JP6661555B2 - ニトロベンゼンの製造方法 - Google Patents

ニトロベンゼンの製造方法 Download PDF

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Publication number
JP6661555B2
JP6661555B2 JP2016575028A JP2016575028A JP6661555B2 JP 6661555 B2 JP6661555 B2 JP 6661555B2 JP 2016575028 A JP2016575028 A JP 2016575028A JP 2016575028 A JP2016575028 A JP 2016575028A JP 6661555 B2 JP6661555 B2 JP 6661555B2
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plant
nitrobenzene
washing
phase
sulfuric acid
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Japanese (ja)
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JP2017525666A (ja
JP2017525666A5 (enExample
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トーマス、クナーフ
ペーター、ドリンダ
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Covestro Deutschland AG
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Covestro Deutschland AG
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2455—Stationary reactors without moving elements inside provoking a loop type movement of the reactants
    • B01J19/2465—Stationary reactors without moving elements inside provoking a loop type movement of the reactants externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/16—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/06—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/00033—Continuous processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/0004—Processes in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00245—Avoiding undesirable reactions or side-effects
    • B01J2219/00268—Detecting faulty operations

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Heat Treatment Of Water, Waste Water Or Sewage (AREA)
  • Physical Water Treatments (AREA)
JP2016575028A 2014-06-24 2015-06-22 ニトロベンゼンの製造方法 Active JP6661555B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP14173583 2014-06-24
EP14173583.7 2014-06-24
PCT/EP2015/063924 WO2015197521A1 (de) 2014-06-24 2015-06-22 Verfahren zur herstellung von nitrobenzol

Publications (3)

Publication Number Publication Date
JP2017525666A JP2017525666A (ja) 2017-09-07
JP2017525666A5 JP2017525666A5 (enExample) 2018-08-16
JP6661555B2 true JP6661555B2 (ja) 2020-03-11

Family

ID=50979654

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2016575028A Active JP6661555B2 (ja) 2014-06-24 2015-06-22 ニトロベンゼンの製造方法

Country Status (8)

Country Link
US (2) US10023524B2 (enExample)
EP (1) EP3160932B1 (enExample)
JP (1) JP6661555B2 (enExample)
KR (1) KR102414963B1 (enExample)
CN (1) CN106660934B (enExample)
PT (1) PT3160932T (enExample)
SA (1) SA516380565B1 (enExample)
WO (1) WO2015197521A1 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102414963B1 (ko) * 2014-06-24 2022-07-01 코베스트로 도이칠란트 아게 니트로벤젠의 제조 방법
US10577311B2 (en) * 2015-09-24 2020-03-03 Covestro Deutschland Ag Method for producing isocyanates
CN110573491B (zh) * 2017-03-07 2022-11-11 科思创德国股份有限公司 制备硝基苯的方法
CN107512810B (zh) * 2017-07-13 2021-04-16 安徽东至广信农化有限公司 一种硝基氯苯生产后废水处理方法
WO2020212334A1 (de) 2019-04-17 2020-10-22 Covestro Deutschland Ag Verfahren und vorrichtung zur herstellung von nitrobenzol
CN110511146A (zh) * 2019-09-17 2019-11-29 四川北方红光特种化工有限公司 一种废酸量低的单硝基邻二甲苯的生产方法及其生产系统
CN115397779B (zh) * 2020-04-27 2024-12-06 科思创德国股份有限公司 净化被硝基苯污染的水性废水料流的方法
CN115193366B (zh) * 2021-04-09 2024-04-09 万华化学集团股份有限公司 一种硝化反应装置及利用该反应装置进行硝化反应的方法
WO2025045698A1 (en) 2023-08-25 2025-03-06 Covestro Deutschland Ag Reactor for the nitration of aromatic compounds, production plant comprising said reactor and nitration process using said reactor
CN119819213A (zh) * 2023-10-13 2025-04-15 中国石油化工股份有限公司 一种硝基苯废水减量化装置及方法

Family Cites Families (34)

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US2256999A (en) 1939-03-08 1941-09-23 Du Pont Nitration of organic compounds
US2739174A (en) 1951-09-08 1956-03-20 Eastman Kodak Co Nitrating aromatic hydrocarbons with only nitric acid
DE1593045A1 (de) * 1966-07-02 1970-04-09 Meissner Fa Josef Verfahren und Vorrichtung zum zeitweiligen Abschalten der Produktion von Trinitrotoluol
US3692477A (en) 1969-08-04 1972-09-19 Victor R Thayer Process for enrichment by countercurrent mass transfer
US3780116A (en) 1972-06-15 1973-12-18 Zaverchand & Co Method for nitration of aromatic hydrocarbon compounds
FR2453492A1 (fr) 1979-04-03 1980-10-31 Cgr Mev Dispositif de deviation magnetique achromatique d'un faisceau de particules chargees et appareil d'irradiation utilisant un tel dispositif
EP0078247B1 (en) 1981-10-21 1985-11-27 Monsanto Company Process and catalysts for vapor phase nitration of aromatic compounds
DE3409717C2 (de) 1984-03-16 1994-03-31 Bayer Ag Verfahren zur Herstellung von Nitrobenzol
FR2656679A1 (fr) 1990-01-02 1991-07-05 Armines Dispositif concentrateur de rayonnements.
EP0436443B1 (en) 1990-01-04 1996-04-17 Nrm International Technologies C.V. Nitration process
US5158537A (en) 1990-10-29 1992-10-27 Alza Corporation Iontophoretic delivery device and method of hydrating same
CH683919A5 (de) 1992-01-15 1994-06-15 Uetikon Chemie Ag Verfahren zur Herstellung von Nitrobenzol.
US5756857A (en) 1992-10-29 1998-05-26 Hisamitsu Pharmaceutical Co., Inc. Cyclohexanol derivative, cool feeling and cool feeling composition containing the same, process for producing the derivative and intermediate therefor
DE19512114C2 (de) 1995-04-04 2000-04-27 Meissner Gmbh & Co Kg Josef Rückgewinnung von Salpetersäure aus Nitrierprozessen
DE19539205A1 (de) 1995-10-22 1997-04-24 Meissner Gmbh & Co Kg Josef Verfahren zur Aromatennitrierung
US6288289B1 (en) 2000-01-27 2001-09-11 Noram Engineering And Constructors Ltd. Integrated effluent treatment process for nitroaromatic manufacture
US6506949B2 (en) 2000-03-02 2003-01-14 Dow Global Technologies, Inc. Process for ring nitrating aromatic compounds in a tubular reactor having static mixing elements separated by coalescing zones
WO2001091897A1 (en) 2000-05-31 2001-12-06 Huntsman International Llc Process and unit for the continuous preparation of isocyanate-containing polyurethane prepolymers
DE10249270B4 (de) 2002-10-23 2008-02-21 Bayer Materialscience Ag Rücklöseverfahren
DE102004017628A1 (de) 2004-04-10 2005-11-03 Bayer Materialscience Ag Verfahren zur Aufarbeitung von aromatische Nitroverbindungen enthaltenden Abwässern
DE102005050106B4 (de) 2005-10-18 2008-04-30 Josef Meissner Gmbh & Co. Kg Rückgewinnung von Nitriersäuregemischen aus Nitrienprozessen
DE102006004943A1 (de) * 2006-02-03 2007-08-09 Bayer Materialscience Ag Verfahren zur Herstellung von Nitrobenzol
EP2014641A3 (en) 2007-06-06 2009-03-18 Huntsman International Llc Process for preparing mixtures of diphenylmethane diisocyanates and polyphenyl polymethylene polyisocyanates
DE102007059513A1 (de) 2007-12-11 2009-06-18 Bayer Materialscience Ag Verfahren zur Herstellung von Nitrobenzol durch adiabate Nitrierung
HUE029695T2 (en) 2008-11-14 2017-03-28 Noram Int Ltd Process for reducing the formation of dinitrobenzene by-product in the production of mononitrobenzene
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DE102010006984A1 (de) 2010-02-05 2011-08-11 Bayer MaterialScience AG, 51373 Verfahren zur kontinuierlichen Herstellung von Nitrobenzol
DE102010038319A1 (de) 2010-07-23 2012-01-26 Krones Aktiengesellschaft Verfahren und Vorrichtung zur Medienführung durch eine Behandlungsanlage für ein flüssiges Produkt
EP2418176A1 (de) * 2010-08-12 2012-02-15 Basf Se Verfahren zur Aufreinigung von Abwässern aus der Aufarbeitung vom rohem Mononitrobenzol
US20120205308A1 (en) * 2010-08-12 2012-08-16 Basf Se Process for purifying wastewaters from the workup of crude aromatic nitro compounds
CN104066709B (zh) 2012-01-31 2016-08-24 科思创德国股份有限公司 用于生产硝基苯的方法和设备
KR102067307B1 (ko) * 2012-07-27 2020-01-16 코베스트로 도이칠란드 아게 단열 니트로화에 의한 니트로벤젠의 제조방법
US9260377B2 (en) * 2012-07-27 2016-02-16 Bayer Materialscience Ag Method for producing nitrobenzene by adiabatic nitriding
KR102414963B1 (ko) * 2014-06-24 2022-07-01 코베스트로 도이칠란트 아게 니트로벤젠의 제조 방법

Also Published As

Publication number Publication date
JP2017525666A (ja) 2017-09-07
WO2015197521A1 (de) 2015-12-30
KR20170021851A (ko) 2017-02-28
US10023524B2 (en) 2018-07-17
CN106660934B (zh) 2020-03-03
EP3160932B1 (de) 2018-03-14
KR102414963B1 (ko) 2022-07-01
SA516380565B1 (ar) 2020-11-03
PT3160932T (pt) 2018-06-15
US20170174612A1 (en) 2017-06-22
CN106660934A (zh) 2017-05-10
US11136285B2 (en) 2021-10-05
US20180346405A1 (en) 2018-12-06
EP3160932A1 (de) 2017-05-03

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