JP6684659B2 - 金属表面コーティング用組成物および端子付き被覆電線 - Google Patents
金属表面コーティング用組成物および端子付き被覆電線 Download PDFInfo
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- JP6684659B2 JP6684659B2 JP2016115798A JP2016115798A JP6684659B2 JP 6684659 B2 JP6684659 B2 JP 6684659B2 JP 2016115798 A JP2016115798 A JP 2016115798A JP 2016115798 A JP2016115798 A JP 2016115798A JP 6684659 B2 JP6684659 B2 JP 6684659B2
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
- C10M2223/042—Metal salts thereof
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- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
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- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
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- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
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- C10N2010/00—Metal present as such or in compounds
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
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- H01R4/10—Electrically-conductive connections between two or more conductive members in direct contact, i.e. touching one another; Means for effecting or maintaining such contact; Electrically-conductive connections having two or more spaced connecting locations for conductors and using contact members penetrating insulation effected solely by twisting, wrapping, bending, crimping, or other permanent deformation
- H01R4/18—Electrically-conductive connections between two or more conductive members in direct contact, i.e. touching one another; Means for effecting or maintaining such contact; Electrically-conductive connections having two or more spaced connecting locations for conductors and using contact members penetrating insulation effected solely by twisting, wrapping, bending, crimping, or other permanent deformation by crimping
- H01R4/183—Electrically-conductive connections between two or more conductive members in direct contact, i.e. touching one another; Means for effecting or maintaining such contact; Electrically-conductive connections having two or more spaced connecting locations for conductors and using contact members penetrating insulation effected solely by twisting, wrapping, bending, crimping, or other permanent deformation by crimping for cylindrical elongated bodies, e.g. cables having circular cross-section
- H01R4/184—Electrically-conductive connections between two or more conductive members in direct contact, i.e. touching one another; Means for effecting or maintaining such contact; Electrically-conductive connections having two or more spaced connecting locations for conductors and using contact members penetrating insulation effected solely by twisting, wrapping, bending, crimping, or other permanent deformation by crimping for cylindrical elongated bodies, e.g. cables having circular cross-section comprising a U-shaped wire-receiving portion
- H01R4/185—Electrically-conductive connections between two or more conductive members in direct contact, i.e. touching one another; Means for effecting or maintaining such contact; Electrically-conductive connections having two or more spaced connecting locations for conductors and using contact members penetrating insulation effected solely by twisting, wrapping, bending, crimping, or other permanent deformation by crimping for cylindrical elongated bodies, e.g. cables having circular cross-section comprising a U-shaped wire-receiving portion combined with a U-shaped insulation-receiving portion
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- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Inorganic Chemistry (AREA)
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Description
(化3)
R21−CO−NH−R22 (3)
(化4)
R23−CO−NH−Y31−NH−CO−R24 (4)
(化5)
R25−NH−CO−Y32−CO−NH−R26 (5)
ただし、R21〜R26は、それぞれ個別に炭素数5〜25の飽和または不飽和の鎖状炭化水素基を示し、R22は水素であってもよい、Y31およびY32は、炭素数1〜10のアルキレン基、フェニレン基、または炭素数7〜10のアルキルフェニレン基からなる群より選ばれる炭素数1〜10の2価の炭化水素基を示す。
(化3)
R21−CO−NH−R22 (3)
(化4)
R23−CO−NH−Y31−NH−CO−R24 (4)
(化5)
R25−NH−CO−Y32−CO−NH−R26 (5)
(化8)
P(=O)(−OR14)(−OH)2 ・・・(6)
(化9)
P(=O)(−OR14)2(−OH) ・・・(7)
表1、2に示す配合組成(質量部)にて、潤滑油基油とアミド化合物を混合することにより、粘稠性物質を調製した。
・潤滑油基油A:鉱物系基油(動粘度=4.0mm2/s(100℃))
・潤滑油基油B:鉱物系基油(動粘度=11.1mm2/s(100℃))
・潤滑油基油C:合成油基油(動粘度=100.0mm2/s(100℃))
・アミド化合物:エチレンビスステアリルアミド(融点150℃、分子量592)、日本化成製「スリパックスE」
<調製例1> OL−Li
500mlのフラスコにオレイルアシッドホスフェイト(SC有機化学社製「Phoslex A18D」、分子量467(平均)、酸価183mgKOH/g)を50g(酸価0.163mol)とメタノール50mLを加え、50℃で撹拌し、均一溶液とした。そこに、水酸化リチウム一水塩6.84g(0.163mol)/メタノール50mL溶液を少しずつ加えた。加え終わった澄明溶液を50℃のまま30分間撹拌した後、ロータリーエバポレータにて、メタノールと生成水を減圧留去した。次いで、トルエン50mLを加えた後、同様に減圧留去する事で生成水を共沸によって留去し、澄明粘性物である目的物を得た。
オレイルアシッドホスフェイトに代えてイソステアリルアシッドホスフェイト(SC有機化学社製「Phoslex A18OL」、分子量487(平均)、酸価178 mgKOH/g)50g(酸価0.159mol)とし、そこに加える水酸化リチウム一水塩を6.67g(0.159mol)とした以外は調製例1と同様にして、澄明粘性物である目的物を得た。
オレイルアシッドホスフェイトに代えてイソステアリルアシッドホスフェイト(SC有機化学社製「Phoslex A18OL」、分子量487(平均)、酸価178 mgKOH/g)50g(酸価0.159mol)とし、そこに加える水酸化カルシウムの量を5.89g(0.0795mol)とした以外は調製例1と同様にして、澄明粘性物である目的物を得た。
500mlのフラスコにイソステアリルアシッドホスフェイト(SC有機化学社製「Phoslex A18OL」、分子量487(平均)、酸価178 mgKOH/g)100g(酸価0.317mol)と過塩基性アルキルサリチル酸カルシウム塩(Ca含有量8.0質量%、過塩基性Ca含有量5.5質量%)116g(過塩基性Ca質量6.4g=0.159mol)を入れ、120℃で3時間攪拌した後、室温まで冷却し、褐色粘性物である目的物を得た。
計算により、分子量を算出した。なお、IS−SA−Caについては、GPCにて分子量(重量平均分子量)を測定した。(溶剤:クロロホルム、カラム:TSKgel G2500HxL(東ソー))
調製例1〜4により得られた、各リン化合物と金属との組成物と、粘稠性物質と、をそれぞれ所定の割合(質量部)で160℃の加温下にて混合することにより、金属表面コーティング用組成物を調製した。この際、表2に示すように、任意の添加剤として、酸化防止剤を添加した。
・酸化防止剤:BASF社製「Irganox1010」
DSCを用いて測定した(昇温速度10℃/分、空気中)。
160℃に加温して液状とした金属表面コーティング用組成物に、長さ80mmの錫めっき銅板を40mmまで浸漬し、錫めっき銅板に薄膜コーティングした。次いで、そのコーティング面が上に配置されるように錫めっき銅板を立てかけたまま、120℃の恒温槽で120時間放置した。その後、恒温槽から錫めっき銅板を取り出し、常温まで放冷した後、金属表面コーティング用組成物の垂れ落ちた距離を測定した。垂れ落ち距離が1.0mm以下の場合を高温維持性が特に良好「○」とし、垂れ落ち距離が1.0mm超5.0mm以下の場合を高温維持性がやや劣る「△」とし、垂れ落ち距離が5.0mm超の場合を高温維持性が劣る「×」とした。
160℃に加温して液状とした金属表面コーティング用組成物に、60×80mmの錫めっき銅板を15秒間浸漬し、その後、10mm/秒の速度で引き上げ、錫めっき銅板に薄膜コーティングした。次いで、JIS K2246に準拠して35℃(塩溶液濃度50g/L)にて中性塩水噴霧試験を行い、120時間後のさび発生度を評価した。また、薄膜コーティングした後、長さ方向に立てかけて120℃の恒温槽で120時間放置した錫めっき銅板についても、同様に中性塩水噴霧試験を行った。
等級 さび発生度
A級 0%
B級 1〜10%
C級 11〜25%
D級 26〜50%
E級 50〜100%
2 被覆電線
3 電線導体
4 絶縁被覆(絶縁体)
5 端子金具
6 電気接続部
7 粘稠性膜
Claims (7)
- 潤滑油基油およびアミド化合物から構成される粘稠性物質と、下記の一般式(1)および(2)で表される化合物の1種または2種以上からなるリン化合物と金属との組成物と、を含有し、アミド基数aと酸性基数bの比(a/b)が1.1〜6.0の範囲内であり、前記リン化合物と組成物を形成する金属が、アルカリ金属、アルカリ土類金属、アルミニウム、亜鉛から選択される少なくとも1種であり、前記アミド化合物の融点が120℃以上である金属表面コーティング用組成物により端子金具と電線導体との電気接続部が覆われていることを特徴とする端子付き被覆電線。
- 前記リン化合物と金属との組成物は、金属水酸化物および金属カルボン酸塩のうちの少なくとも1種と前記リン化合物から形成されたものであることを特徴とする請求項1に記載の端子付き被覆電線。
- 前記金属カルボン酸塩が、金属サリチル酸塩であることを特徴とする請求項2に記載の端子付き被覆電線。
- 前記アミド化合物は、下記の一般式(3)〜(5)で表される化合物の1種または2種以上であることを特徴とする請求項1から3のいずれか1項に記載の端子付き被覆電線。
(化3)
R21−CO−NH−R22 (3)
(化4)
R23−CO−NH−Y31−NH−CO−R24 (4)
(化5)
R25−NH−CO−Y32−CO−NH−R26 (5)
ただし、R21〜R26は、それぞれ個別に炭素数5〜25の飽和または不飽和の鎖状炭化水素基を示し、R22は水素であってもよい、Y31およびY32は、炭素数1〜10のアルキレン基、フェニレン基、または炭素数7〜10のアルキルフェニレン基からなる群より選ばれる炭素数1〜10の2価の炭化水素基を示す。 - 前記アミド化合物は、融点が120〜200℃の範囲内にある脂肪酸アミドであることを特徴とする請求項1から4のいずれか1項に記載の端子付き被覆電線。
- 前記リン化合物が、その炭素数8〜30の炭化水素基の構造中に、1以上の分岐鎖構造または1以上の炭素−炭素二重結合構造を有することを特徴とする請求項1から5のいずれか1項に記載の端子付き被覆電線。
- 前記リン化合物と金属との組成物の分子量が、3000以下であることを特徴とする請求項1から6のいずれか1項に記載の端子付き被覆電線。
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JP5864509B2 (ja) | 2013-10-17 | 2016-02-17 | 株式会社オートネットワーク技術研究所 | 油膜保持機能を有する組成物およびこれを用いた防食剤ならびに端子付き絶縁電線 |
WO2015146985A1 (ja) | 2014-03-24 | 2015-10-01 | Jx日鉱日石エネルギー株式会社 | 表面保護剤組成物及びこれを用いた電気接続構造並びに電気接続構造の製造方法 |
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US20180179400A1 (en) | 2018-06-28 |
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