JP6544473B1 - 樹脂組成物、光学性層、カバー部材および移動体 - Google Patents
樹脂組成物、光学性層、カバー部材および移動体 Download PDFInfo
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- JP6544473B1 JP6544473B1 JP2018182900A JP2018182900A JP6544473B1 JP 6544473 B1 JP6544473 B1 JP 6544473B1 JP 2018182900 A JP2018182900 A JP 2018182900A JP 2018182900 A JP2018182900 A JP 2018182900A JP 6544473 B1 JP6544473 B1 JP 6544473B1
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- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
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Abstract
Description
(1) 透光性を有する主材料としての樹脂材料と、該樹脂材料中に分散され、可視光を吸収する可視光吸収剤とを含む第1層と、該第1層を保護する第2層とを備える光学性層における、前記第2層を形成するために用いられる樹脂組成物であって、
シリコン変性(メタ)アクリル樹脂と、ウレタン(メタ)アクリレートと、多官能(メタ)アクリレートとを含み、前記多官能(メタ)アクリレートは、4官能(メタ)アクリレートを含有し、当該樹脂組成物中における4官能(メタ)アクリレートの含有量は、40wt%以上70wt%以下であり、下記要件Aを満足することを特徴とする樹脂組成物。
要件B:ビスフェノール型ポリカーボネート系樹脂で構成される平均厚さ2mmの基材上に、平均厚さ12μmの前記第2層を設けて、前記基材と前記第2層とで構成される積層体を形成し、前記混合溶剤の塗膜を前記第2層上に形成した状態で、85℃×24時間の条件下で静置した後、25℃の雰囲気に戻し、前記混合溶剤の除去後における、前記積層体の波長900nmにおける透過率(%)を測定したとき、前記透過率は60%以上であること。
(13) 上記(12)に記載のカバー部材を備えることを特徴とする移動体。
<<第1実施形態>>
まず、本発明の光学性層の第1実施形態について説明する。
この保護層2は、本発明の樹脂組成物を用いて形成された第2層により構成される。
その他の材料としては、例えば、前記シリコン変性(メタ)アクリル樹脂以外の樹脂材料、着色剤、増感剤、安定剤、界面活性剤、酸化防止剤、還元防止剤、帯電防止剤、表面調整剤および溶剤等が挙げられる。
次に、本発明の光学性層の第2実施形態について説明する。
図2は、本発明の光学性層の第2実施形態を示す縦断面図である。
[実施例1]
[1]まず、99.62wt%のビスフェノールA型ポリカーボネート(三菱エンジニアプラスチックス社製、「E2000」)と、0.03wt%の第1光吸収剤(キノリン;有本化学工業社製、「plastyellow8050」)と、0.05wt%の第2光吸収剤(アントラキノンA;有本化学工業社製、「Plast blue 8590」)と、0.05wt%の第2光吸収剤(アントラキノンB;有本化学工業社製、「SDO−7」)と、0.07wt%の第3光吸収剤(ペリノン;有本化学工業社製、「Plast red 8370」)と、0.18wt%の第4光吸収剤(UVA;ADEKA社製、「LA−31G」)とを撹拌・混合することにより、基材層形成用樹脂組成物を用意した。
保護層形成用樹脂組成物中に含まれる構成材料の含有量を表1に示すように変更して、保護層形成用樹脂組成物を調製したこと以外は、前記実施例1と同様にして、実施例2〜6、比較例1、2の光学性層を得た。
各実施例および各比較例の光学性層を、以下の方法で評価した。
石油系溶剤を45wt%以上65wt%以下含む混合溶剤1に対する耐薬品性の評価を以下に示す通り実施した。
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、混合溶剤1の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、混合溶剤1の除去後における、外観変化を観察し、以下の評価基準にしたがって評価した。
◎:保護層の外観に変化が全く認められない
〇:保護層の外観に若干の変化が認められる
△:保護層の外観に変化が認められるが、
光学性層としての使用には耐え得る範囲である
×:保護層の外観に変化が明らかに認められ、
光学性層として使用できるものではない
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、混合溶剤1の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、混合溶剤1を除去した。そして、保護層に対して、幅18mmの粘着テープ(ニチバン社製、「セロテープ(登録商標)」)を貼付し、その後、25℃において90°の方向に10mm/分の速度で引き剥がした後の保護層の剥離の有無を観察し、以下の評価基準にしたがって評価した。
◎:保護層の剥離が全く認められない
〇:保護層の剥離が若干認められる
△:保護層の剥離が認められ、
剥離した保護層の光学性層側への転写が若干認められる
×:保護層の剥離が明らかに認められ、
剥離した保護層の光学性層側への転写も明らかに認められる
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、混合溶剤1の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、混合溶剤1を除去した。そして、25℃の雰囲気に戻し、JIS K 5600−5−6で規定されたクロスカット法により、格子状に切断された100個の保護層の基材層に対する付着の有無を観察した。
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、混合溶剤1の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、混合溶剤1を除去した。そして、25℃の雰囲気に戻し、光学性層の波長900nmにおける透過率(%)を測定した。
石油系溶剤を50wt%以上70wt%以下含む混合溶剤2に対する耐薬品性の評価を以下に示す通り実施した。
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、混合溶剤2の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、混合溶剤2の除去後における、外観変化を観察し、以下の評価基準にしたがって評価した。
◎:保護層の外観に変化が全く認められない
〇:保護層の外観に若干の変化が認められる
△:保護層の外観に変化が認められるが、
光学性層としての使用には耐え得る範囲である
×:保護層の外観に変化が明らかに認められ、
光学性層として使用できるものではない
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、混合溶剤2の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、混合溶剤2を除去した。そして、保護層に対して、幅18mmの粘着テープ(ニチバン社製、「セロテープ(登録商標)」)を貼付し、その後、25℃において90°の方向に10mm/分の速度で引き剥がした後の保護層の剥離の有無を観察し、以下の評価基準にしたがって評価した。
◎:保護層の剥離が全く認められない
〇:保護層の剥離が若干認められる
△:保護層の剥離が認められ、
剥離した保護層の光学性層側への転写が若干認められる
×:保護層の剥離が明らかに認められ、
剥離した保護層の光学性層側への転写も明らかに認められる
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、混合溶剤2の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、混合溶剤2を除去した。そして、25℃の雰囲気に戻し、JIS K 5600−5−6で規定されたクロスカット法により、格子状に切断された100個の保護層の基材層に対する付着の有無を観察した。
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、混合溶剤2の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、混合溶剤2を除去した。そして、25℃の雰囲気に戻し、光学性層の波長900nmにおける透過率(%)を測定した。
ニトリル酢酸とその塩とで合計15wt%以上30wt%以下含む酸溶液1に対する耐薬品性の評価を以下に示す通り実施した。
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、酸溶液1の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、酸溶液1の除去後における、外観変化を観察し、以下の評価基準にしたがって評価した。
◎:保護層の外観に変化が全く認められない
〇:保護層の外観に若干の変化が認められる
△:保護層の外観に変化が認められるが、
光学性層としての使用には耐え得る範囲である
×:保護層の外観に変化が明らかに認められ、
光学性層として使用できるものではない
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、酸溶液1の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、酸溶液1を除去した。そして、保護層に対して、幅18mmの粘着テープ(ニチバン社製、「セロテープ(登録商標)」)を貼付し、その後、25℃において90°の方向に10mm/分の速度で引き剥がした後の保護層の剥離の有無を観察し、以下の評価基準にしたがって評価した。
◎:保護層の剥離が全く認められない
〇:保護層の剥離が若干認められる
△:保護層の剥離が認められ、
剥離した保護層の光学性層側への転写が若干認められる
×:保護層の剥離が明らかに認められ、
剥離した保護層の光学性層側への転写も明らかに認められる
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、酸溶液1の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、酸溶液1を除去した。そして、25℃の雰囲気に戻し、JIS K 5600−5−6で規定されたクロスカット法により、格子状に切断された100個の保護層の基材層に対する付着の有無を観察した。
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)上に、酸溶液1の塗膜を形成した状態で、85℃×24時間の条件下で静置した後、酸溶液1を除去した。そして、25℃の雰囲気に戻し、光学性層の波長900nmにおける透過率(%)を測定した。
光学性層の成形性の評価を以下に示す通り実施した。
各実施例および各比較例の光学性層について、それぞれ、幅60mm、長さ120mm、厚さ2mmの大きさの試料を用意し、この試料を、170℃に設定した熱風循環型オーブンで3分間加熱し軟化させオーブンから取り出した直後に、保護層側を外側にして各半径の木製円柱にネル布を介して添わせ、試料が室温付近に冷却されるまでそのままに保つことで単曲面成形を行った。そして、外観変化が起きていない半径を最小曲率半径Rとして、以下の評価基準にしたがって、熱曲げ性を評価した。
◎:最小曲率半径Rが50mmR以下である
〇:最小曲率半径Rが50mmR超100mmR以下である
△:最小曲率半径Rが100mmR超300mmR以下である
×:最小曲率半径Rが300mmR超である
光学性層の耐候性の評価を以下に示す通り実施した。
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)を上側にして、アイスーパーUVテスター(岩崎電気(株)製 紫外線照度150mW/cm2、温度63℃/湿度50%RH、シャワー頻度120分中18分)の条件下に120時間晒した。そして、保護層に対して、幅18mmの粘着テープ(ニチバン社製、「セロテープ(登録商標)」)を貼付し、その後、25℃において90°の方向に10mm/分の速度で引き剥がした後の保護層の剥離の有無を観察し、以下の評価基準にしたがって評価した。
◎:保護層の剥離が全く認められない
〇:保護層の剥離が若干認められる
△:保護層の剥離が認められ、
剥離した保護層の光学性層側への転写が若干認められる
×:保護層の剥離が明らかに認められ、
剥離した保護層の光学性層側への転写も明らかに認められる
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)を上側にして、アイスーパーUVテスター(岩崎電気(株)製 紫外線照度150mW/cm2、温度63℃/湿度50%RH、シャワー頻度120分中18分)の条件下に120時間晒した。そして、25℃の雰囲気に戻し、JIS K 5600−5−6で規定されたクロスカット法により、格子状に切断された100個の保護層の基材層に対する付着の有無を観察した。
各実施例および各比較例の光学性層について、それぞれ、保護層(第2層)を上側にして、アイスーパーUVテスター(岩崎電気(株)製 紫外線照度150mW/cm2、温度63℃/湿度50%RH、シャワー頻度120分中18分)の条件下に120時間晒した。そして、25℃の雰囲気に戻し、光学性層の波長900nmにおける透過率(%)を測定した。
2 保護層
3 可視光吸収層
4 紫外線吸収層
10、10A 光学性層
Claims (13)
- 透光性を有する主材料としての樹脂材料と、該樹脂材料中に分散され、可視光を吸収する可視光吸収剤とを含む第1層と、該第1層を保護する第2層とを備える光学性層における、前記第2層を形成するために用いられる樹脂組成物であって、
シリコン変性(メタ)アクリル樹脂と、ウレタン(メタ)アクリレートと、多官能(メタ)アクリレートとを含み、前記多官能(メタ)アクリレートは、4官能(メタ)アクリレートを含有し、当該樹脂組成物中における4官能(メタ)アクリレートの含有量は、40wt%以上70wt%以下であり、下記要件Aを満足することを特徴とする樹脂組成物。
要件A:主材料としてビスフェノール型ポリカーボネート系樹脂を含有する基材上に、平均厚さ12μmの前記第2層を形成したとき、石油系溶剤を45wt%以上含む混合溶剤の塗膜を前記第2層上に形成した状態で、85℃×24時間の条件下で静置した後、25℃の雰囲気に戻し、前記混合溶剤の除去後における、JIS K 5600−5−6で規定されたクロスカット法による、格子状に切断された前記第2層の前記基材に対する付着性が95%以上となる。 - さらに、下記要件Bを満足する請求項1に記載の樹脂組成物。
要件B:ビスフェノール型ポリカーボネート系樹脂で構成される平均厚さ2mmの基材上に、平均厚さ12μmの前記第2層を設けて、前記基材と前記第2層とで構成される積層体を形成し、前記混合溶剤の塗膜を前記第2層上に形成した状態で、85℃×24時間の条件下で静置した後、25℃の雰囲気に戻し、前記混合溶剤の除去後における、前記積層体の波長900nmにおける透過率(%)を測定したとき、前記透過率は60%以上であること。 - 当該樹脂組成物は、さらに、イソシアネートを含有する請求項1または2に記載の樹脂組成物。
- 前記多官能(メタ)アクリレートは、さらに、芳香族2官能(メタ)アクリレートを含む請求項1ないし3のいずれか1項に記載の樹脂組成物。
- 前記ウレタン(メタ)アクリレートは、カーボネート構造を有する脂環式ウレタン(メタ)アクリレートである請求項1ないし4のいずれか1項に記載の樹脂組成物。
- 当該樹脂組成物は、さらに、紫外線を吸収する紫外線吸収剤を含有する請求項1ないし4のいずれか1項に記載の樹脂組成物。
- 前記光学性層は、光透過性を有するカバー部材として使用される請求項1ないし6のいずれか1項に記載の樹脂組成物。
- 前記第1層と、請求項1ないし7のいずれか1項に記載の樹脂組成物を用いて形成された前記第2層とを備えることを特徴とする光学性層。
- 前記第1層に含まれる前記樹脂材料は、ビスフェノール型ポリカーボネート系樹脂である請求項8に記載の光学性層。
- 前記第1層に含まれる前記可視光吸収剤は、波長が300nm以上550nm以下の光を吸収する第1光吸収剤と、波長が450nm以上800nm以下の光を吸収する第2光吸収剤と、波長が400nm以上800nm以下の光を吸収する第3光吸収剤とのうちの少なくとも1つを含む請求項8または9に記載の光学性層。
- 前記第1層は、さらに、紫外線を吸収する紫外線吸収剤を含有する請求項8ないし10のいずれか1項に記載の光学性層。
- 移動体が備える、光透過性を有するカバー部材として、請求項8ないし11のいずれか1項に記載の光学性層を備えることを特徴とするカバー部材。
- 請求項12に記載のカバー部材を備えることを特徴とする移動体。
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CN201980008688.9A CN111630121B (zh) | 2018-09-27 | 2019-09-24 | 树脂组合物、光学层、罩构件及移动体 |
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