JP5683107B2 - プロセスフローストリーム採取システム - Google Patents
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0203—Solvent extraction of solids with a supercritical fluid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0403—Solvent extraction of solutions which are liquid with a supercritical fluid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0403—Solvent extraction of solutions which are liquid with a supercritical fluid
- B01D11/0407—Solvent extraction of solutions which are liquid with a supercritical fluid the supercritical fluid acting as solvent for the solute
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0484—Controlling means
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
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- B01D19/0021—Degasification of liquids by bringing the liquid in a thin layer
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0042—Degasification of liquids modifying the liquid flow
- B01D19/0052—Degasification of liquids modifying the liquid flow in rotating vessels, vessels containing movable parts or in which centrifugal movement is caused
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
- B01D15/40—Selective adsorption, e.g. chromatography characterised by the separation mechanism using supercritical fluid as mobile phase or eluent
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T137/00—Fluid handling
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- Y10T137/3003—Fluid separating traps or vents
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- Sampling And Sample Adjustment (AREA)
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Description
Claims (14)
- 流体と混合された圧力下の液化気体又は超臨界流体を含むフローストリームから、液体フローを採取するプロセスに使用される装置において、
注入口と、液体フローの排出口と、気体フローの排出口とを有する容器として形成されているスプリッタであって、注入口は、スプリッタにフローストリームを送る排出ラインを受け入れるスプリッタを備えており、
スプリッタは、フローストリーム中の気相がフローストリームから分離されて、スプリッタを出るための非制限ゾーンを生成し、
フローストリームから液相を分離して、制限されることなくスプリッタの外に流すと共に、スプリッタの外へと液相が流れる経路を気相が進むことを防止する制限ゾーンを更に備えており、
スプリッタの下部の内壁は、スプリッタの内部空間が液体フローの排出口に向かって狭くなるようにテーパー状に形成されており、スプリッタの上部の内壁は、スプリッタの内部空間が気体フローの排出口に向かって狭くなるようにテーパー状に形成されており、
排出ラインは、注入口を通ってスプリッタの内部空間へと延びており、スプリッタの上部の内壁の一部にぶつかるように、水平方向に対して下側に傾いた角度でフローストリームを排出する装置。 - スプリッタ内が大気圧又は大気圧に近い圧力である状態で、フローストリームから液相が分離されて、液体フローの排出口からスプリッタの外へと重力排出される、請求項1の装置。
- スプリッタ内が大気圧又は大気圧に近い圧力である状態で、フローストリームから気相が分離されて、気体フローの排出口からスプリッタの外へと排気される、請求項1の装置。
- スプリッタは、スムースな内壁を有するように形成されており、液体フローの排出口に向かって内壁の直径が減少する、請求項1の装置。
- 液体フローの排出口は、スプリッタの細長い下端に形成されており、スプリッタの外へ液体フローの重力排出がもたらされる、請求項1の装置。
- 接続管を用いて液体フローの排出口に接続されており、スプリッタから液体フローを受け取る採取容器を更に備えている、請求項1の装置。
- 複数のスプリッタをサポートに保持するマニホールドを更に備えており、各スプリッタからの気体フローの排出口は、マニホールドの共通の気体排出口に接続されている、請求項1の装置。
- フローストリームを生成する超臨界ガスクロマトグラフィシステム及び超臨界流体抽出システムの何れかに接続されている、請求項1の装置。
- 流体と混合された圧力下の液化気体又は超臨界流体を含むフローストリームから、液体フローを採取する方法において、
スプリッタへのフローストリームを受け取る工程であって、スプリッタは、注入口と、液体フローの排出口と、気体フローの排出口とを有する容器として形成されており、注入口は、スプリッタにフローストリームを送る排出ラインを受け入れる工程と、
フローストリームの気相をフローストリームから分離して、スプリッタから出すための非制限ゾーンを与える工程と、
フローストリームから液相を分離して、制限されることなくスプリッタの外に流すと共に、スプリッタの外へと液相が流れる経路を気相が進むことを防止する制限ゾーンを与える工程とを備えており、
スプリッタの下部の内壁は、スプリッタの内部空間が液体フローの排出口に向かって狭くなるようにテーパー状に形成されており、スプリッタの上部の内壁は、スプリッタの内部空間が気体フローの排出口に向かって狭くなるようにテーパー状に形成されており、
スプリッタにフローストリームを送る排出ラインは、注入口を通ってスプリッタの内部空間へと延びており、
スプリッタの上部の内壁の一部にぶつかるように、水平方向に対して下側に傾いた角度でフローストリームを排出する工程を更に含んでいる方法。 - 制限ゾーンを与える工程では、スプリッタ内が大気圧又は大気圧に近い圧力である状態で、フローストリームから液相が分離されて、液体フローの排出口からスプリッタの外へと重力排出される、請求項9の方法。
- 非制限ゾーンを与える工程では、スプリッタ内が大気圧又は大気圧に近い圧力である状態で、フローストリームから気相が分離されて、気体フローの排出口からスプリッタの外へと排気される、請求項9の方法。
- スプリッタは、スムースな内壁を有するように形成されており、液体フローの排出口に向かって内壁の直径が減少する、請求項9の方法。
- 液体フローの排出口は、スプリッタの細長い下端に形成されており、スプリッタの外へ液体フローの重力排出がもたらされる、請求項9の方法。
- フローストリームがスプリッタに入る前にフローストリームの温度調整をする工程を更に含む、請求項9の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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US11/487,581 US7964029B2 (en) | 2006-07-17 | 2006-07-17 | Process flowstream collection system |
US11/487,581 | 2006-07-17 | ||
PCT/US2007/073696 WO2008011416A2 (en) | 2006-07-17 | 2007-07-17 | Process flowstream collection system |
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JP2009544042A JP2009544042A (ja) | 2009-12-10 |
JP5683107B2 true JP5683107B2 (ja) | 2015-03-11 |
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US (2) | US7964029B2 (ja) |
EP (1) | EP2040819B1 (ja) |
JP (1) | JP5683107B2 (ja) |
WO (1) | WO2008011416A2 (ja) |
Families Citing this family (28)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7813627B2 (en) * | 2006-09-29 | 2010-10-12 | Praxair Technology, Inc. | Low vapor pressure high purity gas delivery system |
JP4675406B2 (ja) | 2008-09-29 | 2011-04-20 | 日本分光株式会社 | 超臨界流体システムにおける試料回収容器と、試料回収装置および試料回収方法 |
CN102216769B (zh) * | 2008-11-12 | 2014-10-29 | 沃特世科技公司 | 用于提纯流动流的收集系统 |
US8419936B2 (en) * | 2010-03-23 | 2013-04-16 | Agilent Technologies, Inc. | Low noise back pressure regulator for supercritical fluid chromatography |
WO2012040252A2 (en) * | 2010-09-20 | 2012-03-29 | Aurora Sfc Systems, Inc. | System and process for an active drain for gas-liquid separators |
JP6031098B2 (ja) * | 2011-06-17 | 2016-11-24 | ウオーターズ・テクノロジーズ・コーポレイシヨン | 超臨界流体クロマトグラフィー用の開放型常圧回収のための方法および装置 |
WO2012177259A1 (en) * | 2011-06-23 | 2012-12-27 | Aurora Sfc Systems, Llc | A low noise back pressure regulator for supercritical fluid chromatography |
US20130333467A1 (en) * | 2012-06-19 | 2013-12-19 | Waters Technologies Corporation | Measuring Fluid Density |
CN107694217B (zh) * | 2012-07-18 | 2020-11-27 | 亚历山大·博齐克 | 气液分离器 |
CN104813163B (zh) * | 2012-11-28 | 2019-05-14 | 株式会社岛津制作所 | 超临界流体处理装置 |
KR101497641B1 (ko) * | 2013-05-28 | 2015-03-03 | 엔비스아나(주) | 시료 샘플링 장치, 시료 샘플링 방법 및 시료 샘플링 분석 시스템 |
JP6406358B2 (ja) * | 2014-12-05 | 2018-10-17 | 株式会社島津製作所 | 試料回収機構及びその試料回収機構を備えた超臨界流体装置 |
CN107107076B (zh) | 2015-01-30 | 2019-11-08 | 安捷伦科技有限公司 | 撞击式离心分离器及其制造方法和级分收集系统 |
CN107430099B (zh) * | 2015-03-19 | 2020-04-03 | 株式会社岛津制作所 | 超临界流体装置 |
EP3281008B1 (en) * | 2015-04-10 | 2024-05-29 | Waters Technologies Corporation | Cooling a liquid eluent of a carbon dioxide based chromatography system after gas-liquid separation |
JP6921759B2 (ja) * | 2015-06-04 | 2021-08-18 | クリティテック・インコーポレイテッド | 捕集装置および使用法 |
JP6264500B2 (ja) * | 2015-10-02 | 2018-01-24 | 株式会社島津製作所 | サンプル捕集装置及び超臨界流体装置並びにサンプル捕集方法 |
CN105194964A (zh) * | 2015-10-20 | 2015-12-30 | 秦皇岛首创思泰意达环保科技有限公司 | 一种气体中污染物洗涤和热传质的方法及装置 |
CN109477818A (zh) * | 2016-08-03 | 2019-03-15 | 株式会社岛津制作所 | 流体处理装置以及处理液回收方法 |
US11015142B1 (en) * | 2016-10-20 | 2021-05-25 | Unified Science, LLC | Extraction system and methods for preparing a botanical oil |
CN108251641A (zh) * | 2016-12-18 | 2018-07-06 | 吴彬 | 一种稀土氧化物萃取设备 |
EP3398669B1 (en) * | 2017-05-03 | 2021-02-17 | Vaisala, OYJ | Method for preventing gas bubbles in oil flow to enter a high-voltage device. |
JP6852796B2 (ja) * | 2017-09-15 | 2021-03-31 | 株式会社島津製作所 | 超臨界流体装置 |
GB2567233A (en) * | 2017-10-09 | 2019-04-10 | Linde Ag | Apparatus and method for controlling a near-critical fluid |
CN109364524A (zh) * | 2018-11-23 | 2019-02-22 | 宝鸡市辰光生物科技有限公司 | 一种液-液萃取分离装置及分离方法 |
US20200200716A1 (en) * | 2018-12-20 | 2020-06-25 | Waters Technologies Corporation | System and method for extracting co2 from a mobile phase |
US11149723B2 (en) * | 2019-12-31 | 2021-10-19 | Psg California Llc | Diaphragm pump leak detection |
CN111420470A (zh) * | 2020-05-12 | 2020-07-17 | 广州松和环保科技有限公司 | 一种基于湿法脱硫后的除尘除雾装置 |
Family Cites Families (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1817048A (en) * | 1928-12-31 | 1931-08-04 | Albert P Hunt | Dehydrating apparatus |
US2461342A (en) * | 1947-09-17 | 1949-02-08 | Jr Joseph W Obreiter | Removal of liquid refrigerant from the supply line to a compressor |
US2958189A (en) * | 1955-05-31 | 1960-11-01 | Phillips Petroleum Co | Method and apparatus for providing improved combustion in jet engines |
BE624585A (ja) * | 1961-11-22 | |||
DE1493190C3 (de) * | 1963-04-16 | 1980-10-16 | Studiengesellschaft Kohle Mbh, 4330 Muelheim | Verfahren zur Trennung von Stoffgemischen |
US3224173A (en) * | 1964-12-31 | 1965-12-21 | Nasa | Liquid-gas separation system |
FR2586938B1 (fr) * | 1985-09-06 | 1989-10-20 | Commissariat Energie Atomique | Procede et dispositif pour l'extraction de constituants par un fluide supercritique |
US5339844A (en) * | 1992-08-10 | 1994-08-23 | Hughes Aircraft Company | Low cost equipment for cleaning using liquefiable gases |
US5355901A (en) * | 1992-10-27 | 1994-10-18 | Autoclave Engineers, Ltd. | Apparatus for supercritical cleaning |
EP0724901B1 (en) * | 1995-02-02 | 2002-09-25 | ISCO, Inc. | Apparatus and method for supercritical fluid extraction or supercritical fluid chromatography |
FR2754464B1 (fr) * | 1996-10-14 | 1998-10-30 | Commissariat Energie Atomique | Procede et installation d'extraction de composes organiques et/ou inorganiques du bois par un fluide supercritique |
US5993747A (en) * | 1997-06-25 | 1999-11-30 | Ferro Corporation | Mixing system for processes using supercritical fluids |
AU737746B2 (en) * | 1998-02-28 | 2001-08-30 | Air-Maze Corporation | Conically shaped air-oil separator |
GB9911336D0 (en) * | 1999-05-15 | 1999-07-14 | Graseby Dynamics Ltd | Separation and collection of analyte materials |
US6685828B2 (en) | 1999-09-16 | 2004-02-03 | Berger Instruments, Inc. | Automated sample collection in supercritical fluid chromatography |
US6413428B1 (en) | 1999-09-16 | 2002-07-02 | Berger Instruments, Inc. | Apparatus and method for preparative supercritical fluid chromatography |
US6632353B2 (en) | 2000-06-26 | 2003-10-14 | Berger Instruments, Inc. | Rapid sample collection in supercritical fluid chromatography |
US6558540B2 (en) * | 2000-06-26 | 2003-05-06 | Berger Instruments, Inc. | Exhaust gas collection system for supercritical fluid chromatography |
CN1216493C (zh) * | 2000-07-21 | 2005-08-24 | 皇家菲利浦电子有限公司 | 确定用户简档的方法和系统 |
US6485534B2 (en) * | 2000-12-20 | 2002-11-26 | Axcellis Technologies, Inc. | Contaminant collector trap for ion implanter |
US6960242B2 (en) * | 2002-10-02 | 2005-11-01 | The Boc Group, Inc. | CO2 recovery process for supercritical extraction |
US6735978B1 (en) * | 2003-02-11 | 2004-05-18 | Advanced Technology Materials, Inc. | Treatment of supercritical fluid utilized in semiconductor manufacturing applications |
JP2006136838A (ja) * | 2004-11-15 | 2006-06-01 | Jasco Corp | 捕集物採取用ノズル |
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2006
- 2006-07-17 US US11/487,581 patent/US7964029B2/en active Active
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