JP6873057B2 - 複合磁性体および製造方法 - Google Patents
複合磁性体および製造方法 Download PDFInfo
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- 239000002131 composite material Substances 0.000 title claims description 82
- 239000000696 magnetic material Substances 0.000 title claims description 79
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- 230000005291 magnetic effect Effects 0.000 claims description 135
- 239000002184 metal Substances 0.000 claims description 117
- 229910052751 metal Inorganic materials 0.000 claims description 117
- 239000000843 powder Substances 0.000 claims description 117
- 239000002245 particle Substances 0.000 claims description 83
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 30
- 239000011230 binding agent Substances 0.000 claims description 25
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 8
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 7
- 239000003125 aqueous solvent Substances 0.000 claims description 7
- 238000009826 distribution Methods 0.000 claims description 7
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 5
- 239000000377 silicon dioxide Substances 0.000 claims description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 3
- 239000000395 magnesium oxide Substances 0.000 claims description 3
- 238000013329 compounding Methods 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 230000000052 comparative effect Effects 0.000 description 23
- 238000000034 method Methods 0.000 description 16
- 230000035699 permeability Effects 0.000 description 15
- 239000006247 magnetic powder Substances 0.000 description 12
- 239000011248 coating agent Substances 0.000 description 11
- 238000000576 coating method Methods 0.000 description 11
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- 238000005859 coupling reaction Methods 0.000 description 9
- 238000011156 evaluation Methods 0.000 description 9
- 238000004891 communication Methods 0.000 description 8
- 230000007423 decrease Effects 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 230000005294 ferromagnetic effect Effects 0.000 description 5
- 239000010419 fine particle Substances 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 229920005989 resin Polymers 0.000 description 5
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- 229910045601 alloy Inorganic materials 0.000 description 3
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- 238000012856 packing Methods 0.000 description 2
- 229920000058 polyacrylate Polymers 0.000 description 2
- 230000001629 suppression Effects 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- 229910017060 Fe Cr Inorganic materials 0.000 description 1
- 229910002544 Fe-Cr Inorganic materials 0.000 description 1
- 229910017082 Fe-Si Inorganic materials 0.000 description 1
- 229910017133 Fe—Si Inorganic materials 0.000 description 1
- 229910003271 Ni-Fe Inorganic materials 0.000 description 1
- 239000006087 Silane Coupling Agent Substances 0.000 description 1
- 229910002796 Si–Al Inorganic materials 0.000 description 1
- 150000001768 cations Chemical group 0.000 description 1
- UPHIPHFJVNKLMR-UHFFFAOYSA-N chromium iron Chemical compound [Cr].[Fe] UPHIPHFJVNKLMR-UHFFFAOYSA-N 0.000 description 1
- 239000007822 coupling agent Substances 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- -1 for example Inorganic materials 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007257 malfunction Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 239000002923 metal particle Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 229910001928 zirconium oxide Inorganic materials 0.000 description 1
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
- H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
- H01F1/12—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials
- H01F1/14—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys
- H01F1/20—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of particles, e.g. powder
- H01F1/22—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of particles, e.g. powder pressed, sintered, or bound together
- H01F1/24—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of particles, e.g. powder pressed, sintered, or bound together the particles being insulated
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/05—Metallic powder characterised by the size or surface area of the particles
- B22F1/052—Metallic powder characterised by the size or surface area of the particles characterised by a mixture of particles of different sizes or by the particle size distribution
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/06—Metallic powder characterised by the shape of the particles
- B22F1/068—Flake-like particles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/10—Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
- B22F1/102—Metallic powder coated with organic material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/10—Metallic powder containing lubricating or binding agents; Metallic powder containing organic material
- B22F1/103—Metallic powder containing lubricating or binding agents; Metallic powder containing organic material containing an organic binding agent comprising a mixture of, or obtained by reaction of, two or more components other than a solvent or a lubricating agent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/16—Metallic particles coated with a non-metal
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
- H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
- H01F1/12—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials
- H01F1/14—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys
- H01F1/147—Alloys characterised by their composition
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- H01F41/00—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
- H01F41/02—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets
- H01F41/0206—Manufacturing of magnetic cores by mechanical means
- H01F41/0246—Manufacturing of magnetic circuits by moulding or by pressing powder
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- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
- H05K9/00—Screening of apparatus or components against electric or magnetic fields
- H05K9/0073—Shielding materials
- H05K9/0075—Magnetic shielding materials
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
- H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
- H01F1/12—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials
- H01F1/14—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys
- H01F1/20—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of particles, e.g. powder
- H01F1/22—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of particles, e.g. powder pressed, sintered, or bound together
- H01F1/24—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of particles, e.g. powder pressed, sintered, or bound together the particles being insulated
- H01F1/26—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of particles, e.g. powder pressed, sintered, or bound together the particles being insulated by macromolecular organic substances
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- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Nanotechnology (AREA)
- Physics & Mathematics (AREA)
- Electromagnetism (AREA)
- Soft Magnetic Materials (AREA)
- Powder Metallurgy (AREA)
Description
図1は本発明による複合磁性体の断面構造を示す模式図である。図1に示すように、本実施の形態に係る複合磁性体の構成は、扁平状の軟磁性金属粉末1と、軟磁性金属粉末の平均厚さよりも小さく、軟磁性金属粉末の表面に配する絶縁粒子2と、軟磁性金属粉末1および絶縁粒子2を分散保持する有機結合材3からなる。
軟磁性金属粉末としてカルボニル鉄粉、絶縁粒子としてジルコニア粒子を用いて実施の形態に示す複合磁性体を作製した。
扁平状の軟磁性金属粉末に絶縁粒子を被覆させない事以外、実施例1と同様にして、厚み100μmのシート状の複合磁性体を得た。シート状複合磁性体の表面抵抗は2.5×101Ω、シート密度は4.3g/ccであった。
2 絶縁粒子
3 有機結合剤
10、12 ε’
11、13 ε’’
21 電子部品
22 アンテナ
23 金属筐体
24 金属板
25 磁性シート
31 第1周波数特性
32 第2周波数特性
100 通信機器
110 反射領域
200 評価系
Claims (6)
- 扁平状の軟磁性金属粉末と、前記軟磁性金属粉末の平均厚さよりも小さく、前記軟磁性金属粉末の表面に、水性溶媒を乾燥させて配した絶縁粒子と、前記軟磁性金属粉末および前記絶縁粒子を分散保持する有機結合材を含む複合磁性体であって、
前記軟磁性金属粉末の厚さ方向の断面における前記軟磁性金属粉末の表面の長さ0.2μmあたり前記絶縁粒子を1個以上配し、
前記軟磁性金属粉末の比表面積をSp、前記絶縁粒子の比表面積をSz、前記絶縁粒子の積層数をnとすると、(Sz/2)/Sp=n(nは1)を満たすことを特徴とする複合磁性体。 - 前記軟磁性金属粉末の体積粒度分布の積算10%粒子径D10が2μm以上6μm以下、かつ積算90%粒子径D90が8μm以上27μm以下である、請求項1に記載の複合磁性体。
- 前記絶縁粒子が、アルミナ、シリカ、マグネシア、チタニア、ジルコニアの少なくとも1種を含む、請求項1または請求項2に記載の複合磁性体。
- 前記絶縁粒子の体積抵抗率が1×1013Ω・cm以上である、請求項1乃至請求項3のいずれか1項に記載の複合磁性体。
- 前記絶縁粒子の体積粒度分布のメジアン径D50が10nm以上70nm以下である、請求項1乃至請求項4のいずれか1項に記載の複合磁性体。
- 扁平状の軟磁性金属粉末を、前記軟磁性金属粉末の平均厚さよりも小さい絶縁粒子を水性溶媒に分散させたpH>7.0のゾルに浸漬した後、前記水性溶媒を乾燥させて前記軟磁性金属粉末の表面に前記絶縁粒子を被覆し、前記軟磁性金属粉末を有機結合材と混練、分散して、前記軟磁性金属粉末の厚さ方向の断面における前記軟磁性金属粉末の表面の長さ0.2μmあたり前記絶縁粒子を1個以上配したシート状に成形することを含み、
前記軟磁性金属粉末の比表面積をSp、前記絶縁粒子の比表面積をSz、前記絶縁粒子の積層数をnとすると、(Sz/2)/Sp=n(nは1)を満たすように、前記軟磁性金属粉末と前記絶縁粒子の配合比を調整することを特徴とする複合磁性体の製造方法。
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JP2016023273 | 2016-02-10 | ||
JP2016023273 | 2016-02-10 | ||
PCT/JP2016/063345 WO2017138158A1 (ja) | 2016-02-10 | 2016-04-28 | 複合磁性体および製造方法 |
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JPWO2017138158A1 JPWO2017138158A1 (ja) | 2018-12-27 |
JP6873057B2 true JP6873057B2 (ja) | 2021-05-19 |
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US (1) | US11756714B2 (ja) |
JP (1) | JP6873057B2 (ja) |
KR (1) | KR102369203B1 (ja) |
CN (1) | CN108604487A (ja) |
TW (1) | TWI642070B (ja) |
WO (1) | WO2017138158A1 (ja) |
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JP7283031B2 (ja) * | 2017-03-09 | 2023-05-30 | Tdk株式会社 | 圧粉磁心 |
CN114369762B (zh) * | 2022-01-07 | 2022-10-18 | 鞍钢股份有限公司 | 一种复合磁性金属粉末材料及其制备方法与用途 |
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US3568554A (en) * | 1967-11-13 | 1971-03-09 | Core Memories Ltd | Magnetic core forming system |
JP4065578B2 (ja) * | 1996-09-12 | 2008-03-26 | Necトーキン株式会社 | 電磁干渉抑制体 |
JPH10335128A (ja) | 1997-03-31 | 1998-12-18 | Tdk Corp | 圧粉コア用強磁性粉末、圧粉コアおよびその製造方法 |
US6102980A (en) * | 1997-03-31 | 2000-08-15 | Tdk Corporation | Dust core, ferromagnetic powder composition therefor, and method of making |
KR100335128B1 (ko) | 1999-11-22 | 2002-05-04 | 박종섭 | 반도체소자 제조를 위한 이온주입장치 |
JP4684461B2 (ja) | 2000-04-28 | 2011-05-18 | パナソニック株式会社 | 磁性素子の製造方法 |
JP3865601B2 (ja) * | 2001-06-12 | 2007-01-10 | 日東電工株式会社 | 電磁波抑制体シート |
JP4655540B2 (ja) * | 2004-08-06 | 2011-03-23 | 株式会社豊田中央研究所 | 表面層被覆金属及び圧粉体 |
JP5145923B2 (ja) * | 2007-12-26 | 2013-02-20 | パナソニック株式会社 | 複合磁性材料 |
JP2010080508A (ja) * | 2008-09-24 | 2010-04-08 | Daihatsu Motor Co Ltd | 複合軟磁性材料および複合軟磁性材料の製造方法 |
JP5032711B1 (ja) | 2011-07-05 | 2012-09-26 | 太陽誘電株式会社 | 磁性材料およびそれを用いたコイル部品 |
JP5082002B1 (ja) * | 2011-08-26 | 2012-11-28 | 太陽誘電株式会社 | 磁性材料およびコイル部品 |
JP5822146B2 (ja) | 2013-03-29 | 2015-11-24 | パウダーテック株式会社 | ノイズ抑制用複合磁性粉 |
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- 2016-04-28 US US16/074,424 patent/US11756714B2/en active Active
- 2016-04-28 CN CN201680081129.7A patent/CN108604487A/zh active Pending
- 2016-04-28 KR KR1020187023622A patent/KR102369203B1/ko active IP Right Grant
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TW201729223A (zh) | 2017-08-16 |
JPWO2017138158A1 (ja) | 2018-12-27 |
WO2017138158A1 (ja) | 2017-08-17 |
KR20180111851A (ko) | 2018-10-11 |
US11756714B2 (en) | 2023-09-12 |
US20190035525A1 (en) | 2019-01-31 |
KR102369203B1 (ko) | 2022-02-28 |
TWI642070B (zh) | 2018-11-21 |
CN108604487A (zh) | 2018-09-28 |
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