JP5650331B2 - 鏡状表面を備えて良好な磁気的性能を有する粒配向珪素鋼を製造するためのアニール分離剤 - Google Patents
鏡状表面を備えて良好な磁気的性能を有する粒配向珪素鋼を製造するためのアニール分離剤 Download PDFInfo
- Publication number
- JP5650331B2 JP5650331B2 JP2013535244A JP2013535244A JP5650331B2 JP 5650331 B2 JP5650331 B2 JP 5650331B2 JP 2013535244 A JP2013535244 A JP 2013535244A JP 2013535244 A JP2013535244 A JP 2013535244A JP 5650331 B2 JP5650331 B2 JP 5650331B2
- Authority
- JP
- Japan
- Prior art keywords
- silicon steel
- annealing separator
- oriented silicon
- steel
- magnetic performance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
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- 238000000137 annealing Methods 0.000 title claims description 32
- 229910000976 Electrical steel Inorganic materials 0.000 title claims description 23
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 12
- 229910000287 alkaline earth metal oxide Inorganic materials 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 5
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 4
- 229910001514 alkali metal chloride Inorganic materials 0.000 claims description 4
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 4
- FGDZQCVHDSGLHJ-UHFFFAOYSA-M rubidium chloride Chemical compound [Cl-].[Rb+] FGDZQCVHDSGLHJ-UHFFFAOYSA-M 0.000 claims description 4
- 229910001617 alkaline earth metal chloride Inorganic materials 0.000 claims description 3
- 239000011780 sodium chloride Substances 0.000 claims description 2
- 229910000831 Steel Inorganic materials 0.000 description 32
- 239000010959 steel Substances 0.000 description 32
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 16
- 239000003795 chemical substances by application Substances 0.000 description 12
- 239000011521 glass Substances 0.000 description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 11
- 238000005261 decarburization Methods 0.000 description 10
- 238000000034 method Methods 0.000 description 10
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 8
- 239000000395 magnesium oxide Substances 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- 239000000047 product Substances 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 5
- 229910004298 SiO 2 Inorganic materials 0.000 description 5
- 238000001953 recrystallisation Methods 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 229910004283 SiO 4 Inorganic materials 0.000 description 4
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 description 4
- 239000000391 magnesium silicate Substances 0.000 description 4
- 229910052919 magnesium silicate Inorganic materials 0.000 description 4
- 235000019792 magnesium silicate Nutrition 0.000 description 4
- 230000003287 optical effect Effects 0.000 description 4
- 239000012298 atmosphere Substances 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 238000005554 pickling Methods 0.000 description 3
- 238000004080 punching Methods 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 230000001680 brushing effect Effects 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 230000005381 magnetic domain Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 230000001681 protective effect Effects 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 101100496858 Mus musculus Colec12 gene Proteins 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 238000003723 Smelting Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000005097 cold rolling Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000005098 hot rolling Methods 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 238000010406 interfacial reaction Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000005304 joining Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000005121 nitriding Methods 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 230000035882 stress Effects 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/68—Temporary coatings or embedding materials applied before or during heat treatment
- C21D1/70—Temporary coatings or embedding materials applied before or during heat treatment while heating or quenching
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/26—Methods of annealing
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D1/00—General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
- C21D1/68—Temporary coatings or embedding materials applied before or during heat treatment
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D3/00—Diffusion processes for extraction of non-metals; Furnaces therefor
- C21D3/02—Extraction of non-metals
- C21D3/04—Decarburising
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D8/00—Modifying the physical properties by deformation combined with, or followed by, heat treatment
- C21D8/12—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
- C21D9/46—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for sheet metals
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/06—Ferrous alloys, e.g. steel alloys containing aluminium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/16—Ferrous alloys, e.g. steel alloys containing copper
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
- H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
- H01F1/12—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials
- H01F1/14—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys
- H01F1/16—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of soft-magnetic materials metals or alloys in the form of sheets
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Organic Chemistry (AREA)
- Metallurgy (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Thermal Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Electromagnetism (AREA)
- Dispersion Chemistry (AREA)
- Power Engineering (AREA)
- Manufacturing Of Steel Electrode Plates (AREA)
- Chemical Treatment Of Metals (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2010105180375A CN102453793B (zh) | 2010-10-25 | 2010-10-25 | 用于具有优良磁性能的镜面取向硅钢制备的退火隔离剂 |
CN201010518037.5 | 2010-10-25 | ||
PCT/CN2011/072771 WO2012055214A1 (zh) | 2010-10-25 | 2011-04-14 | 用于具有优良磁性能的镜面取向硅钢制备的退火隔离剂 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2013545892A JP2013545892A (ja) | 2013-12-26 |
JP5650331B2 true JP5650331B2 (ja) | 2015-01-07 |
Family
ID=45993115
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2013535244A Active JP5650331B2 (ja) | 2010-10-25 | 2011-04-14 | 鏡状表面を備えて良好な磁気的性能を有する粒配向珪素鋼を製造するためのアニール分離剤 |
Country Status (8)
Country | Link |
---|---|
US (1) | US20130292005A1 (zh) |
EP (1) | EP2634270B1 (zh) |
JP (1) | JP5650331B2 (zh) |
KR (1) | KR20130081297A (zh) |
CN (1) | CN102453793B (zh) |
MX (1) | MX352637B (zh) |
RU (1) | RU2552791C2 (zh) |
WO (1) | WO2012055214A1 (zh) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104928452B (zh) * | 2015-05-15 | 2018-03-20 | 武汉钢铁有限公司 | 一种能防止取向硅钢二次再结晶退火边裂的涂料 |
CN109306198A (zh) * | 2018-08-22 | 2019-02-05 | 武汉钢铁有限公司 | 用于改善高磁感取向硅钢硅酸镁底层质量的涂液及其制备方法 |
RU2771130C1 (ru) * | 2019-01-16 | 2022-04-26 | Ниппон Стил Корпорейшн | Способ производства листа электротехнической стали с ориентированной зеренной структурой |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SU413200A1 (zh) * | 1971-06-29 | 1974-01-30 | ||
DE3875676T2 (de) * | 1987-08-31 | 1993-03-18 | Nippon Steel Corp | Verfahren zur herstellung von kornorientierten stahlblechen mit metallglanz und ausgezeichneter stanzbarkeit. |
EP0416420B1 (en) * | 1989-09-08 | 1994-12-14 | Armco Inc. | Magnesium oxide coating for electrical steels and the method of coating |
JP2674917B2 (ja) * | 1991-12-06 | 1997-11-12 | 新日本製鐵株式会社 | フォルステライト被膜のない高磁束密度方向性珪素鋼板の製造方法 |
JP2706040B2 (ja) * | 1993-12-21 | 1998-01-28 | 新日本製鐵株式会社 | 鏡面方向性珪素鋼板の製造方法 |
DE4409691A1 (de) * | 1994-03-22 | 1995-09-28 | Ebg Elektromagnet Werkstoffe | Verfahren zur Herstellung von Elektroblechen mit einem Glasüberzug |
JP3412959B2 (ja) * | 1994-04-22 | 2003-06-03 | 新日本製鐵株式会社 | 鉄損の低い鏡面方向性珪素鋼板の製造方法 |
US5685920A (en) * | 1994-05-13 | 1997-11-11 | Nippon Steel Corporation | Annealing separator having excellent reactivity for grain-oriented electrical steel sheet and method of use the same |
JPH08134542A (ja) * | 1994-11-08 | 1996-05-28 | Sumitomo Metal Ind Ltd | 打抜き性に優れた方向性電磁鋼板の製造方法 |
JP4116702B2 (ja) * | 1998-07-21 | 2008-07-09 | 新日本製鐵株式会社 | 方向性電磁鋼板の製造方法 |
KR100542618B1 (ko) * | 2001-04-23 | 2006-01-11 | 신닛뽄세이테쯔 카부시키카이샤 | 무기광물질 피막이 없는 일방향성 규소강판의 제조방법 |
JP2003253334A (ja) * | 2002-03-01 | 2003-09-10 | Jfe Steel Kk | 磁気特性および打ち抜き性に優れた方向性電磁鋼板の製造方法 |
JP4569070B2 (ja) * | 2003-03-13 | 2010-10-27 | Jfeスチール株式会社 | 方向性電磁鋼板の仕上焼鈍方法 |
JP2007131880A (ja) * | 2005-11-08 | 2007-05-31 | Jfe Steel Kk | フォルステライト被膜のない方向性電磁鋼板の製造方法 |
-
2010
- 2010-10-25 CN CN2010105180375A patent/CN102453793B/zh active Active
-
2011
- 2011-04-14 WO PCT/CN2011/072771 patent/WO2012055214A1/zh active Application Filing
- 2011-04-14 MX MX2013004592A patent/MX352637B/es active IP Right Grant
- 2011-04-14 RU RU2013127583/02A patent/RU2552791C2/ru active
- 2011-04-14 KR KR1020137012552A patent/KR20130081297A/ko active Pre-grant Review Request
- 2011-04-14 US US13/880,278 patent/US20130292005A1/en not_active Abandoned
- 2011-04-14 EP EP11835488.5A patent/EP2634270B1/en active Active
- 2011-04-14 JP JP2013535244A patent/JP5650331B2/ja active Active
Also Published As
Publication number | Publication date |
---|---|
KR20130081297A (ko) | 2013-07-16 |
US20130292005A1 (en) | 2013-11-07 |
EP2634270A1 (en) | 2013-09-04 |
EP2634270B1 (en) | 2021-06-02 |
CN102453793B (zh) | 2013-09-25 |
MX352637B (es) | 2017-12-01 |
CN102453793A (zh) | 2012-05-16 |
RU2013127583A (ru) | 2014-12-27 |
WO2012055214A1 (zh) | 2012-05-03 |
JP2013545892A (ja) | 2013-12-26 |
RU2552791C2 (ru) | 2015-06-10 |
MX2013004592A (es) | 2013-07-17 |
EP2634270A4 (en) | 2018-01-17 |
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