JP5946835B2 - 実質的に閉ループの方法およびシステムにおける多結晶シリコンの製造 - Google Patents
実質的に閉ループの方法およびシステムにおける多結晶シリコンの製造 Download PDFInfo
- Publication number
- JP5946835B2 JP5946835B2 JP2013534917A JP2013534917A JP5946835B2 JP 5946835 B2 JP5946835 B2 JP 5946835B2 JP 2013534917 A JP2013534917 A JP 2013534917A JP 2013534917 A JP2013534917 A JP 2013534917A JP 5946835 B2 JP5946835 B2 JP 5946835B2
- Authority
- JP
- Japan
- Prior art keywords
- hydrogen
- trichlorosilane
- gas
- silicon tetrachloride
- hydrogen chloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/021—Preparation
- C01B33/027—Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/021—Preparation
- C01B33/027—Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material
- C01B33/03—Preparation by decomposition or reduction of gaseous or vaporised silicon compounds other than silica or silica-containing material by decomposition of silicon halides or halosilanes or reduction thereof with hydrogen as the only reducing agent
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/037—Purification
- C01B33/039—Purification by conversion of the silicon into a compound, optional purification of the compound, and reconversion into silicon
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/910,553 US8449848B2 (en) | 2010-10-22 | 2010-10-22 | Production of polycrystalline silicon in substantially closed-loop systems |
| US12/910,540 | 2010-10-22 | ||
| US12/910,553 | 2010-10-22 | ||
| US12/910,540 US20120100061A1 (en) | 2010-10-22 | 2010-10-22 | Production of Polycrystalline Silicon in Substantially Closed-loop Processes |
| PCT/US2011/052691 WO2012054170A1 (en) | 2010-10-22 | 2011-09-22 | Production of polycrystalline silicon in substantially closed-loop processes and systems |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013540095A JP2013540095A (ja) | 2013-10-31 |
| JP2013540095A5 JP2013540095A5 (enExample) | 2014-11-06 |
| JP5946835B2 true JP5946835B2 (ja) | 2016-07-06 |
Family
ID=45975555
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013534917A Active JP5946835B2 (ja) | 2010-10-22 | 2011-09-22 | 実質的に閉ループの方法およびシステムにおける多結晶シリコンの製造 |
Country Status (7)
| Country | Link |
|---|---|
| EP (1) | EP2630081B1 (enExample) |
| JP (1) | JP5946835B2 (enExample) |
| KR (1) | KR101948332B1 (enExample) |
| CN (2) | CN103153855A (enExample) |
| BR (1) | BR112013008586A2 (enExample) |
| TW (2) | TW201329280A (enExample) |
| WO (1) | WO2012054170A1 (enExample) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101515117B1 (ko) * | 2014-01-24 | 2015-04-24 | 한화케미칼 주식회사 | 폐가스의 정제방법 및 정제장치 |
| KR101452354B1 (ko) * | 2014-01-24 | 2014-10-22 | 한화케미칼 주식회사 | 폐가스의 정제방법 및 정제장치 |
| CN106061585B (zh) | 2014-01-24 | 2018-12-11 | 韩华化学株式会社 | 废气的净化方法和净化设备 |
| CN104003402B (zh) * | 2014-05-30 | 2016-08-24 | 中国恩菲工程技术有限公司 | 三氯氢硅的提纯方法 |
| KR102009929B1 (ko) * | 2015-09-15 | 2019-08-12 | 주식회사 엘지화학 | 트리클로로실란 제조방법 |
| US10953469B2 (en) * | 2016-04-21 | 2021-03-23 | Tokuyama Corporation | Method of producing metal powder |
| DE102017125232A1 (de) * | 2017-10-27 | 2019-05-02 | Nexwafe Gmbh | Verfahren und Vorrichtung zur kontinuierlichen Gasphasenabscheidung von Silizium auf Substraten |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4092446A (en) * | 1974-07-31 | 1978-05-30 | Texas Instruments Incorporated | Process of refining impure silicon to produce purified electronic grade silicon |
| GB2028289B (en) * | 1978-08-18 | 1982-09-02 | Schumacher Co J C | Producing silicon |
| US4676967A (en) | 1978-08-23 | 1987-06-30 | Union Carbide Corporation | High purity silane and silicon production |
| DE3024319C2 (de) * | 1980-06-27 | 1983-07-21 | Wacker-Chemitronic Gesellschaft für Elektronik-Grundstoffe mbH, 8263 Burghausen | Kontinuierliches Verfahren zur Herstellung von Trichlorsilan |
| US4526769A (en) | 1983-07-18 | 1985-07-02 | Motorola, Inc. | Trichlorosilane production process |
| US5871705A (en) | 1996-09-19 | 1999-02-16 | Tokuyama Corporation | Process for producing trichlorosilane |
| JPH1149508A (ja) * | 1997-06-03 | 1999-02-23 | Tokuyama Corp | 多結晶シリコンの廃棄物の少ない製造方法 |
| US6277194B1 (en) * | 1999-10-21 | 2001-08-21 | Applied Materials, Inc. | Method for in-situ cleaning of surfaces in a substrate processing chamber |
| NO20033207D0 (no) * | 2002-07-31 | 2003-07-15 | Per Kristian Egeberg | Fremgangsmåte og reaktor for fremstilling av höyrent silisium, samt anvendelse av fremgangsmåten og reaktoren ved fremstilling av höyrentsilisium fra uraffinert silisium |
| CN101460398B (zh) * | 2006-04-13 | 2012-08-29 | 卡伯特公司 | 通过闭合环路方法生产硅 |
| US7935327B2 (en) * | 2006-08-30 | 2011-05-03 | Hemlock Semiconductor Corporation | Silicon production with a fluidized bed reactor integrated into a siemens-type process |
| JP5435188B2 (ja) * | 2006-11-14 | 2014-03-05 | 三菱マテリアル株式会社 | 多結晶シリコンの製造方法および多結晶シリコン製造設備 |
| CN101497442B (zh) * | 2008-01-31 | 2012-07-04 | 桑中生 | 一种多晶硅的制备方法 |
| SG192438A1 (en) * | 2008-06-30 | 2013-08-30 | Memc Electronic Materials | Fluidized bed reactor systems and methods for reducing the deposition of silicon on reactor walls |
| US8187361B2 (en) * | 2009-07-02 | 2012-05-29 | America Air Liquide, Inc. | Effluent gas recovery system in polysilicon and silane plants |
| CN102030329B (zh) * | 2009-09-29 | 2012-10-03 | 重庆大全新能源有限公司 | 一种多晶硅生产装置及工艺 |
| DE102010000981A1 (de) * | 2010-01-18 | 2011-07-21 | Evonik Degussa GmbH, 45128 | Closed loop-Verfahren zur Herstellung von Trichlorsilan aus metallurgischem Silicium |
| CN102180467B (zh) * | 2010-12-24 | 2012-12-26 | 江苏中能硅业科技发展有限公司 | Gcl法多晶硅生产方法 |
-
2011
- 2011-09-22 EP EP11761811.6A patent/EP2630081B1/en active Active
- 2011-09-22 KR KR1020137010094A patent/KR101948332B1/ko active Active
- 2011-09-22 JP JP2013534917A patent/JP5946835B2/ja active Active
- 2011-09-22 BR BR112013008586A patent/BR112013008586A2/pt not_active IP Right Cessation
- 2011-09-22 CN CN201180049322XA patent/CN103153855A/zh active Pending
- 2011-09-22 CN CN201710761183.2A patent/CN107555438A/zh active Pending
- 2011-09-22 WO PCT/US2011/052691 patent/WO2012054170A1/en not_active Ceased
- 2011-10-04 TW TW102107553A patent/TW201329280A/zh unknown
- 2011-10-04 TW TW100135943A patent/TWI403610B/zh active
Also Published As
| Publication number | Publication date |
|---|---|
| JP2013540095A (ja) | 2013-10-31 |
| TW201329280A (zh) | 2013-07-16 |
| EP2630081B1 (en) | 2016-04-20 |
| TWI403610B (zh) | 2013-08-01 |
| WO2012054170A1 (en) | 2012-04-26 |
| CN103153855A (zh) | 2013-06-12 |
| BR112013008586A2 (pt) | 2017-07-25 |
| TW201221685A (en) | 2012-06-01 |
| EP2630081A1 (en) | 2013-08-28 |
| CN107555438A (zh) | 2018-01-09 |
| KR20130138357A (ko) | 2013-12-18 |
| KR101948332B1 (ko) | 2019-02-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US8956584B2 (en) | Production of polycrystalline silicon in substantially closed-loop processes that involve disproportionation operations | |
| JP5946835B2 (ja) | 実質的に閉ループの方法およびシステムにおける多結晶シリコンの製造 | |
| JP2013540095A5 (enExample) | ||
| KR20110037967A (ko) | 실리콘 미분의 재순환에 의한 다결정 실리콘 반응로 생산성 향상 방법 | |
| US9394180B2 (en) | Production of polycrystalline silicon in substantially closed-loop systems | |
| JP6037047B2 (ja) | 卜リクロロシラン製造方法 | |
| US8449848B2 (en) | Production of polycrystalline silicon in substantially closed-loop systems | |
| US8974761B2 (en) | Methods for producing silane | |
| US9487406B2 (en) | Systems for producing silane | |
| CN111971253B (zh) | 制备氯硅烷的方法 | |
| KR101580171B1 (ko) | 금속 실리사이드 표면개질 방법, 표면개질된 금속 실리사이드를 이용한 삼염화실란의 제조방법 및 제조장치 | |
| CN103384640A (zh) | 用于制备硅烷的方法和系统 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20140917 |
|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20140917 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20160105 |
|
| RD04 | Notification of resignation of power of attorney |
Free format text: JAPANESE INTERMEDIATE CODE: A7424 Effective date: 20160218 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20160510 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20160601 |
|
| R150 | Certificate of patent or registration of utility model |
Ref document number: 5946835 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
| S531 | Written request for registration of change of domicile |
Free format text: JAPANESE INTERMEDIATE CODE: R313531 |
|
| S533 | Written request for registration of change of name |
Free format text: JAPANESE INTERMEDIATE CODE: R313533 |
|
| R350 | Written notification of registration of transfer |
Free format text: JAPANESE INTERMEDIATE CODE: R350 |
|
| S111 | Request for change of ownership or part of ownership |
Free format text: JAPANESE INTERMEDIATE CODE: R313113 |
|
| R350 | Written notification of registration of transfer |
Free format text: JAPANESE INTERMEDIATE CODE: R350 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |