-β-BISABOLOL ALS DUFT-UND AROMASTOFF
KR101142653B1 (ko) 2004-02-09 2012-05-10 미츠비시 레이온 가부시키가이샤 α,β-불포화 카복실산의 제조방법
KR100843594B1 (ko) 2005-09-07 2008-07-03 주식회사 엘지화학 액상 산화 반응을 이용한 알데히드 화합물로부터의유기산의 제조 방법
EP1969131A1 (en) 2005-12-15 2008-09-17 Isobionics B.V. Process for the preparation of delta lactones
DE102005060816B3 (de) 2005-12-21 2007-03-29 Rudolf Aigner Verfahren zur Sulfonierung bzw. Sulfatierung von sulfonierbaren bzw. sulfatierbaren organischen Substanzen
DE102006021438A1 (de) 2006-05-09 2007-11-15 Cognis Ip Management Gmbh Verfahren zur Ozonolyse von ungesättigten Verbindungen
WO2008145683A1 (en) 2007-06-01 2008-12-04 Dsm Fine Chemicals Austria Nfg Gmbh & Co Kg Tube bundle falling film microreactor for performing gas liquid reactions
US7829342B2 (en) 2007-10-03 2010-11-09 The Board Of Trustees Of The Universiy Of Illinois Selective aliphatic C-H oxidation
US8425784B2 (en) 2007-11-05 2013-04-23 University Of Kansas Ozonolysis reactions in liquid CO2 and CO2-expanded solvents
EP2404666A1 (fr) * 2010-07-09 2012-01-11 Rhodia Opérations Module de transformation continue d'au moins un produit fluide, unité et procédé associés.
CN102653531B (zh) 2011-03-04 2014-08-13 上海爱普植物科技有限公司 一种马索亚内酯的合成方法
EP2683699B1 (de) 2011-03-08 2015-06-24 Sanofi Di- und trisubstituierte oxathiazinderivate, verfahren zu deren herstellung, ihre verwendung als medikament sowie sie enthaltendes arzneimittel und deren verwendung
US8912350B2 (en) 2011-06-23 2014-12-16 The Procter & Gamble Company Perfume systems
US8840705B2 (en) 2011-07-07 2014-09-23 Linde Aktiengesellschaft Methods for the ozonolysis of organic compounds
DE102011083285A1 (de) 2011-09-23 2013-03-28 Evonik Degussa Gmbh Ozonolyse von ungesättigten Fettsäuren und Derivaten davon
WO2013053102A1 (en) 2011-10-11 2013-04-18 Givaudan Sa Improvements in or relating to organic compounds
CN102795987A (zh) 2012-08-09 2012-11-28 西安近代化学研究所 3，3，3-三氟丙酸的制备方法
US9586883B2 (en) 2013-04-19 2017-03-07 California Institute Of Technology Aldehyde-selective wacker-type oxidation of unbiased alkenes
AP2016009125A0 (en) 2013-09-16 2016-04-30 Emergent Virology Llc Deoxynojirimycin derivatives and methods of their using
US9682914B2 (en) 2014-01-13 2017-06-20 P2 Science, Inc. Terpene-derived acids and esters and methods for preparing and using same
WO2015126936A1 (en) 2014-02-19 2015-08-27 P2 Science, Inc. Substituted delta-lactones and methods of preparing same
US10071941B2 (en) 2014-06-10 2018-09-11 P2 Science, Inc. Terpene-derived compounds and methods for preparing and using same
US20170247314A1 (en) 2014-08-06 2017-08-31 P2 Science, Inc. Fragrances from the esters of fatty acids
GB201421855D0 (en) 2014-12-09 2015-01-21 Givaudan Sa Improvements in or relating to organic compounds
WO2017223220A1 (en) 2016-06-21 2017-12-28 P2 Science, Inc. Flow-through reactors for the continuous quenching of peroxide mixtures and methods comprising the same
EP3512631B1 (en) 2016-09-16 2022-03-23 P2 Science, Inc. Uses of vanadium to oxidize aldehydes and ozonides

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010095669A1 (ja) 2009-02-17 2010-08-26 国立大学法人宇都宮大学 含酸素化合物の製造方法
JP2015529647A (ja) 2012-07-19 2015-10-08 ピー２ サイエンス，インコーポレイティド 還元および／または酸化された生成物流を発生させるためのオゾン分解操作
WO2015196019A1 (en) 2014-06-20 2015-12-23 P2 Science, Inc. Film ozonolysis in a tubular or multitubular reactor

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
Irfan, Muhammad; Glasnov, Toma N.; Kappe, C. Oliver，Continuous Flow Ozonolysis in a Laboratory Scale Reactor，Organic Letters ，2011年，13(5)，984-987
Lange, Gordon L.; Neidert, Eli，Preparation of diketoheptadecanolides and cyclohexadecanediones by thermolysis of a cyclic diperoxide，Journal of Organic Chemistry ，1975年，40(24)，3604-6
Roydhouse, M. D.; Ghaini, A.; Constantinou, A.; Cantu-Perez, A.; Motherwell, W. B.; Gavriilidis, A.，Ozonolysis in Flow Using Capillary Reactors，Organic Process Research & Development，2011年，15(5)，989-996

Also Published As

Publication number Publication date
US10668446B2 (en) 2020-06-02
EP3472124A1 (en) 2019-04-24
US20190091645A1 (en) 2019-03-28
WO2017223220A1 (en) 2017-12-28
JP2019524661A (ja) 2019-09-05
CA3026192A1 (en) 2017-12-28
EP3472124A4 (en) 2020-03-04

Similar Documents

Publication Publication Date Title
JP7028457B2 (ja) 過酸化物混合物の連続クエンチのためのフロースルー反応器およびそれを含む方法
JP7104083B2 (ja) 管式又は多管式反応器における膜オゾン分解
CN101443299B (zh) 用于直接氧化烷烃气体的方法
CN101835733B (zh) 氧化有机化合物的方法和装置
JP2019524661A5 (enExample)
US8524175B2 (en) Tandem reactor system having an injectively-mixed backmixing reaction chamber, tubular-reactor, and axially movable interface
US20070196252A1 (en) System For Direct-Oxygenation of Alkane Gases
CN101784511B (zh) 用于氧化有机化合物的方法和设备
US7687669B2 (en) Method for direct-oxygenation of alkane gases
WO2007133313A1 (en) System for direct-oxygenation of alkane gases
Wandell et al. Formation of alcohols and carbonyl compounds from hexane and cyclohexane with water in a liquid film plasma reactor
WO2001051443A2 (en) Method for increasing oxidation reactor production capacity
US20070167533A1 (en) Method for Direct-Oxygenation of Alkane Gases
CN101657257B (zh) 氧化脱金属方面的改进
JP6017710B2 (ja) 流通反応器を用いたケトマロン酸化合物の連続製造方法
US9073883B2 (en) Production of hexafluoropropylene oxide
RU2049086C1 (ru) Способ получения метанола
CN107954823B (zh) 一种连续生产2,3-二氯-1,1,1-三氟丙烷的光氯化反应系统及方法
CN105793227B (zh) 醛氧化方法
CN110818558A (zh) 利用微通道连续制备氯代特戊酰氯的方法及其装置
CN118715202A (zh) 用于生产烷基磺酸的方法
AU2022418834A1 (en) Novel process for the production of hydrogen peroxide
CN101016250A (zh) 一种生产1－氨基蒽醌的方法及装置
EP3453447A1 (en) Process for the preparation of alkanesulfonic acid
US20120149950A1 (en) Plant for the homogeneous oxidation of methane-containing gas and process for the oxidation of methane-containing gas

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20200109

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20200109

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20201210

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20201222

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20210318

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20210803

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20211102

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20211217

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20220111

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20220209

R150 Certificate of patent or registration of utility model

Ref document number: 7028457

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250