JP5802213B2 - ５−フッ素−１−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボン酸クロライドの製造方法 - Google Patents

５−フッ素−１−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボン酸クロライドの製造方法 Download PDF

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Publication number
JP5802213B2
JP5802213B2 JP2012539308A JP2012539308A JP5802213B2 JP 5802213 B2 JP5802213 B2 JP 5802213B2 JP 2012539308 A JP2012539308 A JP 2012539308A JP 2012539308 A JP2012539308 A JP 2012539308A JP 5802213 B2 JP5802213 B2 JP 5802213B2
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Prior art keywords
pyrazole
alkyl
fluoroalkyl
carbaldehyde
formula
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Japanese (ja)
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JP2013511485A (ja
Inventor
パツエノク，サージル
ルイ，ノルベルト
コステン，マルク
バーテルス，ギユンター
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Bayer Intellectual Property GmbH
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Bayer Intellectual Property GmbH
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D231/16—Halogen atoms or nitro radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Diaphragms For Electromechanical Transducers (AREA)
  • Finger-Pressure Massage (AREA)
  • Vehicle Interior And Exterior Ornaments, Soundproofing, And Insulation (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2012539308A 2009-11-19 2010-11-17 ５−フッ素−１−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボン酸クロライドの製造方法 Active JP5802213B2 (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US26264109P 2009-11-19 2009-11-19
EP09176426.6 2009-11-19
US61/262,641 2009-11-19
EP09176426A EP2325173A1 (de) 2009-11-19 2009-11-19 Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden
PCT/EP2010/067630 WO2011061205A1 (de) 2009-11-19 2010-11-17 Verfahren zum herstellen von 5-fluor-1-alkyl-3-fluoralkyl-1h-pyrazol-4-carbonsäurechloriden

Publications (2)

Publication Number Publication Date
JP2013511485A JP2013511485A (ja) 2013-04-04
JP5802213B2 true JP5802213B2 (ja) 2015-10-28

Family

ID=42077022

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2012539308A Active JP5802213B2 (ja) 2009-11-19 2010-11-17 ５−フッ素−１−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボン酸クロライドの製造方法

Country Status (13)

Country Link
US (2) US8436191B2 (en:Method)
EP (2) EP2325173A1 (en:Method)
JP (1) JP5802213B2 (en:Method)
KR (2) KR101635046B1 (en:Method)
CN (1) CN102666492B (en:Method)
BR (1) BR112012011961B1 (en:Method)
DK (1) DK2501682T3 (en:Method)
ES (1) ES2600864T3 (en:Method)
IL (1) IL219682A (en:Method)
IN (1) IN2012DN04414A (en:Method)
MX (2) MX2012005676A (en:Method)
TW (1) TWI510473B (en:Method)
WO (1) WO2011061205A1 (en:Method)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR076839A1 (es) * 2009-05-15 2011-07-13 Bayer Cropscience Ag Derivados fungicidas de pirazol carboxamidas
EP2325173A1 (de) 2009-11-19 2011-05-25 Bayer CropScience AG Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden
JP5819938B2 (ja) 2010-04-23 2015-11-24 バイエル・インテレクチュアル・プロパティ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツングＢａｙｅｒ Ｉｎｔｅｌｌｅｃｔｕａｌ Ｐｒｏｐｅｒｔｙ ＧｍｂＨ ５−フルオロ−１−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボニルクロリドおよびフルオリドの調製方法
DK2850066T3 (en) 2012-05-14 2016-04-25 Bayer Cropscience Ag PROCESS FOR THE PREPARATION OF 1-alkyl-3-fluoroalkyl-1H-pyrazole-4-carboxylic acid chlorides
DK2882717T3 (en) 2012-08-07 2017-07-03 Bayer Cropscience Ag PROCEDURE FOR THE PREPARATION OF PERFLUORALLY COOL-CONTAINED PYRAZOL CARBOXYLATES
TWI597270B (zh) * 2013-01-17 2017-09-01 拜耳作物科學公司 製備５－氟－１－甲基－３－二氟甲基－１ｈ－吡唑－４－甲醛的方法
DK3046908T3 (en) * 2013-09-20 2017-10-02 Bayer Cropscience Ag METHOD FOR PREPARING 5-FLOUR-1-ALKYL-3-FLOURALKYL-1H-PYRAZOL-4-CARBALDEHYDE.
CN105934430B (zh) * 2014-01-24 2018-03-16 拜耳作物科学股份公司 制备1‑烷基‑3‑二氟甲基‑5‑氟‑1h‑吡唑‑4‑甲醛和1‑烷基‑3‑二氟甲基‑5‑氟‑1h‑吡唑‑4‑甲酸酯的方法
EP3015458A1 (en) * 2014-11-03 2016-05-04 Bayer CropScience AG Process for preparing 3,5-bis(haloalkyl)pyrazole derivatives from a,a-dihaloamines and ketimines
CN106164049B (zh) 2014-03-24 2019-04-12 拜耳作物科学股份公司 由α,α-二卤胺和酮亚胺制备3,5-二(卤代烷基)吡唑衍生物的方法
TWI705055B (zh) 2015-04-29 2020-09-21 德商拜耳作物科學公司 製備5-氟-1h-吡唑-4-羰基氟化物之方法
JP6911143B2 (ja) 2018-11-07 2021-07-28 福建永晶科技股▲ふん▼有限公司Ｆｕｊｉａｎ Ｙｏｎｇｊｉｎｇ Ｔｅｃｈｎｏｌｏｇｙ Ｃｏ．， Ｌｔｄ ピラゾール又はピリミジノンの新しい製造方法
WO2021082997A1 (zh) 2019-10-29 2021-05-06 沈阳中化农药化工研发有限公司 一种含取代苯乙酮结构片段的酰胺类化合物及其制备方法和用途
WO2022233129A1 (en) 2021-05-05 2022-11-10 Fujian Yongjing Technology Co., Ltd New process for the synthesis of 5-fluoro-3- (difuoromethyl) -5-fluoro-1-methyl-1h-pyrazole-4-carboxylic acid derivatives and the free acid thereof

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5223526A (en) * 1991-12-06 1993-06-29 Monsanto Company Pyrazole carboxanilide fungicides and use
DE19544800A1 (de) * 1995-12-01 1997-06-05 Bayer Ag Verfahren zur Herstellung von 1,3-Dimethyl-5-fluor-pyrazol-4-carboxaniliden
JP4465133B2 (ja) 2001-02-08 2010-05-19 クミアイ化学工業株式会社 イソオキサゾリン誘導体及びこれを有効成分とする除草剤
EP1405853B1 (en) * 2001-06-21 2010-11-03 Kumiai Chemical Industry Co., Ltd. Isoxazoline derivatives and herbicides
UA78071C2 (en) 2002-08-07 2007-02-15 Kumiai Chemical Industry Co Herbicidal composition
RU2346996C2 (ru) 2004-06-29 2009-02-20 ЮРОПИЭН НИКЕЛЬ ПиЭлСи Усовершенствованное выщелачивание основных металлов
SI1781662T1 (sl) 2004-08-18 2011-07-29 Pfizer Zaviralci RNA-odvisne RNA-polimeraze hepatitisa C in sestavki in zdravljenja, v katerih se uporabljajo
MX2007016203A (es) 2005-06-29 2008-03-10 Compumedics Ltd Ensamble de sensor con puente conductivo.
DE102005044451A1 (de) * 2005-09-17 2007-03-22 Bayer Cropscience Gmbh Verfahren zum Herstellen von 5-Fluor-1,3-dialkyl-1H-pyrazol-4-carbonsäurefluoriden
DE602006021374D1 (de) * 2005-09-27 2011-06-01 Fujifilm Corp Lithographisches Druckverfahren
AR056882A1 (es) 2006-02-01 2007-10-31 Bayer Cropscience Sa Derivados del fungicida n- cicloalquil- bencil- amida
DE102007002674A1 (de) * 2007-01-18 2008-07-24 Bayer Cropscience Ag Verfahren zum Herstellen von substituierten Pyrazolcarbonsäurechloriden
EP2325173A1 (de) 2009-11-19 2011-05-25 Bayer CropScience AG Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden

Also Published As

Publication number Publication date
EP2501682A1 (de) 2012-09-26
KR20160054041A (ko) 2016-05-13
WO2011061205A1 (de) 2011-05-26
EP2501682B1 (de) 2016-08-03
BR112012011961B1 (pt) 2018-05-08
CN102666492A (zh) 2012-09-12
US8436191B2 (en) 2013-05-07
IL219682A (en) 2016-08-31
US20110207940A1 (en) 2011-08-25
KR101749561B1 (ko) 2017-06-21
DK2501682T3 (en) 2016-11-14
BR112012011961A2 (pt) 2015-09-08
TW201127817A (en) 2011-08-16
US8765971B2 (en) 2014-07-01
JP2013511485A (ja) 2013-04-04
KR20120084325A (ko) 2012-07-27
MX2012005676A (es) 2012-06-19
IL219682A0 (en) 2012-07-31
TWI510473B (zh) 2015-12-01
US20130165664A1 (en) 2013-06-27
ES2600864T3 (es) 2017-02-13
MX344246B (es) 2016-12-07
CN102666492B (zh) 2016-03-23
KR101635046B1 (ko) 2016-07-01
EP2325173A1 (de) 2011-05-25
IN2012DN04414A (en:Method) 2015-08-07

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