JP6667568B2 - 酸化繊維の製造方法及び酸化繊維 - Google Patents
酸化繊維の製造方法及び酸化繊維 Download PDFInfo
- Publication number
- JP6667568B2 JP6667568B2 JP2018072900A JP2018072900A JP6667568B2 JP 6667568 B2 JP6667568 B2 JP 6667568B2 JP 2018072900 A JP2018072900 A JP 2018072900A JP 2018072900 A JP2018072900 A JP 2018072900A JP 6667568 B2 JP6667568 B2 JP 6667568B2
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- oxidized
- fiber
- fiber bundle
- microwave
- heating furnace
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- 239000000835 fiber Substances 0.000 title claims description 378
- 238000004519 manufacturing process Methods 0.000 title claims description 103
- 238000010438 heat treatment Methods 0.000 claims description 92
- 238000000034 method Methods 0.000 claims description 37
- 230000005540 biological transmission Effects 0.000 claims description 29
- 238000011282 treatment Methods 0.000 claims description 25
- 238000004804 winding Methods 0.000 claims description 23
- 229920002239 polyacrylonitrile Polymers 0.000 claims description 19
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 14
- 229910052760 oxygen Inorganic materials 0.000 claims description 14
- 239000001301 oxygen Substances 0.000 claims description 14
- 239000007789 gas Substances 0.000 claims description 8
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 5
- 230000001590 oxidative effect Effects 0.000 claims description 4
- 239000010426 asphalt Substances 0.000 claims description 3
- 229910044991 metal oxide Inorganic materials 0.000 claims description 3
- 150000004706 metal oxides Chemical class 0.000 claims description 3
- 238000007254 oxidation reaction Methods 0.000 description 41
- 230000003647 oxidation Effects 0.000 description 37
- 229920000049 Carbon (fiber) Polymers 0.000 description 28
- 239000004917 carbon fiber Substances 0.000 description 28
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 25
- 230000000052 comparative effect Effects 0.000 description 11
- 230000000704 physical effect Effects 0.000 description 8
- 238000003763 carbonization Methods 0.000 description 6
- 238000010000 carbonizing Methods 0.000 description 6
- 238000005485 electric heating Methods 0.000 description 5
- 238000007363 ring formation reaction Methods 0.000 description 5
- 238000010923 batch production Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000007380 fibre production Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000020169 heat generation Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
Images
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/003—Treatment with radio-waves or microwaves
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F11/00—Chemical after-treatment of artificial filaments or the like during manufacture
- D01F11/10—Chemical after-treatment of artificial filaments or the like during manufacture of carbon
- D01F11/16—Chemical after-treatment of artificial filaments or the like during manufacture of carbon by physicochemical methods
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D10/00—Physical treatment of artificial filaments or the like during manufacture, i.e. during a continuous production process before the filaments have been collected
- D01D10/04—Supporting filaments or the like during their treatment
- D01D10/0436—Supporting filaments or the like during their treatment while in continuous movement
- D01D10/0454—Supporting filaments or the like during their treatment while in continuous movement using reels
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/145—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from pitch or distillation residues
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/18—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from proteins, e.g. from wool
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/20—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
- D01F9/21—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F9/22—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/20—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
- D01F9/21—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F9/22—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
- D01F9/225—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles from stabilised polyacrylonitriles
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/32—Apparatus therefor
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2101/00—Inorganic fibres
- D10B2101/10—Inorganic fibres based on non-oxides other than metals
- D10B2101/12—Carbon; Pitch
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2211/00—Protein-based fibres, e.g. animal fibres
- D10B2211/01—Natural animal fibres, e.g. keratin fibres
- D10B2211/04—Silk
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2321/00—Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D10B2321/10—Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds polymers of unsaturated nitriles, e.g. polyacrylonitrile, polyvinylidene cyanide
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/06—Load-responsive characteristics
- D10B2401/063—Load-responsive characteristics high strength
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Inorganic Fibers (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
- Treatment Of Fiber Materials (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
TW107103128A TWI695099B (zh) | 2018-01-29 | 2018-01-29 | 氧化纖維 |
TW107103128 | 2018-01-29 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2019131940A JP2019131940A (ja) | 2019-08-08 |
JP6667568B2 true JP6667568B2 (ja) | 2020-03-18 |
Family
ID=62116203
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2018072900A Active JP6667568B2 (ja) | 2018-01-29 | 2018-04-05 | 酸化繊維の製造方法及び酸化繊維 |
Country Status (6)
Country | Link |
---|---|
US (1) | US20190233977A1 (zh) |
EP (1) | EP3517660A1 (zh) |
JP (1) | JP6667568B2 (zh) |
KR (1) | KR20200068527A (zh) |
CN (1) | CN110093685A (zh) |
TW (1) | TWI695099B (zh) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110983493A (zh) * | 2019-12-28 | 2020-04-10 | 西安康本材料有限公司 | 一种提高pan基碳纤维碳化效率的工艺 |
CN112142487B (zh) * | 2020-09-22 | 2021-09-10 | 中国科学院山西煤炭化学研究所 | 一种微波辅助的沥青氧化不融化方法 |
KR102458266B1 (ko) * | 2021-12-10 | 2022-10-24 | 케이에이에프 주식회사 | 생분해성 폴리올레핀 섬유 및 이의 제조방법 |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2392143A1 (fr) * | 1977-05-25 | 1978-12-22 | British Petroleum Co | Procede de fabrication de fibres de carbone ou de graphite a partir de fibres de matieres organiques naturelles par utilisation d'hyperfrequences |
US6733737B1 (en) * | 2001-08-29 | 2004-05-11 | Wright Materials Research Corp. | Rapid oxidation/stabilization technique for carbon foams, carbon fibers and C/C composites |
CN1202297C (zh) * | 2002-03-05 | 2005-05-18 | 陈新谋 | 聚丙烯腈纤维预氧化及碳化新工艺及装置 |
US7534854B1 (en) * | 2005-03-29 | 2009-05-19 | Ut-Battelle, Llc | Apparatus and method for oxidation and stabilization of polymeric materials |
US7824495B1 (en) * | 2005-11-09 | 2010-11-02 | Ut-Battelle, Llc | System to continuously produce carbon fiber via microwave assisted plasma processing |
RU2416682C1 (ru) * | 2009-07-28 | 2011-04-20 | Марина Владимировна Соболева | Способ стабилизации углеродсодержащего волокна и способ получения углеродного волокна |
AU2010294347B2 (en) * | 2009-09-11 | 2014-06-26 | Toho Tenax Europe Gmbh | Stabilizing polyacrylonitrile precursor yarns |
TWI384098B (zh) * | 2009-12-30 | 2013-02-01 | 高模數碳纖維及其製造方法 | |
JP2011162898A (ja) * | 2010-02-06 | 2011-08-25 | Toho Tenax Co Ltd | 炭素繊維前駆体繊維及びそれを用いた炭素繊維の製造方法 |
CN102505188B (zh) * | 2011-11-10 | 2013-07-10 | 中国科学院宁波材料技术与工程研究所 | 一种以聚偏氯乙烯为基体制备活性碳纤维的方法 |
CN104047073B (zh) * | 2014-06-26 | 2016-02-10 | 吉林大学 | 一种聚丙烯腈预氧化处理装置及方法 |
CN105696113B (zh) * | 2015-12-04 | 2018-06-26 | 江西大有科技有限公司 | 一种利用非平衡等离子体制造碳纤维的装置及其方法 |
CN105544021A (zh) * | 2016-02-18 | 2016-05-04 | 上海应用技术学院 | 一种抑制碳纤维结构不均匀性的方法 |
JP6446573B1 (ja) * | 2018-01-18 | 2018-12-26 | マイクロ波化学株式会社 | マイクロ波処理装置、および炭素繊維の製造方法 |
TWM564598U (zh) * | 2018-01-29 | 2018-08-01 | 永虹先進材料股份有限公司 | Oxidized fiber structure |
-
2018
- 2018-01-29 TW TW107103128A patent/TWI695099B/zh active
- 2018-02-02 CN CN201810114753.3A patent/CN110093685A/zh not_active Withdrawn
- 2018-04-05 JP JP2018072900A patent/JP6667568B2/ja active Active
- 2018-04-12 US US15/951,341 patent/US20190233977A1/en not_active Abandoned
- 2018-04-18 EP EP18168095.0A patent/EP3517660A1/en not_active Withdrawn
- 2018-12-07 KR KR1020180156625A patent/KR20200068527A/ko active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
KR20200068527A (ko) | 2020-06-15 |
TWI695099B (zh) | 2020-06-01 |
JP2019131940A (ja) | 2019-08-08 |
CN110093685A (zh) | 2019-08-06 |
US20190233977A1 (en) | 2019-08-01 |
EP3517660A1 (en) | 2019-07-31 |
TW201932652A (zh) | 2019-08-16 |
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