JP6920462B2 - オキシレスベラトロールのアルトカルプス・ヒルスタスからの新規な抽出方法 - Google Patents
オキシレスベラトロールのアルトカルプス・ヒルスタスからの新規な抽出方法 Download PDFInfo
- Publication number
- JP6920462B2 JP6920462B2 JP2019555560A JP2019555560A JP6920462B2 JP 6920462 B2 JP6920462 B2 JP 6920462B2 JP 2019555560 A JP2019555560 A JP 2019555560A JP 2019555560 A JP2019555560 A JP 2019555560A JP 6920462 B2 JP6920462 B2 JP 6920462B2
- Authority
- JP
- Japan
- Prior art keywords
- extract
- powder
- oxyresveratrol
- drying
- volume
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
- C07C37/84—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by crystallisation
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/045—Hydroxy compounds, e.g. alcohols; Salts thereof, e.g. alcoholates
- A61K31/05—Phenols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/60—Moraceae (Mulberry family), e.g. breadfruit or fig
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/028—Flow sheets
- B01D11/0284—Multistage extraction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0288—Applications, solvents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/37—Extraction at elevated pressure or temperature, e.g. pressurized solvent extraction [PSE], supercritical carbon dioxide extraction or subcritical water extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Veterinary Medicine (AREA)
- Pharmacology & Pharmacy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Epidemiology (AREA)
- Medicinal Chemistry (AREA)
- Botany (AREA)
- Physics & Mathematics (AREA)
- Microbiology (AREA)
- Medical Informatics (AREA)
- Biotechnology (AREA)
- Alternative & Traditional Medicine (AREA)
- Engineering & Computer Science (AREA)
- Mycology (AREA)
- Thermal Sciences (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Extraction Or Liquid Replacement (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/US2016/068161 WO2018118059A1 (en) | 2016-12-22 | 2016-12-22 | Novel method for extraction of oxyresveratrol from artocarpus hirsutus |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2020503387A JP2020503387A (ja) | 2020-01-30 |
| JP2020503387A5 JP2020503387A5 (https=) | 2021-02-18 |
| JP6920462B2 true JP6920462B2 (ja) | 2021-08-18 |
Family
ID=62627685
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2019555560A Expired - Fee Related JP6920462B2 (ja) | 2016-12-22 | 2016-12-22 | オキシレスベラトロールのアルトカルプス・ヒルスタスからの新規な抽出方法 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US20200039907A1 (https=) |
| EP (1) | EP3558283B1 (https=) |
| JP (1) | JP6920462B2 (https=) |
| CA (1) | CA3047702C (https=) |
| WO (1) | WO2018118059A1 (https=) |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060216253A1 (en) * | 2005-03-23 | 2006-09-28 | Time And Cross, Inc. | Whitening cosmetics containing morus alba extracts |
| US7253324B1 (en) * | 2007-01-23 | 2007-08-07 | Sami Labs Limited | Process for the synthesis of biologically active oxygenated compounds by dealkylation of the corresponding alkylethers |
| US20110021640A1 (en) * | 2009-07-27 | 2011-01-27 | Kailash Chandra Agarwal | Mechanism-based biochemical standardization of resveratrol products and their uses thereof |
| CN102942455B (zh) * | 2012-11-26 | 2014-08-13 | 苏州农业职业技术学院 | 一种从桑枝中提取氧化芪三酚的方法 |
| KR101480600B1 (ko) * | 2013-01-22 | 2015-01-08 | 경북대학교 산학협력단 | 레스베라트롤 유도체의 피부미백 용도 |
| KR101479902B1 (ko) * | 2013-06-17 | 2015-01-08 | 세종대학교산학협력단 | 유효성분 함량이 증대된 청미래덩굴 뿌리 추출물 제조방법 및 이 추출물을 함유하는 해독용 음료 조성물 |
| EP3204346B1 (en) * | 2014-10-07 | 2020-09-02 | Council of Scientific and Industrial Research | A process for extraction and separation of oxyresveratrol from artocarpus lakoocha roxb |
| CN105418381A (zh) * | 2015-12-04 | 2016-03-23 | 陕西嘉禾生物科技股份有限公司 | 一种氧化白藜芦醇的合成方法 |
-
2016
- 2016-12-22 CA CA3047702A patent/CA3047702C/en active Active
- 2016-12-22 WO PCT/US2016/068161 patent/WO2018118059A1/en not_active Ceased
- 2016-12-22 US US16/471,148 patent/US20200039907A1/en not_active Abandoned
- 2016-12-22 JP JP2019555560A patent/JP6920462B2/ja not_active Expired - Fee Related
- 2016-12-22 EP EP16924736.8A patent/EP3558283B1/en not_active Not-in-force
Also Published As
| Publication number | Publication date |
|---|---|
| US20200039907A1 (en) | 2020-02-06 |
| EP3558283B1 (en) | 2022-11-16 |
| CA3047702C (en) | 2021-05-18 |
| EP3558283A1 (en) | 2019-10-30 |
| EP3558283A4 (en) | 2020-08-12 |
| WO2018118059A1 (en) | 2018-06-28 |
| JP2020503387A (ja) | 2020-01-30 |
| CA3047702A1 (en) | 2018-06-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR20190084094A (ko) | 오록실린 a를 함유하는 조성물 및 이의 추출방법 | |
| CN104592330B (zh) | 一种从国槐中分离出的山奈酚衍生物及其制备方法和用途 | |
| JP2014534183A (ja) | インゲノールを単離する方法 | |
| JP6920462B2 (ja) | オキシレスベラトロールのアルトカルプス・ヒルスタスからの新規な抽出方法 | |
| JP2021506307A5 (https=) | ||
| CN104592185B (zh) | 荸荠皮提取槲皮素的方法 | |
| CN107753542B (zh) | 南美蟛蜞菊花抗氧化提取物及其制备方法和用途 | |
| JPS617285A (ja) | 精製サポニン抽出方法 | |
| CN106690320B (zh) | 一种高纯度茶多酚的制备方法 | |
| CN110935191B (zh) | 一种工业大麻蜡质的提取纯化方法 | |
| WO2022138915A1 (ja) | 精製ロズマリン酸含有組成物の製造方法 | |
| CN116270571B (zh) | 一种萜酸类化合物及其从金银花中分离的方法及其应用 | |
| CN106939006B (zh) | 一种从赛北紫堇中提取分离白毛茛碱的方法 | |
| CN103193750B (zh) | 一种利用大孔树脂xad7hp联合分离制备莽草酸和八角黄酮的方法 | |
| KR101949617B1 (ko) | 이리도이드 고함유 노니 부산물의 추출물 제조방법 | |
| CN106038652A (zh) | 菊花总黄酮的提取纯化方法 | |
| Faizi et al. | Host-plant effect on the chemical constituents of Cuscuta reflexa | |
| CN104004034B (zh) | 一种制备开环异落叶松脂素9’-O-β-木糖苷的方法 | |
| US6384246B1 (en) | Process for the preparation of maltol from plants belonging to the genus Abies | |
| CN116270615B (zh) | 一种具有抗菌活性的倍半萜内酰胺类化合物 | |
| CN107935824B (zh) | 一种从铁皮石斛中提取高纯度毛兰素的方法 | |
| WO2007066926A1 (en) | A mass production method of brazilein from caesalpinia sappan l | |
| CN110642824A (zh) | 土肉桂以水解技术制备抗氧成分山奈酚的方法 | |
| SU1261667A1 (ru) | Способ получени валирацила | |
| JP6294259B2 (ja) | β−アルブチンの製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20190826 |
|
| A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20200630 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20200811 |
|
| A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20201110 |
|
| A524 | Written submission of copy of amendment under article 19 pct |
Free format text: JAPANESE INTERMEDIATE CODE: A524 Effective date: 20210108 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20210624 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20210726 |
|
| R150 | Certificate of patent or registration of utility model |
Ref document number: 6920462 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| LAPS | Cancellation because of no payment of annual fees |