JP6702974B2 - 光学活性カルボニル化合物を合成する方法 - Google Patents

光学活性カルボニル化合物を合成する方法 Download PDF

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JP6702974B2
JP6702974B2 JP2017532651A JP2017532651A JP6702974B2 JP 6702974 B2 JP6702974 B2 JP 6702974B2 JP 2017532651 A JP2017532651 A JP 2017532651A JP 2017532651 A JP2017532651 A JP 2017532651A JP 6702974 B2 JP6702974 B2 JP 6702974B2
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formula
group
alkyl
compound
cycloalkyl
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JP2017537965A (ja
JP2017537965A5 (cg-RX-API-DMAC7.html
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シェルヴィース，マティアス
パチェロ，ロッコ
ハイドリヒ，グンナー
ヴェグナー，ギュンター
テッベン，ゲルト−ディーター
ハウブナー，マルティン
ケラー，アンドレアス
バイ，オリヴァー
レンツ，シュテファニー
ゼーベル，ゲオルク
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/17—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds
    • C07C29/172—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrogenation of carbon-to-carbon double or triple bonds with the obtention of a fully saturated alcohol
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/56—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by isomerisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/62—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by hydrogenation of carbon-to-carbon double or triple bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07—Optical isomers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2017532651A 2014-12-19 2015-12-18 光学活性カルボニル化合物を合成する方法 Active JP6702974B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP14199410 2014-12-19
EP14199410.3 2014-12-19
PCT/EP2015/080392 WO2016097242A1 (de) 2014-12-19 2015-12-18 Verfahren zur herstellung optisch aktiver carbonylverbindungen

Publications (3)

Publication Number Publication Date
JP2017537965A JP2017537965A (ja) 2017-12-21
JP2017537965A5 JP2017537965A5 (cg-RX-API-DMAC7.html) 2019-02-07
JP6702974B2 true JP6702974B2 (ja) 2020-06-03

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JP2017532651A Active JP6702974B2 (ja) 2014-12-19 2015-12-18 光学活性カルボニル化合物を合成する方法

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US (3) US9975837B2 (cg-RX-API-DMAC7.html)
EP (2) EP3489213B1 (cg-RX-API-DMAC7.html)
JP (1) JP6702974B2 (cg-RX-API-DMAC7.html)
CN (1) CN107250091B (cg-RX-API-DMAC7.html)
ES (2) ES2883557T3 (cg-RX-API-DMAC7.html)
MX (1) MX375969B (cg-RX-API-DMAC7.html)
WO (1) WO2016097242A1 (cg-RX-API-DMAC7.html)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107735392B (zh) 2015-05-04 2021-12-03 巴斯夫欧洲公司 制备甜瓜醛的方法
WO2017064064A1 (en) 2015-10-12 2017-04-20 Basf Se Hydroformylation process for producing 1,6-disubstituted hexane derivatives
BR112018011459A2 (pt) 2015-12-08 2018-11-27 Basf Se processo, material zeolítico, e, uso de um material zeolítico.
CN109311789B (zh) 2016-06-07 2023-04-04 巴斯夫欧洲公司 制备2,3-不饱和醇的方法
ES2867052T3 (es) 2016-06-29 2021-10-20 Basf Se Procedimiento de preparación de aldehídos alfa, beta insaturados por oxidación de alcoholes en presencia de una fase líquida
US10669222B2 (en) 2016-10-06 2020-06-02 Basf Se Process for enriching enantiomers from an enantiomer mixture
MX2020006560A (es) * 2017-12-21 2020-09-24 Basf Se Proceso para la preparacion de aldehidos alfa-beta insaturados mediante oxidacion de alcoholes en presencia de una fase liquida.
JP7433298B2 (ja) * 2018-09-05 2024-02-19 ビーエーエスエフ ソシエタス・ヨーロピア 気／液二相高圧反応を行う方法
BR112021001695B1 (pt) 2018-09-05 2023-12-26 Basf Se Processos para produção contínua de um composto de carbonila e para produzir mentol opticamente ativo
ES2934908T3 (es) 2018-09-05 2023-02-27 Basf Se Reactor para llevar a cabo una reacción bifásica de gas/líquido de alta presión con un medio espumante
CN112654421B (zh) * 2018-09-05 2023-05-09 巴斯夫欧洲公司 用于进行两种不同密度的不混溶流体之间的反应的反应器
EP3976569B1 (en) * 2019-05-27 2023-11-08 DSM IP Assets B.V. Selective hydrogenation of alkynols to alkenols in the presence of a phosphorus compound
CN110872217A (zh) * 2019-12-09 2020-03-10 万华化学集团股份有限公司 一种光学活性的香茅醛的制备方法
WO2021114021A1 (zh) 2019-12-09 2021-06-17 万华化学集团股份有限公司 一种光学活性的香茅醛的制备方法
CN111056932A (zh) * 2019-12-09 2020-04-24 万华化学集团股份有限公司 一种制备光学活性香茅醛的方法
CN111004102B (zh) * 2019-12-23 2022-11-04 万华化学集团股份有限公司 一种制备光学活性香茅醛的方法及用于该方法的催化剂
CN111056933B (zh) * 2019-12-24 2022-11-08 万华化学集团股份有限公司 一种制备光学活性香茅醛的方法及用于该方法的催化剂体系
CN111792986B (zh) * 2020-07-22 2022-09-20 万华化学集团股份有限公司 一种制备r-香茅醛的方法
CN112142583B (zh) * 2020-10-26 2022-07-26 万华化学集团股份有限公司 一种香叶醛制备橙花醛的方法
CN113527367B (zh) * 2021-07-14 2022-08-02 南开沧州渤海新区绿色化工研究有限公司 一种含四（3,5-二三氟甲基苯基）硼阴离子的手性双膦配体铑络合物和制备方法及应用
WO2025011972A1 (en) 2023-07-07 2025-01-16 Basf Se Photoisomerization of geranial and neral

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4115417A (en) * 1975-10-16 1978-09-19 Hoffmann-La Roche Inc. Asymmetric hydrogenation catalyzed by rhodium complexes of chiral tertiary phosphines
JPS5278812A (en) 1975-12-26 1977-07-02 Nikki Chem Co Ltd Selective production method of saturated aldehyde
FR2396735A1 (fr) * 1977-07-04 1979-02-02 Rhone Poulenc Ind Procede de preparation de citronellal optiquement actif
DE19854637A1 (de) 1998-11-26 2000-05-31 Basf Ag Reaktor zur kontinuierlichen Durchführung von Gas-Flüssig-, Flüssig-Flüssig- oder Gas-Flüssig-Fest-Reaktionen
JP4676617B2 (ja) 2001-01-18 2011-04-27 高砂香料工業株式会社 イソプレゴールの製造方法
DE102004049631A1 (de) 2004-10-11 2006-04-20 Basf Ag Verfahren zur Herstellung optisch aktiver Carbonylverbindungen
DE102004057277A1 (de) * 2004-11-26 2006-06-01 Basf Ag Verfahren zur Herstellung von Menthol
JP5479320B2 (ja) * 2007-04-25 2014-04-23 ビーエーエスエフ ソシエタス・ヨーロピア 光学活性カルボニル化合物の調製方法
AR070176A1 (es) * 2008-01-17 2010-03-17 Novartis Ag Procesos de sintesis de inhibidores de nep, compuestos intermediarios y uso de los mismos en la sintesis
EP2543437A4 (en) * 2010-03-04 2014-09-03 Takasago Perfumery Co Ltd HOMOGENEOUS ASYMMETRIC HYDROGENATION CATALYST

Also Published As

Publication number Publication date
US20180244598A1 (en) 2018-08-30
US20180057437A1 (en) 2018-03-01
MX2017008170A (es) 2017-09-18
ES2727384T3 (es) 2019-10-15
EP3489213B1 (de) 2021-04-28
JP2017537965A (ja) 2017-12-21
EP3489213A1 (de) 2019-05-29
EP3233778B1 (de) 2019-02-20
CN107250091B (zh) 2021-05-04
US10301244B2 (en) 2019-05-28
CN107250091A (zh) 2017-10-13
ES2883557T3 (es) 2021-12-09
WO2016097242A1 (de) 2016-06-23
MX375969B (es) 2025-03-06
USRE49036E1 (en) 2022-04-19
US9975837B2 (en) 2018-05-22
EP3233778A1 (de) 2017-10-25

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