JP6526714B2 - ナノメートルサイズの金属粒子をポリマー表面に塗布するための紫外線硬化性転写コーティング - Google Patents
ナノメートルサイズの金属粒子をポリマー表面に塗布するための紫外線硬化性転写コーティング Download PDFInfo
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Description
ND−9740−1という名称のUV硬化性転写コーティング(大韓民国、京畿道、始興市のNanoPhotonic Chemicalから市販される)の接着性を、ポリカーボネート基材に対する接着性について試験した。ASTM D3359に従って決定された接着性は結果的に0Bであった。接着性の結果が0Bであったことから、この試料を沸騰水試験にかけなかった。
Claims (7)
- 多官能アクリレート、
アクリレートモノマー、および
光開始剤
を含む紫外線硬化性転写コーティングであって、前記紫外線硬化性転写コーティングの総重量の30%〜80%が前記多官能アクリレートで構成され、前記総重量の15%〜65%が前記アクリレートモノマーで構成され、前記総重量の3%〜7%が前記光開始剤で構成され、
前記多官能アクリレートが、脂肪族ウレタンアクリレートオリゴマー、ペンタエリスリトールテトラアクリレート、脂肪族ウレタンアクリレート、アクリル酸エステル、ジペンタエリスリトールヘキサアクリレート、アクリレート化樹脂、トリメチロールプロパントリアクリレート(TMPTA)、ジペンタエリスリトールペンタアクリレートエステル、またはこれらの少なくとも1種を含む組み合わせを含み、前記多官能アクリレートが、3〜15の官能価を有し、
前記アクリレートモノマーが、C6〜C12炭化水素ジオールジアクリレート、またはジメタクリレート、または、メタ(アクリレート)を含み、
ASTM D3359に従って測定された3B以上の接着強度でポリカーボネート基材に接着することができることを特徴とする、紫外線硬化性転写コーティング。 - 請求項1に記載の紫外線硬化性転写コーティングであって、前記多官能アクリレートが、脂肪族ウレタンアクリレートオリゴマーおよびペンタエリスリトールテトラアクリレートを含み、前記多官能アクリレートの重量の30%〜50%が前記脂肪族ウレタンアクリレートオリゴマーで構成され、前記多官能アクリレートの重量の50%〜70%が前記ペンタエリスリトールテトラアクリレートで構成されることを特徴とする、紫外線硬化性転写コーティング。
- 第1の表面と第2の表面とを含む基材、
前記第1の表面に接着された、請求項1〜2のいずれか1項に記載の紫外線硬化性転写コーティング、および
前記紫外線硬化性転写コーティングと隣り合った導電性コーティングを含み、前記導電性コーティングがネットワーク中に配置されるナノメートルサイズの金属粒子を含み、前記導電性コーティングが0.1オーム/スクエア以下の表面抵抗を有し、
シートまたはフィルムは、1キログラムの荷重を有する三菱ユニ鉛筆を使用してASTM D3363に従って測定された鉛筆硬度がH以上であり、CIE標準光源Cを使用してASTM D1003手順Aに従って測定されたヘイズが6%以下であることを特徴とする、導電性シートまたはフィルム。 - 請求項3に記載の導電性シートまたはフィルムであって、前記基材が、ポリカーボネート、ポリ(メタクリル酸メチル)(PMMA)、ガラス、または前述の少なくとも1種を含む組み合わせを含むことを特徴とする、導電性シートまたはフィルム。
- 請求項3または4に記載の導電性シートまたはフィルムであって、CIE標準光源Cを使用してASTM D1003手順Aに従って測定された透過率が、430THz〜790THzの周波数を有する入射光の70%以上であることを特徴とする、導電性シートまたはフィルム。
- 導電性基材を作製する方法であって、
請求項1から2のいずれか1項に記載の紫外線硬化性転写コーティングを受容基材の第1の表面または供与基材の第1の表面に塗布する工程であって、前記供与基材の前記第1の表面が、そこに結合した導電性コーティングを含む工程、
前記受容基材の前記第1の表面と前記供与基材の前記第1の表面とを一緒にプレス成形して積層体を形成する工程であって、それらの間に前記紫外線硬化性転写コーティングが配置される工程、
前記積層体を加熱する工程、
前記紫外線硬化性転写コーティングを紫外線放射源で活性化させる工程、
前記積層体から前記供与基材を除去して導電性基材を残す工程であって、前記紫外線硬化性転写コーティングが前記受容基材の第1の表面および前記導電性コーティングに接着したままである工程を含み、
前記加熱する工程が、70℃超に加熱する工程をさらに含むことを特徴とする、方法。 - 請求項6に記載の方法であって、前記紫外線硬化性転写コーティングを紫外線放射源で硬化する工程を含むことを特徴とする方法。
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US201461982703P | 2014-04-22 | 2014-04-22 | |
US61/982,703 | 2014-04-22 | ||
PCT/IB2015/052885 WO2015162546A1 (en) | 2014-04-22 | 2015-04-20 | Ultraviolet curable transfer coating for applying nanometer sized metal particles to polymer surface |
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JP2017517597A JP2017517597A (ja) | 2017-06-29 |
JP2017517597A5 JP2017517597A5 (ja) | 2017-08-10 |
JP6526714B2 true JP6526714B2 (ja) | 2019-06-05 |
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EP3177677A1 (en) | 2014-08-07 | 2017-06-14 | SABIC Global Technologies B.V. | Conductive multilayer sheet for thermal forming applications |
US20190152196A1 (en) * | 2015-09-14 | 2019-05-23 | Sabic Global Technologies B.V. | Conductive multilayer sheet for thermal forming and injection molding applications |
CN107254803B (zh) * | 2017-07-14 | 2019-05-24 | 上海维凯光电新材料有限公司 | 用于易碎电子标签纸张的uv涂料及其制备方法 |
CN107573876A (zh) * | 2017-09-15 | 2018-01-12 | 和鸿电气股份有限公司 | 一种银包铜粉填充改性的导电胶粘剂的uv固化工艺 |
KR102036858B1 (ko) * | 2017-12-07 | 2019-10-25 | 건양대학교 산학협력단 | 폴리실라잔을 이용한 uv 경화형 하드 코팅액 및 도막 제조방법 |
JP7135351B2 (ja) * | 2018-03-13 | 2022-09-13 | 東洋インキScホールディングス株式会社 | 硬化物の製造方法 |
EP3963007A1 (en) | 2019-04-30 | 2022-03-09 | SHPP Global Technologies B.V. | Curable poly(polyphenylene ether) oligomer compositions for coatings |
CN111916249B (zh) * | 2020-06-30 | 2022-05-20 | 嘉兴中科枫林生物技术有限公司 | 高性能柔性电子功能基础材料 |
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IL106958A (en) | 1993-09-09 | 1996-06-18 | Ultrafine Techn Ltd | Method of producing high-purity ultra-fine metal powder |
JP3469499B2 (ja) * | 1999-03-16 | 2003-11-25 | 住友ベークライト株式会社 | ダイアタッチペースト |
CN1304506C (zh) * | 2004-11-22 | 2007-03-14 | 中国化工建设总公司常州涂料化工研究院 | 用于转移涂装的紫外光固化涂料 |
SG183720A1 (en) * | 2005-08-12 | 2012-09-27 | Cambrios Technologies Corp | Nanowires-based transparent conductors |
US7320600B2 (en) * | 2005-10-25 | 2008-01-22 | Research In Motion Limited | Device opener and vibration mechanism |
US7662456B2 (en) * | 2005-12-12 | 2010-02-16 | Eastman Kodak Company | Guarded cover sheet for LCD polarizers and method of making the same |
JP5343452B2 (ja) * | 2008-08-26 | 2013-11-13 | Dic株式会社 | 光ディスク用紫外線硬化型組成物および光ディスク |
KR100983219B1 (ko) * | 2008-12-05 | 2010-09-20 | 조근호 | 직접인쇄방식에 의한 인쇄회로기판의 제조방법 및 이에 의하여 제조된 인쇄회로기판 |
JP5158989B2 (ja) * | 2009-06-11 | 2013-03-06 | 高知県 | 転写シートを用いた成形品への加飾膜形成方法 |
JP5472299B2 (ja) * | 2009-06-24 | 2014-04-16 | コニカミノルタ株式会社 | 透明電極、該透明電極に用いられる導電性繊維の精製方法、及び有機エレクトロルミネッセンス素子 |
JP2011178910A (ja) * | 2010-03-02 | 2011-09-15 | Nissha Printing Co Ltd | グラビア印刷適性を有する活性エネルギー線硬化型ハードコート樹脂組成物 |
US20130136874A1 (en) * | 2010-08-18 | 2013-05-30 | 3M Innovative Properties Company | Optical assemblies including stress-relieving optical adhesives and methods of making same |
KR101226696B1 (ko) * | 2011-10-31 | 2013-01-25 | 장성용 | 원터치 장착식 인조네일 |
JP5793142B2 (ja) * | 2011-03-28 | 2015-10-14 | 東レ株式会社 | 導電積層体およびタッチパネル |
WO2013077358A1 (ja) * | 2011-11-22 | 2013-05-30 | 日立化成株式会社 | 感光性樹脂組成物、これを用いた感光性樹脂フィルム、並びにこれらを用いた電子部品 |
CN103013416B (zh) * | 2012-12-19 | 2014-01-01 | 苏州威仕科贸有限公司 | 一种光敏感型玻璃贴膜粘合剂 |
EP3177677A1 (en) * | 2014-08-07 | 2017-06-14 | SABIC Global Technologies B.V. | Conductive multilayer sheet for thermal forming applications |
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EP3134259A1 (en) | 2017-03-01 |
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US20170044394A1 (en) | 2017-02-16 |
CN106715615A (zh) | 2017-05-24 |
JP2017517597A (ja) | 2017-06-29 |
KR20160146840A (ko) | 2016-12-21 |
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