JP6517787B2 - リチウムチタンスピネルの調製方法及びその使用 - Google Patents

リチウムチタンスピネルの調製方法及びその使用 Download PDF

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Publication number
JP6517787B2
JP6517787B2 JP2016517188A JP2016517188A JP6517787B2 JP 6517787 B2 JP6517787 B2 JP 6517787B2 JP 2016517188 A JP2016517188 A JP 2016517188A JP 2016517188 A JP2016517188 A JP 2016517188A JP 6517787 B2 JP6517787 B2 JP 6517787B2
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Japan
Prior art keywords
lithium
tio
composition
lithium titanate
doped
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Expired - Fee Related
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JP2016517188A
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Japanese (ja)
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JP2016526008A (ja
JP2016526008A5 (enExample
Inventor
ステファニー ルデンコ，
ステファニー ルデンコ，
マニュエル ファンツェルト，
マニュエル ファンツェルト，
アンドレア ローマン，
アンドレア ローマン，
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Johnson Matthey PLC
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Johnson Matthey PLC
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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/003—Titanates
    • C01G23/005—Alkali titanates
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00—Secondary cells; Manufacture thereof
    • H01M10/05—Accumulators with non-aqueous electrolyte
    • H01M10/052—Li-accumulators
    • H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/50—Solid solutions
    • C01P2002/52—Solid solutions containing elements as dopants
    • C01P2002/54—Solid solutions containing elements as dopants one element only
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/50—Agglomerated particles
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C01P2004/52—Particles with a specific particle size distribution highly monodisperse size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/027—Negative electrodes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
JP2016517188A 2013-06-05 2014-05-28 リチウムチタンスピネルの調製方法及びその使用 Expired - Fee Related JP6517787B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP13170658 2013-06-05
EP13170658.2 2013-06-05
PCT/EP2014/001451 WO2014194996A1 (en) 2013-06-05 2014-05-28 Process for the preparation of lithium titanium spinel and its use

Publications (3)

Publication Number Publication Date
JP2016526008A JP2016526008A (ja) 2016-09-01
JP2016526008A5 JP2016526008A5 (enExample) 2017-07-13
JP6517787B2 true JP6517787B2 (ja) 2019-05-22

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JP2016517188A Expired - Fee Related JP6517787B2 (ja) 2013-06-05 2014-05-28 リチウムチタンスピネルの調製方法及びその使用

Country Status (9)

Country Link
US (2) US10170758B2 (enExample)
EP (1) EP3003983A1 (enExample)
JP (1) JP6517787B2 (enExample)
KR (1) KR102190774B1 (enExample)
CN (1) CN105358485B (enExample)
BR (1) BR112015030347A2 (enExample)
CA (1) CA2914443C (enExample)
TW (1) TW201509816A (enExample)
WO (1) WO2014194996A1 (enExample)

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CN105244491A (zh) * 2015-10-20 2016-01-13 四川科能锂电有限公司 一种制造钛酸锂锂离子电池负极材料的工艺
WO2017073765A1 (ja) * 2015-10-30 2017-05-04 宇部興産株式会社 蓄電デバイスの電極用リチウムナトリウムチタン複合酸化物粉末、及び活物質材料、並びにそれを用いた電極シートおよび蓄電デバイス
CN105406046A (zh) * 2015-12-21 2016-03-16 深圳市金润能源材料有限公司 钛酸锂负极材料及其制备方法
US20170214038A1 (en) * 2016-01-25 2017-07-27 Ford Cheer International Limited Lithium titanate electrode material, producing method and applications of same
CN107437618B (zh) * 2016-05-27 2022-01-28 松下知识产权经营株式会社 电化学装置
WO2018097429A1 (ko) * 2016-11-22 2018-05-31 주식회사 포스코이에스엠 리튬 티탄 복합 산화물, 이의 제조 방법 및 이를 포함하는 리튬 이차 전지
CN108212074B (zh) * 2016-12-12 2020-09-04 中国科学院过程工程研究所 一种可磁性分离的偏钛酸型锂离子筛、制备方法及其应用
CN106910879B (zh) * 2017-03-29 2019-09-20 天津巴莫科技股份有限公司 原位生成钛酸锂—二氧化钛复合材料及其制备方法
CN111710854A (zh) * 2020-06-18 2020-09-25 电子科技大学 具有氧缺陷的钛酸锂电极材料及制备方法和应用
EP4246613A4 (en) * 2020-11-10 2024-02-07 Ningde Amperex Technology Limited ACTIVE MATERIAL OF NEGATIVE ELECTRODE, ELECTROCHEMICAL APPARATUS USING SAME AND ELECTRONIC DEVICE
CN112701264A (zh) * 2020-12-29 2021-04-23 惠州亿纬锂能股份有限公司 一种锂离子电池正极材料、其制备方法和在锂离子电池中的应用
CN112736233B (zh) * 2021-01-14 2023-01-24 武汉船用电力推进装置研究所（中国船舶重工集团公司第七一二研究所） 一种锂离子电池电极活性物质、制备方法及其电极和电池
JP7484790B2 (ja) * 2021-03-30 2024-05-16 トヨタ自動車株式会社 全固体電池
CN113979475A (zh) * 2021-09-08 2022-01-28 湖北工程学院 一种钛酸铬锂负极材料的制备方法及应用
KR102758444B1 (ko) 2022-09-30 2025-01-23 영남대학교 산학협력단 산소 결함 조절한 미세다공 구조의 스피넬 리튬 티타네이트 및 그 제조방법

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JP3502118B2 (ja) 1993-03-17 2004-03-02 松下電器産業株式会社 リチウム二次電池およびその負極の製造法
JP4768901B2 (ja) 1999-06-03 2011-09-07 チタン工業株式会社 リチウムチタン複合酸化物及びその製造方法、並びにその用途
KR20040005831A (ko) * 2000-10-06 2004-01-16 이 아이 듀폰 디 네모아 앤드 캄파니 고성능 리튬 또는 리튬 이온 전지
JP4495336B2 (ja) 2000-11-10 2010-07-07 株式会社Kri 鉄リン酸リチウムの製造方法。
CA2327370A1 (fr) * 2000-12-05 2002-06-05 Hydro-Quebec Nouvelle methode de fabrication de li4ti5o12 pur a partir du compose ternaire tix-liy-carbone: effet du carbone sur la synthese et la conductivite de l'electrode
DE10117904B4 (de) 2001-04-10 2012-11-15 Zentrum für Sonnenenergie- und Wasserstoff-Forschung Baden-Württemberg Gemeinnützige Stiftung Binäre, ternäre und quaternäre Lithiumeisenphosphate, Verfahren zu ihrer Herstellung und ihre Verwendung
DE10319464A1 (de) 2003-04-29 2004-11-18 Basf Ag Verfahren zur Herstellung von nanokristallinen Lithiumtitanat-Spinellen
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Also Published As

Publication number Publication date
US20160126545A1 (en) 2016-05-05
JP2016526008A (ja) 2016-09-01
US10749173B2 (en) 2020-08-18
CN105358485B (zh) 2020-09-18
KR102190774B1 (ko) 2020-12-15
CA2914443A1 (en) 2014-12-11
EP3003983A1 (en) 2016-04-13
TW201509816A (zh) 2015-03-16
KR20160014698A (ko) 2016-02-11
CN105358485A (zh) 2016-02-24
BR112015030347A2 (pt) 2017-07-25
US10170758B2 (en) 2019-01-01
US20190097224A1 (en) 2019-03-28
CA2914443C (en) 2021-10-12
WO2014194996A1 (en) 2014-12-11

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