JP5802213B2 - ５−フッ素−１−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボン酸クロライドの製造方法 - Google Patents
５−フッ素−１−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボン酸クロライドの製造方法 Download PDFInfo
- Publication number
- JP5802213B2 JP5802213B2 JP2012539308A JP2012539308A JP5802213B2 JP 5802213 B2 JP5802213 B2 JP 5802213B2 JP 2012539308 A JP2012539308 A JP 2012539308A JP 2012539308 A JP2012539308 A JP 2012539308A JP 5802213 B2 JP5802213 B2 JP 5802213B2
- Authority
- JP
- Japan
- Prior art keywords
- pyrazole
- alkyl
- fluoroalkyl
- carbaldehyde
- formula
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/16—Halogen atoms or nitro radicals
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- General Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Plural Heterocyclic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Diaphragms For Electromechanical Transducers (AREA)
- Finger-Pressure Massage (AREA)
- Vehicle Interior And Exterior Ornaments, Soundproofing, And Insulation (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US26264109P | 2009-11-19 | 2009-11-19 | |
| EP09176426.6 | 2009-11-19 | ||
| EP09176426A EP2325173A1 (de) | 2009-11-19 | 2009-11-19 | Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden |
| US61/262,641 | 2009-11-19 | ||
| PCT/EP2010/067630 WO2011061205A1 (de) | 2009-11-19 | 2010-11-17 | Verfahren zum herstellen von 5-fluor-1-alkyl-3-fluoralkyl-1h-pyrazol-4-carbonsäurechloriden |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2013511485A JP2013511485A (ja) | 2013-04-04 |
| JP5802213B2 true JP5802213B2 (ja) | 2015-10-28 |
Family
ID=42077022
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012539308A Active JP5802213B2 (ja) | 2009-11-19 | 2010-11-17 | ５−フッ素−１−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボン酸クロライドの製造方法 |
Country Status (13)
| Country | Link |
|---|---|
| US (2) | US8436191B2 (OSRAM) |
| EP (2) | EP2325173A1 (OSRAM) |
| JP (1) | JP5802213B2 (OSRAM) |
| KR (2) | KR101749561B1 (OSRAM) |
| CN (1) | CN102666492B (OSRAM) |
| BR (1) | BR112012011961B1 (OSRAM) |
| DK (1) | DK2501682T3 (OSRAM) |
| ES (1) | ES2600864T3 (OSRAM) |
| IL (1) | IL219682A (OSRAM) |
| IN (1) | IN2012DN04414A (OSRAM) |
| MX (2) | MX344246B (OSRAM) |
| TW (1) | TWI510473B (OSRAM) |
| WO (1) | WO2011061205A1 (OSRAM) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AR076839A1 (es) * | 2009-05-15 | 2011-07-13 | Bayer Cropscience Ag | Derivados fungicidas de pirazol carboxamidas |
| EP2325173A1 (de) | 2009-11-19 | 2011-05-25 | Bayer CropScience AG | Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden |
| BR112012027170B1 (pt) | 2010-04-23 | 2018-02-14 | Bayer Intellectual Property Gmbh | Processo para a preparação de cloretos e fluoretos de 5-fluoro-1-alquil-3-fluoroalquil-1h- pirazol-4-carbonila, bem como compostos intermediários dos mesmos |
| ES2568979T3 (es) | 2012-05-14 | 2016-05-05 | Bayer Cropscience Ag | Procedimiento de preparación de cloruros de ácido 1-alquil-3-fluoroalquil-1H-pirazol-4-carboxílico |
| DK2882717T3 (en) | 2012-08-07 | 2017-07-03 | Bayer Cropscience Ag | PROCEDURE FOR THE PREPARATION OF PERFLUORALLY COOL-CONTAINED PYRAZOL CARBOXYLATES |
| ES2610380T3 (es) | 2013-01-17 | 2017-04-27 | Bayer Cropscience Ag | Procedimiento de preparación de 5-fluoro-1-metil-3-difluorometil-1H-pirazol-4-carbaldehído |
| JP6366722B2 (ja) * | 2013-09-20 | 2018-08-01 | バイエル・クロップサイエンス・アクチェンゲゼルシャフト | ５−フルオロ−１−アルキル−３−フルオロアルキル−１ｈ−ピラゾール−４−カルボアルデヒドの製造方法 |
| KR102319577B1 (ko) * | 2014-01-24 | 2021-10-29 | 바이엘 크롭사이언스 악티엔게젤샤프트 | １-알킬-３-디플루오로메틸-５-플루오르-１ｈ-피라졸-４-카르브알데히드 및 １-알킬-３-디플루오로메틸-５-플루오르-１ｈ-피라졸-４-카르복실레이트의 제조 방법 |
| KR102410034B1 (ko) | 2014-03-24 | 2022-06-15 | 바이엘 크롭사이언스 악티엔게젤샤프트 | α,α-디할로아민 및 케트이민으로부터 3,5-비스(할로알킬)피라졸 유도체의 제조방법 |
| EP3015458A1 (en) * | 2014-11-03 | 2016-05-04 | Bayer CropScience AG | Process for preparing 3,5-bis(haloalkyl)pyrazole derivatives from a,a-dihaloamines and ketimines |
| TWI705055B (zh) | 2015-04-29 | 2020-09-21 | 德商拜耳作物科學公司 | 製備5-氟-1h-吡唑-4-羰基氟化物之方法 |
| JP6911143B2 (ja) | 2018-11-07 | 2021-07-28 | 福建永晶科技股▲ふん▼有限公司Ｆｕｊｉａｎ Ｙｏｎｇｊｉｎｇ Ｔｅｃｈｎｏｌｏｇｙ Ｃｏ．， Ｌｔｄ | ピラゾール又はピリミジノンの新しい製造方法 |
| WO2021082997A1 (zh) | 2019-10-29 | 2021-05-06 | 沈阳中化农药化工研发有限公司 | 一种含取代苯乙酮结构片段的酰胺类化合物及其制备方法和用途 |
| WO2022233129A1 (en) | 2021-05-05 | 2022-11-10 | Fujian Yongjing Technology Co., Ltd | New process for the synthesis of 5-fluoro-3- (difuoromethyl) -5-fluoro-1-methyl-1h-pyrazole-4-carboxylic acid derivatives and the free acid thereof |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5223526A (en) * | 1991-12-06 | 1993-06-29 | Monsanto Company | Pyrazole carboxanilide fungicides and use |
| DE19544800A1 (de) * | 1995-12-01 | 1997-06-05 | Bayer Ag | Verfahren zur Herstellung von 1,3-Dimethyl-5-fluor-pyrazol-4-carboxaniliden |
| JP4465133B2 (ja) | 2001-02-08 | 2010-05-19 | クミアイ化学工業株式会社 | イソオキサゾリン誘導体及びこれを有効成分とする除草剤 |
| WO2003000686A1 (en) * | 2001-06-21 | 2003-01-03 | Kumiai Chemical Industry Co., Ltd. | Isoxazoline derivatives and herbicides |
| UA78071C2 (en) | 2002-08-07 | 2007-02-15 | Kumiai Chemical Industry Co | Herbicidal composition |
| EP1769092A4 (en) | 2004-06-29 | 2008-08-06 | Europ Nickel Plc | IMPROVED LIXIVIATION OF BASE METALS |
| PL1781662T3 (pl) | 2004-08-18 | 2011-08-31 | Pfizer | Inhibitory zależnej od RNA polimerazy RNA wirusa zapalenia wątroby typu C, i kompozycje i terapie wykorzystujące je |
| MX2007016203A (es) | 2005-06-29 | 2008-03-10 | Compumedics Ltd | Ensamble de sensor con puente conductivo. |
| DE102005044451A1 (de) * | 2005-09-17 | 2007-03-22 | Bayer Cropscience Gmbh | Verfahren zum Herstellen von 5-Fluor-1,3-dialkyl-1H-pyrazol-4-carbonsäurefluoriden |
| ATE506185T1 (de) * | 2005-09-27 | 2011-05-15 | Fujifilm Corp | Lithographisches druckverfahren |
| AR056882A1 (es) | 2006-02-01 | 2007-10-31 | Bayer Cropscience Sa | Derivados del fungicida n- cicloalquil- bencil- amida |
| DE102007002674A1 (de) * | 2007-01-18 | 2008-07-24 | Bayer Cropscience Ag | Verfahren zum Herstellen von substituierten Pyrazolcarbonsäurechloriden |
| EP2325173A1 (de) | 2009-11-19 | 2011-05-25 | Bayer CropScience AG | Verfahren zum Herstellen von 5-Fluor-1-alkyl-3-fluoralkyl-1H-pyrazol-4-carbonsäurechloriden |
-
2009
- 2009-11-19 EP EP09176426A patent/EP2325173A1/de not_active Ceased
-
2010
- 2010-11-17 BR BR112012011961A patent/BR112012011961B1/pt active IP Right Grant
- 2010-11-17 KR KR1020167011442A patent/KR101749561B1/ko active Active
- 2010-11-17 ES ES10782247.0T patent/ES2600864T3/es active Active
- 2010-11-17 IN IN4414DEN2012 patent/IN2012DN04414A/en unknown
- 2010-11-17 WO PCT/EP2010/067630 patent/WO2011061205A1/de not_active Ceased
- 2010-11-17 EP EP10782247.0A patent/EP2501682B1/de active Active
- 2010-11-17 KR KR1020127015772A patent/KR101635046B1/ko active Active
- 2010-11-17 MX MX2013009578A patent/MX344246B/es unknown
- 2010-11-17 DK DK10782247.0T patent/DK2501682T3/en active
- 2010-11-17 MX MX2012005676A patent/MX2012005676A/es active IP Right Grant
- 2010-11-17 JP JP2012539308A patent/JP5802213B2/ja active Active
- 2010-11-17 CN CN201080052388.XA patent/CN102666492B/zh active Active
- 2010-11-18 TW TW099139630A patent/TWI510473B/zh active
- 2010-11-19 US US12/950,849 patent/US8436191B2/en active Active
-
2012
- 2012-05-09 IL IL219682A patent/IL219682A/en active IP Right Grant
-
2013
- 2013-02-19 US US13/770,720 patent/US8765971B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN102666492B (zh) | 2016-03-23 |
| EP2501682B1 (de) | 2016-08-03 |
| BR112012011961A2 (pt) | 2015-09-08 |
| IN2012DN04414A (OSRAM) | 2015-08-07 |
| US8436191B2 (en) | 2013-05-07 |
| KR101635046B1 (ko) | 2016-07-01 |
| WO2011061205A1 (de) | 2011-05-26 |
| KR20160054041A (ko) | 2016-05-13 |
| US8765971B2 (en) | 2014-07-01 |
| US20110207940A1 (en) | 2011-08-25 |
| JP2013511485A (ja) | 2013-04-04 |
| BR112012011961B1 (pt) | 2018-05-08 |
| TWI510473B (zh) | 2015-12-01 |
| US20130165664A1 (en) | 2013-06-27 |
| IL219682A0 (en) | 2012-07-31 |
| DK2501682T3 (en) | 2016-11-14 |
| KR20120084325A (ko) | 2012-07-27 |
| CN102666492A (zh) | 2012-09-12 |
| IL219682A (en) | 2016-08-31 |
| KR101749561B1 (ko) | 2017-06-21 |
| MX344246B (es) | 2016-12-07 |
| TW201127817A (en) | 2011-08-16 |
| ES2600864T3 (es) | 2017-02-13 |
| MX2012005676A (es) | 2012-06-19 |
| EP2325173A1 (de) | 2011-05-25 |
| EP2501682A1 (de) | 2012-09-26 |
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