JP5683499B2 - 柱状化ケイ酸塩の製造方法 - Google Patents

柱状化ケイ酸塩の製造方法 Download PDF

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JP5683499B2
JP5683499B2 JP2011552431A JP2011552431A JP5683499B2 JP 5683499 B2 JP5683499 B2 JP 5683499B2 JP 2011552431 A JP2011552431 A JP 2011552431A JP 2011552431 A JP2011552431 A JP 2011552431A JP 5683499 B2 JP5683499 B2 JP 5683499B2
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silicate
mixture
rub
group
range
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JP2012519637A5 (enExample
JP2012519637A (ja
Inventor
イルマズ,ビルジ
ミュラー,ウルリヒ
シャオ,フォン−ショウ
ギース,ヘルマン
辰巳 敬
敬 辰巳
フォス,ディルク デ
フォス,ディルク デ
パオ,シンホー
チャン,ウェイピン
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BASF SE
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/005Silicates, i.e. so-called metallosilicalites or metallozeosilites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/05Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/02Crystalline silica-polymorphs, e.g. silicalites dealuminated aluminosilicate zeolites
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026After-treatment
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46Other types characterised by their X-ray diffraction pattern and their defined composition
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/16Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3201Alkali metal oxides or oxide-forming salts thereof
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
    • C04B2235/3222Aluminates other than alumino-silicates, e.g. spinel (MgAl2O4)
    • CCHEMISTRY; METALLURGY
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    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427Silicates other than clay, e.g. water glass
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54Particle size related information
    • C04B2235/5409Particle size related information expressed by specific surface values

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Structural Engineering (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
JP2011552431A 2009-03-03 2010-03-03 柱状化ケイ酸塩の製造方法 Expired - Fee Related JP5683499B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
PCT/CN2009/070617 WO2010099649A1 (en) 2009-03-03 2009-03-03 Process for preparation of pillared silicates
CNPCT/CN2009/070617 2009-03-03
PCT/EP2010/052695 WO2010100191A2 (en) 2009-03-03 2010-03-03 Process for the preparation of pillared silicates

Publications (3)

Publication Number Publication Date
JP2012519637A JP2012519637A (ja) 2012-08-30
JP2012519637A5 JP2012519637A5 (enExample) 2013-05-02
JP5683499B2 true JP5683499B2 (ja) 2015-03-11

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ID=42709196

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JP2011552431A Expired - Fee Related JP5683499B2 (ja) 2009-03-03 2010-03-03 柱状化ケイ酸塩の製造方法

Country Status (5)

Country Link
US (1) US9260313B2 (enExample)
EP (1) EP2406184B1 (enExample)
JP (1) JP5683499B2 (enExample)
WO (2) WO2010099649A1 (enExample)
ZA (1) ZA201107109B (enExample)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010099652A1 (en) * 2009-03-03 2010-09-10 Basf Se Process for preparation of layered silicate, layered silicate prepared by process, and uses thereof
WO2010099649A1 (en) 2009-03-03 2010-09-10 Basf Se Process for preparation of pillared silicates
WO2010099650A1 (en) * 2009-03-03 2010-09-10 Basf Se Isomorphously substituted silicate
US20140113981A1 (en) * 2012-10-19 2014-04-24 Basf Se Catalyst for the Conversion of Syngas to Olefins and Preparation Thereof
WO2015032851A2 (en) * 2013-09-06 2015-03-12 Basf Se Silicon-bridged pillared silicate compounds and process for their production
CN105819460B (zh) * 2015-01-04 2018-09-14 神华集团有限责任公司 一种氢型层柱皂石及其制备方法和应用

Family Cites Families (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS62278174A (ja) * 1986-05-26 1987-12-03 松下電工株式会社 無機層状多孔体の製法
US5200058A (en) * 1990-01-25 1993-04-06 Mobil Oil Corp. Catalytic conversion over modified synthetic mesoporous crystalline material
DE4117323A1 (de) * 1991-05-27 1992-12-03 Henkel Kgaa Vereinfachtes verfahren zur herstellung von hoch-quellfaehigen schichtsilikaten (iv)
CN1127522C (zh) * 1998-08-20 2003-11-12 出光石油化学株式会社 烯烃聚合物生产用催化剂、其生产方法、和烯烃聚合物的生产方法
JP2003020304A (ja) * 2001-07-09 2003-01-24 Japan Polychem Corp オレフィン重合用触媒成分、オレフィン重合用触媒、及び、オレフィン重合用触媒成分の製造方法
DE102004017915A1 (de) 2004-04-13 2005-11-03 Basf Ag Mikroporöses Gerüstsilikat und Verfahren zu seiner Herstellung
US8343880B2 (en) * 2004-12-15 2013-01-01 Uop Llc Process for preparing a dielectric interlayer film containing silicon beta zeolite
DE102005049362A1 (de) 2005-10-12 2007-04-19 Basf Ag Verfahren zur Herstellung eines Silikates
WO2008044873A1 (en) * 2006-10-10 2008-04-17 Korea Institute Of Industrial Technology Method for preparing permanently hydrophobic aerogel and permanently hydrophobic aerogel prepared by using the method
KR20100016236A (ko) 2007-04-04 2010-02-12 바스프 에스이 헤테로원자 함유 실리케이트의 제조 방법
EP2155390B1 (de) 2007-04-24 2012-10-17 Basf Se Metallorganische gerüstmaterialien mit hexagonal-trigonaler struktur basierend auf aluminium, eisen oder chrom, sowie einer dicarbonsäure
WO2008129024A1 (de) 2007-04-24 2008-10-30 Basf Se Mit katalysator-metallkomponenten beladene poröse metallorganische gerüstmaterialien
ITMI20070932A1 (it) 2007-05-08 2008-11-09 Basf Ag Procedimento per la preparazione di un ossido olefinico
WO2008142059A1 (de) 2007-05-21 2008-11-27 Basf Se Aluminium-aminocarboxylate als poröse metallorganische gerüstmaterialien
EP2394989A1 (de) 2007-06-20 2011-12-14 Basf Se Verfahren zur Herstellung eines N-substituierten Aziridins
WO2009007267A1 (en) 2007-07-10 2009-01-15 Basf Se Process for the separation of unbranched hydrocarbons from their branched isomers
WO2009059941A1 (de) 2007-11-06 2009-05-14 Basf Se Verfahren zur regioselektiven alkoxyalkylierung von substituierten benzolen
WO2009059944A1 (de) 2007-11-06 2009-05-14 Basf Se Elektrochemisches verfahren zur herstellung von benzaldehyddimethylacetalen
CN101230210B (zh) * 2007-12-28 2011-10-26 河北工业大学 有机改性硅酸盐矿物粘土的制备方法
ATE534452T1 (de) 2008-01-24 2011-12-15 Basf Se Poröse metallorganische gerüstmaterialien als trockenmittel
US8343261B2 (en) 2008-03-17 2013-01-01 Basf Se Use of formate-based porous metal organic frameworks for methane storage
DE112009000581A5 (de) 2008-04-08 2011-02-17 Basf Se Katalysator zur Dehydroaromatisierung von aliphatischen Kohlenwasserstoffen mit siliziumhaltigem Bindemittel
US8742189B2 (en) 2008-04-08 2014-06-03 Basf Se Catalyst for the dehydroaromatisation of methane and mixtures containing methane
US8715618B2 (en) 2008-05-21 2014-05-06 Basf Se Process for the direct synthesis of Cu containing zeolites having CHA structure
CN102105421B (zh) 2008-07-21 2013-09-25 巴斯夫欧洲公司 工业分离丙烯的方法
ES2390646T3 (es) 2008-07-30 2012-11-15 Basf Se Materiales estructurales organometálicos a base de litio
EP2172426A1 (de) 2008-10-02 2010-04-07 Ruhr-Universität Bochum Templatfreie Clathrasile und Clathrasil-Membranen
MX2011007483A (es) 2009-01-14 2011-08-04 Basf Se Unidades de aislamiento de vacio con materiales adquiridores.
WO2010099651A1 (en) 2009-03-03 2010-09-10 Basf Se Process for preparation of isomorphously substituted layered silicate, silicate prepared by process, and uses thereof
WO2010099650A1 (en) 2009-03-03 2010-09-10 Basf Se Isomorphously substituted silicate
WO2010099649A1 (en) 2009-03-03 2010-09-10 Basf Se Process for preparation of pillared silicates
WO2010099652A1 (en) 2009-03-03 2010-09-10 Basf Se Process for preparation of layered silicate, layered silicate prepared by process, and uses thereof

Also Published As

Publication number Publication date
WO2010100191A2 (en) 2010-09-10
EP2406184A2 (en) 2012-01-18
US9260313B2 (en) 2016-02-16
WO2010100191A3 (en) 2011-05-12
US20110319250A1 (en) 2011-12-29
EP2406184B1 (en) 2013-05-15
ZA201107109B (en) 2012-12-27
WO2010099649A1 (en) 2010-09-10
JP2012519637A (ja) 2012-08-30

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