JP6170059B2 - ポリ亜リン酸エステル配位子の生産における結晶化溶媒の防止 - Google Patents

ポリ亜リン酸エステル配位子の生産における結晶化溶媒の防止 Download PDF

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JP6170059B2
JP6170059B2 JP2014538998A JP2014538998A JP6170059B2 JP 6170059 B2 JP6170059 B2 JP 6170059B2 JP 2014538998 A JP2014538998 A JP 2014538998A JP 2014538998 A JP2014538998 A JP 2014538998A JP 6170059 B2 JP6170059 B2 JP 6170059B2
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crystals
solvent
group
residual
alkylene
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JP2014532653A (ja
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グレン・エイ・ミラー
ピラモド・ダルウィ
ラヴィンドラクマール・エヌ・ラバル
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ダウ テクノロジー インベストメンツ リミティド ライアビリティー カンパニー
ダウ テクノロジー インベストメンツ リミティド ライアビリティー カンパニー
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    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6564Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
    • C07F9/6571Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
    • C07F9/6574Esters of oxyacids of phosphorus
    • C07F9/65746Esters of oxyacids of phosphorus the molecule containing more than one cyclic phosphorus atom

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
JP2014538998A 2011-10-31 2012-10-25 ポリ亜リン酸エステル配位子の生産における結晶化溶媒の防止 Active JP6170059B2 (ja)

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Application Number Priority Date Filing Date Title
IN3721/CHE/2011 2011-10-31
IN3721CH2011 2011-10-31
PCT/US2012/061874 WO2013066712A1 (en) 2011-10-31 2012-10-25 Preventing solvent of crystallization in production of polyphosphite ligands

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JP2017022824A Division JP6420385B2 (ja) 2011-10-31 2017-02-10 ポリ亜リン酸エステル配位子の生産における結晶化溶媒の防止

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JP2014532653A JP2014532653A (ja) 2014-12-08
JP2014532653A5 JP2014532653A5 (https=) 2015-12-10
JP6170059B2 true JP6170059B2 (ja) 2017-07-26

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JP2014538998A Active JP6170059B2 (ja) 2011-10-31 2012-10-25 ポリ亜リン酸エステル配位子の生産における結晶化溶媒の防止
JP2017022824A Active JP6420385B2 (ja) 2011-10-31 2017-02-10 ポリ亜リン酸エステル配位子の生産における結晶化溶媒の防止

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US (1) US10227365B2 (https=)
EP (1) EP2773649B1 (https=)
JP (2) JP6170059B2 (https=)
CN (1) CN104093729B (https=)
IN (1) IN2014CN03131A (https=)
WO (1) WO2013066712A1 (https=)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9108988B2 (en) 2011-12-30 2015-08-18 Basf Se Method of purifying organic diphosphite compounds
RU2660899C2 (ru) * 2011-12-30 2018-07-11 Басф Се Кристаллический сольват и несольватированные формы 6,6'-[[3,3',5,5'-тетракис(1,1-диметилэтил)-[1,1'-бифенил]-2,2'-диил]бис(окси)]бис-дибензо[d,f][1,3,2]-диоксафосфепина
US8796481B2 (en) 2011-12-30 2014-08-05 Basf Se Crystalline solvate and non-solvated forms of 6,6′-[[3,3′,5,5′-tetrakis(1,1-dimethylethyl)-[1,1′biphenyl]-2,2′-diyl]bis(oxy)]bis-dibenzo [d,f] [1,3,2]-dioxaphosphepine
WO2015175158A1 (en) 2014-05-14 2015-11-19 Dow Technology Investments Llc Stabilized organophosphorous compounds
TWI695009B (zh) * 2015-06-19 2020-06-01 美商陶氏科技投資公司 6,6'-[[3,3',5,5'-肆(1,1-二甲基乙基)-[1,1'-聯二苯]-2,2'-二基]雙(氧基)]雙二苯并[d,f][1,3,2]-二氧雜磷雜庚英之結晶形式
TWI709568B (zh) * 2015-09-30 2020-11-11 美商陶氏科技投資公司 用於製造有機磷化合物的方法
TWI709566B (zh) 2015-09-30 2020-11-11 美商陶氏科技投資公司 用於製造有機磷化合物的方法
US11124531B2 (en) 2017-06-19 2021-09-21 Dow Technology Investments Llc Processes for purifying ligands
EP4229066A1 (en) 2020-10-13 2023-08-23 Dow Silicones Corporation Preparation of organosilicon compounds with aldehyde functionality
EP4508115A1 (en) 2022-04-13 2025-02-19 Dow Global Technologies LLC Preparation of polyether-functional organosilicon compounds

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4182704A (en) * 1976-07-30 1980-01-08 Ciba-Geigy Corporation Hindered phenyl phosphites
DE2733796A1 (de) * 1976-07-30 1978-02-02 Ciba Geigy Ag Neue gehinderte phosphite
US4351759A (en) * 1978-01-03 1982-09-28 Ciba-Geigy Corporation Alkylated 2,2'-biphenylene phosphites and stabilized compositions
US4196117A (en) * 1978-01-03 1980-04-01 Ciba-Geigy Corporation Alkylated 1,1'-biphenyl-2,2'-diyl phosphites and stabilized compositions
DE2940548A1 (de) 1979-10-06 1981-04-16 Hoechst Ag, 6000 Frankfurt Kristallisiertes tris-(2-tert.-butylphenyl)-phosphit und verfahren zu seiner herstellung
US4318845A (en) * 1980-11-24 1982-03-09 Ciba-Geigy Corporation Alkanolamine esters of 1,1'-biphenyl-2,2'-diyl-and alkylidene-1,1'-biphenyl-2,2'-diyl-cyclic phosphites
JPS58103537A (ja) * 1981-12-15 1983-06-20 Adeka Argus Chem Co Ltd 安定化された合成樹脂組成物
US4668651A (en) 1985-09-05 1987-05-26 Union Carbide Corporation Transition metal complex catalyzed processes
US4835299A (en) * 1987-03-31 1989-05-30 Union Carbide Corporation Process for purifying tertiary organophosphites
JPH01121368A (ja) * 1987-11-06 1989-05-15 Adeka Argus Chem Co Ltd 安定化された合成樹脂組成物
KR927003609A (ko) * 1989-12-08 1992-12-18 아이.제이.크라코워 입체장해 아인산 아릴의 제조방법
JP3416956B2 (ja) * 1991-06-11 2003-06-16 三菱化学株式会社 ヒドロホルミル化法およびビスホスファイト化合物
TW213465B (https=) 1991-06-11 1993-09-21 Mitsubishi Chemicals Co Ltd
US5360938A (en) 1991-08-21 1994-11-01 Union Carbide Chemicals & Plastics Technology Corporation Asymmetric syntheses
US5288918A (en) 1992-09-29 1994-02-22 Union Carbide Chemicals & Plastics Technology Corporation Hydroformylation process
DE4238567A1 (de) * 1992-11-16 1994-05-19 Henkel Kgaa Stabilisatormischungen für Polymerisate mit Granaten
US5334739A (en) * 1992-11-30 1994-08-02 Ciba-Geigy Corporation Process an alpha monoclinic crystalline modification of 2,2',2"-nitrilo[triethyl-tris-(3,3',5,5'-tetra-tert-butyl-1,1'-biphenyl-2,2'-diyl)phosphite]
CA2177135C (en) 1993-11-23 2005-04-26 Wilson Tam Processes and catalyst compositions for hydrocyanation of monoolefins
JPH07309884A (ja) * 1994-05-18 1995-11-28 Yotsukaichi Gosei Kk トリスアルキルフェニルホスファイトの製造方法
US5741942A (en) 1996-11-26 1998-04-21 Union Carbide Chemicals & Plastics Technology Corporation Metal-ligand complex catalyzed processes
JPH1053595A (ja) * 1996-05-10 1998-02-24 Sumitomo Chem Co Ltd アリールホスファイト類及びその製造方法
US6069267A (en) 1997-07-29 2000-05-30 E. I. Du Pont De Nemours And Company Selective synthesis of organodiphosphite compounds
DE10360771A1 (de) 2003-12-23 2005-07-28 Oxeno Olefinchemie Gmbh Verfahren zur Herstellung von dreiwertigen Organophosphor-Verbindungen
US8546600B2 (en) * 2008-10-08 2013-10-01 Dow Technology Investments Llc Slurry process for synthesis of bisphosphites and situ use thereof for producing bisphosphite
CN105732703A (zh) 2009-04-21 2016-07-06 因温斯特技术公司 用于制备有机二亚磷酸酯的高选择性方法
DE102011002640B4 (de) * 2011-01-13 2021-10-07 Evonik Operations Gmbh Verfahren zur Aufreinigung von Biphephos

Also Published As

Publication number Publication date
EP2773649B1 (en) 2017-07-12
JP2014532653A (ja) 2014-12-08
US20140288322A1 (en) 2014-09-25
JP2017114881A (ja) 2017-06-29
CN104093729B (zh) 2016-09-07
WO2013066712A1 (en) 2013-05-10
IN2014CN03131A (https=) 2015-07-03
EP2773649A1 (en) 2014-09-10
CN104093729A (zh) 2014-10-08
US10227365B2 (en) 2019-03-12
JP6420385B2 (ja) 2018-11-07

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