JP6799581B2 - モノマー生成で使用するための材料の不活性度を決定する方法 - Google Patents

モノマー生成で使用するための材料の不活性度を決定する方法 Download PDF

Info

Publication number
JP6799581B2
JP6799581B2 JP2018506399A JP2018506399A JP6799581B2 JP 6799581 B2 JP6799581 B2 JP 6799581B2 JP 2018506399 A JP2018506399 A JP 2018506399A JP 2018506399 A JP2018506399 A JP 2018506399A JP 6799581 B2 JP6799581 B2 JP 6799581B2
Authority
JP
Japan
Prior art keywords
pta
acrylic acid
acrolein
inert material
inert
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2018506399A
Other languages
English (en)
Japanese (ja)
Other versions
JP2018525384A (ja
JP2018525384A5 (enExample
Inventor
ジンスオ・シュー
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rohm and Haas Co
Original Assignee
Rohm and Haas Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rohm and Haas Co filed Critical Rohm and Haas Co
Publication of JP2018525384A publication Critical patent/JP2018525384A/ja
Publication of JP2018525384A5 publication Critical patent/JP2018525384A5/ja
Application granted granted Critical
Publication of JP6799581B2 publication Critical patent/JP6799581B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/35Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/86Signal analysis
    • G01N30/8675Evaluation, i.e. decoding of the signal into analytical information
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N31/00Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
    • G01N31/10Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using catalysis
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/22Fuels; Explosives
    • G01N33/227Explosives, e.g. combustive properties thereof
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/44Resins; Plastics; Rubber; Leather
    • G01N33/442Resins; Plastics

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Pathology (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Medicinal Chemistry (AREA)
  • Food Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Combustion & Propulsion (AREA)
  • Library & Information Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Molecular Biology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2018506399A 2015-08-24 2016-08-22 モノマー生成で使用するための材料の不活性度を決定する方法 Active JP6799581B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201562209003P 2015-08-24 2015-08-24
US62/209,003 2015-08-24
PCT/US2016/047977 WO2017035055A1 (en) 2015-08-24 2016-08-22 Method of determining the inertness of materials for use in monomer production

Publications (3)

Publication Number Publication Date
JP2018525384A JP2018525384A (ja) 2018-09-06
JP2018525384A5 JP2018525384A5 (enExample) 2020-09-10
JP6799581B2 true JP6799581B2 (ja) 2020-12-16

Family

ID=56801891

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2018506399A Active JP6799581B2 (ja) 2015-08-24 2016-08-22 モノマー生成で使用するための材料の不活性度を決定する方法

Country Status (6)

Country Link
US (1) US10968155B2 (enExample)
EP (1) EP3341350B1 (enExample)
JP (1) JP6799581B2 (enExample)
CN (1) CN107848934B (enExample)
BR (1) BR112018002552B1 (enExample)
WO (1) WO2017035055A1 (enExample)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3341351B1 (en) * 2015-08-24 2019-10-02 Rohm and Haas Company Method of determining the inertness of materials for use in monomer production

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS52108917A (en) * 1976-03-11 1977-09-12 Nippon Shokubai Kagaku Kogyo Co Ltd Preparation of acrylic acid by vapor-phase catalytic oxidation of prop ylene
JPS58126831A (ja) * 1982-01-22 1983-07-28 Nippon Shokubai Kagaku Kogyo Co Ltd メタクリル酸の捕集方法
JPH0714894B2 (ja) * 1986-04-24 1995-02-22 日本化薬株式会社 メタクリル酸の製造方法
JP2504777B2 (ja) * 1987-06-27 1996-06-05 三井東圧化学株式会社 反応ガスの急冷方法
DE3721865A1 (de) * 1987-07-02 1989-01-12 Basf Ag Verfahren zur herstellung von methacrylsaeure
JPH0813778B2 (ja) * 1988-07-11 1996-02-14 住友化学工業株式会社 メタクリル酸の製造方法
US5532199A (en) 1992-06-19 1996-07-02 Mitsubishi Rayon Co., Ltd. Carrier-supported catalyst for the synthesis of unsaturated aldehydes and unsaturated carboxylic acids and process for preparing the same
JP3786297B2 (ja) 1995-03-03 2006-06-14 日本化薬株式会社 触媒の製造方法
DE59602040D1 (de) * 1995-03-10 1999-07-08 Basf Ag Verfahren der kontinuierlich betriebenen heterogen katalysierten Gasphasenoxidation von Propylen zu Acrolein, Acrylsäure oder deren Gemisch
JP3948798B2 (ja) * 1997-10-27 2007-07-25 株式会社日本触媒 アクリル酸の製造方法
SG81982A1 (en) 1998-05-18 2001-07-24 Nippon Catalytic Chem Ind Method for production of acrolein and acrylic acid
US6762148B2 (en) 1999-09-17 2004-07-13 Nippon Kayaku Kabushiki Kaisha Catalyst process of making
JP3744751B2 (ja) * 1999-12-08 2006-02-15 株式会社日本触媒 担体、複合酸化物触媒、およびアクリル酸の製造方法
US6627445B1 (en) * 1999-12-15 2003-09-30 Uop Llc Process for simultaneously evaluating a plurality of catalysts
CN100378050C (zh) 2001-12-28 2008-04-02 三菱化学株式会社 汽相催化氧化方法
DE10313209A1 (de) * 2003-03-25 2004-03-04 Basf Ag Verfahren der heterogen katalysierten partiellen Gasphasenoxidation von Propen zu Acrylsäure
US7553986B2 (en) * 2003-12-23 2009-06-30 Rohm And Haas Company Process for the selective (amm)oxidation of lower molecular weight alkanes and alkenes
DE102004025445A1 (de) * 2004-05-19 2005-02-10 Basf Ag Verfahren zum Langzeitbetrieb einer heterogen katalysierten Gasphasenpartialoxidation wenigstens einer organischen Verbindung
JP4947917B2 (ja) 2005-04-18 2012-06-06 株式会社日本触媒 気相接触酸化用の固定床反応器およびアクロレインまたはアクリル酸の製造方法
DE102006000996A1 (de) 2006-01-05 2007-07-12 Basf Ag Verfahren der heterogen katalysierten Gasphasen-Partialoxidation wenigstens einer organischen Ausgangsverbindung
EP1734030A1 (de) 2006-01-18 2006-12-20 BASF Aktiengesellschaft Verfahren zum Langzeitbetrieb einer heterogen katalysierten partiellen Gasphasenoxidation einer organischen Ausgangsverbindung
US20090042723A1 (en) * 2007-02-06 2009-02-12 Kun Wang Process for preparing mixed metal oxide catalysts
BRPI0913336A2 (pt) 2008-06-02 2015-11-24 Nippon Kayaku Kk catalisador e método de produção de aldeído insaturado e ácido carboxílico insaturado
MX2013003910A (es) * 2010-10-07 2013-06-07 Rohm & Haas Proceso para la produccion de ester de acido metacrilico.
BR112014008712A2 (pt) * 2011-10-18 2017-04-25 Rohm & Haas processo
US9440903B2 (en) 2012-09-24 2016-09-13 Arkema Inc. Shell and tube oxidation reactor with improved resistance to fouling
CN103721756B (zh) * 2012-10-12 2015-10-28 上海华谊丙烯酸有限公司 催化剂载体及其制备方法、复合氧化物催化剂
US10035747B2 (en) * 2014-08-01 2018-07-31 Nippon Shokubai Co., Ltd. Method for recovering inert material and method for producing acrylic acid using inert material recovered by said method
US10159907B2 (en) * 2018-06-08 2018-12-25 Elliot Kremerman Laminar flow distribution adapter

Also Published As

Publication number Publication date
BR112018002552A2 (pt) 2018-09-25
CN107848934B (zh) 2021-07-20
EP3341350A1 (en) 2018-07-04
JP2018525384A (ja) 2018-09-06
US10968155B2 (en) 2021-04-06
WO2017035055A1 (en) 2017-03-02
CN107848934A (zh) 2018-03-27
EP3341350B1 (en) 2019-09-25
BR112018002552B1 (pt) 2021-07-13
US20180244597A1 (en) 2018-08-30

Similar Documents

Publication Publication Date Title
JP4050184B2 (ja) 脂肪族カルボン酸の製造方法
JP5094459B2 (ja) アルカンを不飽和カルボン酸に変換するための改良法
CN101579630A (zh) 制备用于生产不饱和醛和/或不饱和羧酸的催化剂的方法以及制备不饱和醛和/或不饱和羧酸的方法
KR20120039003A (ko) 글리세롤로부터 생물자원 아크릴산을 제조하는 방법
US8299299B2 (en) Process for separating acrylic acid present as a main constituent and glyoxal present as a by-product in a product gas mixture of a partial heterogeneously catalyzed gas phase oxidation of a C3 precursor compound of acrylic acid
JP6799581B2 (ja) モノマー生成で使用するための材料の不活性度を決定する方法
JP6799582B2 (ja) モノマー生成で使用するための材料の不活性度を決定する方法
JP7651589B2 (ja) 液相pに存在するアクリル酸の望ましくないフリーラジカル重合を抑制する方法
JP7384519B2 (ja) 液相pに存在するアクリル酸の望ましくないラジカル重合を抑制するための方法
JP3938905B2 (ja) (メタ)アクリル酸の製造方法
US10577299B2 (en) Methods for using macroporous inert materials in monomer production
JP4995479B2 (ja) α,β−不飽和カルボン酸およびα,β−不飽和カルボン酸骨格を有する酸無水物の製造方法
KR102893876B1 (ko) 액상 p 중 존재하는 아크릴산의 원치않는 라디칼 중합의 억제 방법
JP3997782B2 (ja) (メタ)アクリル酸の製造方法
JP2010506881A (ja) アクリル酸のc3前駆体化合物の不均一系触媒気相部分酸化の生成物ガス混合物中に含有されるアクリル酸および安息香酸の分離法

Legal Events

Date Code Title Description
RD02 Notification of acceptance of power of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7422

Effective date: 20180220

RD04 Notification of resignation of power of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7424

Effective date: 20180514

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20190815

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20200520

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20200529

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20200731

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20200731

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20201104

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20201120

R150 Certificate of patent or registration of utility model

Ref document number: 6799581

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

S802 Written request for registration of partial abandonment of right

Free format text: JAPANESE INTERMEDIATE CODE: R311802

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250