JP6795521B2 - 単結晶ダイヤモンド、単結晶ダイヤモンドの製造方法およびそれに用いられる化学気相堆積装置 - Google Patents

単結晶ダイヤモンド、単結晶ダイヤモンドの製造方法およびそれに用いられる化学気相堆積装置 Download PDF

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JP6795521B2
JP6795521B2 JP2017562857A JP2017562857A JP6795521B2 JP 6795521 B2 JP6795521 B2 JP 6795521B2 JP 2017562857 A JP2017562857 A JP 2017562857A JP 2017562857 A JP2017562857 A JP 2017562857A JP 6795521 B2 JP6795521 B2 JP 6795521B2
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diamond
crystal
single crystal
main surface
defect
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JPWO2017126561A1 (ja
Inventor
拓也 野原
拓也 野原
夏生 辰巳
夏生 辰巳
西林 良樹
良樹 西林
角谷 均
均 角谷
小林 豊
豊 小林
暁彦 植田
暁彦 植田
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Sumitomo Electric Hardmetal Corp
Sumitomo Electric Industries Ltd
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Sumitomo Electric Hardmetal Corp
Sumitomo Electric Industries Ltd
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    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
    • C30B25/02Epitaxial-layer growth
    • C30B25/18Epitaxial-layer growth characterised by the substrate
    • C30B25/20Epitaxial-layer growth characterised by the substrate the substrate being of the same materials as the epitaxial layer
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/01Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes on temporary substrates, e.g. substrates subsequently removed by etching
    • AHUMAN NECESSITIES
    • A44HABERDASHERY; JEWELLERY
    • A44CPERSONAL ADORNMENTS, e.g. JEWELLERY; COINS
    • A44C27/00Making jewellery or other personal adornments
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    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/25Diamond
    • C01B32/26Preparation
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    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/02Pretreatment of the material to be coated
    • C23C16/0227Pretreatment of the material to be coated by cleaning or etching
    • C23C16/0236Pretreatment of the material to be coated by cleaning or etching by etching with a reactive gas
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    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/22Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
    • C23C16/26Deposition of carbon only
    • C23C16/27Diamond only
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    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/22Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
    • C23C16/26Deposition of carbon only
    • C23C16/27Diamond only
    • C23C16/274Diamond only using microwave discharges
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    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/22Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
    • C23C16/26Deposition of carbon only
    • C23C16/27Diamond only
    • C23C16/277Diamond only using other elements in the gas phase besides carbon and hydrogen; using other elements besides carbon, hydrogen and oxygen in case of use of combustion torches; using other elements besides carbon, hydrogen and inert gas in case of use of plasma jets
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    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/458Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for supporting substrates in the reaction chamber
    • C23C16/4581Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for supporting substrates in the reaction chamber characterised by material of construction or surface finish of the means for supporting the substrate
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    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
    • C30B25/02Epitaxial-layer growth
    • C30B25/08Reaction chambers; Selection of materials therefor
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    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
    • C30B25/02Epitaxial-layer growth
    • C30B25/12Substrate holders or susceptors
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    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
    • C30B25/02Epitaxial-layer growth
    • C30B25/18Epitaxial-layer growth characterised by the substrate
    • C30B25/186Epitaxial-layer growth characterised by the substrate being specially pre-treated by, e.g. chemical or physical means
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    • C30B25/00Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
    • C30B25/02Epitaxial-layer growth
    • C30B25/18Epitaxial-layer growth characterised by the substrate
    • C30B25/20Epitaxial-layer growth characterised by the substrate the substrate being of the same materials as the epitaxial layer
    • C30B25/205Epitaxial-layer growth characterised by the substrate the substrate being of the same materials as the epitaxial layer the substrate being of insulating material
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    • C30B29/00Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/02Elements
    • C30B29/04Diamond
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    • H01L21/02365Forming inorganic semiconducting materials on a substrate
    • H01L21/02367Substrates
    • H01L21/0237Materials
    • H01L21/02373Group 14 semiconducting materials
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    • H01L21/02518Deposited layers
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    • H01L21/0259Microstructure
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    • H01L21/02612Formation types
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  • Chemical & Material Sciences (AREA)
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  • Materials Engineering (AREA)
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  • Geology (AREA)
  • Combustion & Propulsion (AREA)
  • Plasma & Fusion (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Chemical Vapour Deposition (AREA)
JP2017562857A 2016-01-22 2017-01-18 単結晶ダイヤモンド、単結晶ダイヤモンドの製造方法およびそれに用いられる化学気相堆積装置 Active JP6795521B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2016010560 2016-01-22
JP2016010560 2016-01-22
PCT/JP2017/001578 WO2017126561A1 (fr) 2016-01-22 2017-01-18 Diamant monocristallin, procédé destiné à la fabrication d'un diamant monocristallin, et dispositif de dépôt chimique en phase vapeur associé

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Publication Number Publication Date
JPWO2017126561A1 JPWO2017126561A1 (ja) 2018-11-15
JP6795521B2 true JP6795521B2 (ja) 2020-12-02

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US (1) US10737943B2 (fr)
EP (1) EP3406768B1 (fr)
JP (1) JP6795521B2 (fr)
KR (1) KR102653291B1 (fr)
CN (1) CN108474136B (fr)
SG (1) SG11201805526PA (fr)
WO (1) WO2017126561A1 (fr)

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Publication number Priority date Publication date Assignee Title
CN110387534A (zh) * 2019-09-05 2019-10-29 蓬莱市超硬复合材料有限公司 一种纳米金刚石涂层硬质合金材料的制备方法
CN111099586B (zh) * 2019-11-27 2022-05-31 中国科学院金属研究所 一种纳米金刚石中高亮度硅空位色心的制备方法
US20230383387A1 (en) * 2020-10-22 2023-11-30 Sumitomo Electric Hardmetal Corp. Diamond sintered material and tool including diamond sintered material
CN113373512B (zh) * 2021-05-24 2022-02-11 北京科技大学 基于铱-石墨烯结构化缓冲层的单晶金刚石外延生长方法

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JP3041844B2 (ja) 1995-08-11 2000-05-15 住友電気工業株式会社 成膜又はエッチング装置
DE19826681B4 (de) * 1998-06-16 2004-02-12 Marquardt, Niels, Dr. Verfahren zur Herstellung von neuartigen Getter-Werkstoffen in Form dünner metallischer und kohlenstoffhaltiger nanostrukturierter Schichten und Verwendung derselben zur Hochvakuumerzeugung und Gasspeicherung
EP1632590B1 (fr) 2000-06-15 2017-01-11 Element Six Technologies Limited Couche de diamant monocristallin épaisse, procédé de fabrication, et pierres précieuses produites à partir de cette couche
CA2549283A1 (fr) * 2004-11-05 2006-05-11 Sumitomo Electric Industries, Ltd. Diamant monocristallin
JP5594613B2 (ja) 2005-04-15 2014-09-24 住友電気工業株式会社 単結晶ダイヤモンドおよびその製造方法
AU2006251553B2 (en) * 2005-05-25 2011-09-08 Carnegie Institution Of Washington Colorless single-crystal CVD diamond at rapid growth rate
JP5323492B2 (ja) * 2005-12-09 2013-10-23 エレメント シックス テクノロジーズ (プロプライアタリー) リミテッド 高結晶品質の合成ダイヤモンド
JP2009132948A (ja) 2007-11-28 2009-06-18 Toyota Motor Corp プラズマcvd装置
EP2360289A1 (fr) * 2010-02-23 2011-08-24 Saint-Gobain Glass France Dispositif et procédé de dépot d'une couche composée d'au moins deux composants sur un substrat
GB201021985D0 (en) 2010-12-24 2011-02-02 Element Six Ltd Dislocation engineering in single crystal synthetic diamond material
GB201107552D0 (en) 2011-05-06 2011-06-22 Element Six Ltd Diamond sensors, detectors, and quantum devices
GB201320304D0 (en) * 2013-11-18 2014-01-01 Element Six Ltd Methods of fabricating synthetic diamond materials using microwave plasma actived chemical vapour deposition techniques and products obtained using said
JP6708972B2 (ja) * 2014-07-22 2020-06-10 住友電気工業株式会社 単結晶ダイヤモンドおよびその製造方法、単結晶ダイヤモンドを含む工具、ならびに単結晶ダイヤモンドを含む部品
US10697088B2 (en) * 2014-10-29 2020-06-30 Sumitomo Electric Industries, Ltd. Single-crystal diamond material, and tool, radiation temperature monitor, and infrared optical component including said diamond material

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KR102653291B1 (ko) 2024-03-29
KR20180104617A (ko) 2018-09-21
EP3406768A4 (fr) 2019-08-28
EP3406768B1 (fr) 2023-09-20
US10737943B2 (en) 2020-08-11
CN108474136A (zh) 2018-08-31
US20190031515A1 (en) 2019-01-31
WO2017126561A1 (fr) 2017-07-27
JPWO2017126561A1 (ja) 2018-11-15
EP3406768A1 (fr) 2018-11-28
SG11201805526PA (en) 2018-08-30
CN108474136B (zh) 2021-05-28

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