JP5586686B2 - １，６−ヘキサンジオールの製造方法 - Google Patents

１，６−ヘキサンジオールの製造方法 Download PDF

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Publication number
JP5586686B2
JP5586686B2 JP2012503955A JP2012503955A JP5586686B2 JP 5586686 B2 JP5586686 B2 JP 5586686B2 JP 2012503955 A JP2012503955 A JP 2012503955A JP 2012503955 A JP2012503955 A JP 2012503955A JP 5586686 B2 JP5586686 B2 JP 5586686B2
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Japan
Prior art keywords
acid
hydrogenation
cyclohexanediol
catalyst
esterification
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JP2012503955A
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Japanese (ja)
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JP2012522819A5 (enExample
JP2012522819A (ja
Inventor
ピンコス ロルフ
ブロイニンガー ダニエル
テベン ゲアト−ディーター
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/143—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones
    • C07C29/145—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/147—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof
    • C07C29/149—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
JP2012503955A 2009-04-07 2010-03-29 １，６−ヘキサンジオールの製造方法 Expired - Fee Related JP5586686B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09157511.8 2009-04-07
EP09157511 2009-04-07
PCT/EP2010/054053 WO2010115738A1 (de) 2009-04-07 2010-03-29 Verfahren zur herstellung von 1,6-hexandiol

Publications (3)

Publication Number Publication Date
JP2012522819A JP2012522819A (ja) 2012-09-27
JP2012522819A5 JP2012522819A5 (enExample) 2013-05-16
JP5586686B2 true JP5586686B2 (ja) 2014-09-10

Family

ID=42668286

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2012503955A Expired - Fee Related JP5586686B2 (ja) 2009-04-07 2010-03-29 １，６−ヘキサンジオールの製造方法

Country Status (9)

Country Link
US (1) US8629306B2 (enExample)
EP (1) EP2417088B1 (enExample)
JP (1) JP5586686B2 (enExample)
KR (1) KR20120005018A (enExample)
CN (1) CN102388009B (enExample)
CA (1) CA2755696A1 (enExample)
ES (1) ES2415156T3 (enExample)
SG (1) SG174392A1 (enExample)
WO (1) WO2010115738A1 (enExample)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009047194A1 (de) 2009-11-26 2011-06-01 Basf Se Verfahren zur Herstellung von Kunststoffen mit 1,6-Hexandiol mit einem Aldehydanteil von kleiner 500ppm
DE102009047193A1 (de) 2009-11-26 2011-06-01 Basf Se Verfahren zur Herstellung von Diolen durch Hydrierung eines Carbonsäure enthaltenden Gemisches mittels Kobalt enthaltenden Katalysatoren
WO2013101970A1 (en) 2011-12-30 2013-07-04 E. I. Du Pont De Nemours And Company Production of 5-hydroxymethyl-2-furfural from levoglucosenone
WO2013101968A1 (en) 2011-12-30 2013-07-04 E. I. Du Pont De Nemours And Company Process for the production of hexanediols
EP2797904A4 (en) 2011-12-30 2015-08-05 Du Pont PREPARATION OF TETRAHYDROFURAN-2, 5-DIMETHANOL FROM ISOSORBIDE
BR112014015996A2 (pt) 2011-12-30 2017-06-13 Du Pont processo
US8889912B2 (en) 2011-12-30 2014-11-18 E I Du Pont De Nemours And Company Process for preparing 1,6-hexanediol
US8865940B2 (en) 2011-12-30 2014-10-21 E I Du Pont De Nemours And Company Process for preparing 1,6-hexanediol
US8859826B2 (en) 2012-04-27 2014-10-14 E I Du Pont De Nemours And Company Production of alpha, omega-diols
US8846985B2 (en) 2012-04-27 2014-09-30 E I Du Pont De Nemours And Company Production of alpha, omega-diols
US9018423B2 (en) 2012-04-27 2015-04-28 E I Du Pont De Nemours And Company Production of alpha, omega-diols
CN105727962B (zh) * 2016-02-02 2018-07-31 上海华峰新材料研发科技有限公司 用于己二酸二甲酯制己二醇的催化剂及其制备方法和应用
JP7598083B1 (ja) * 2023-04-13 2024-12-11 Dic株式会社 ヘキサメチレン（メタ）アクリレート組成物、活性エネルギー線硬化型樹脂組成物、硬化物

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1235879B (de) 1964-03-17 1967-03-09 Basf Ag Verfahren zur Herstellung von Alkoholen durch katalytische Hydrierung von Carbonsaeuren
JPS4815314B1 (enExample) * 1969-08-18 1973-05-14
DE2060548C3 (de) 1970-12-09 1979-10-11 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von sehr reinem 1,6-Hexandiol durch Kristallisation
DE2321101C2 (de) 1973-04-26 1982-07-22 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung im wesentlichen trägerfreier Kobaltkatalysatoren
US3933930A (en) * 1975-03-06 1976-01-20 Celanese Corporation Hexanediol from cyclohexane
DE4141199A1 (de) 1991-12-13 1993-06-17 Sued Chemie Ag Chromfreier katalysator fuer die hydrierung von organischen verbindungen, die die carbonylfunktionen enthalten
DE19607954A1 (de) 1996-03-01 1997-09-04 Basf Ag Verfahren zur Herstellung von 1,6-Hexandiol und Caprolacton
KR100465468B1 (ko) * 1996-03-01 2005-02-28 바스프 악티엔게젤샤프트 순도99%이상의1,6-헥산디올의제조방법
MY118128A (en) * 1996-03-01 2004-09-30 Basf Ag The preparation of 1, 6-hexanediol and caprolactone
DE19730939A1 (de) 1997-07-18 1999-01-21 Basf Ag Verfahren zur Hydrierung von Carbonylverbindungen
DE19738464A1 (de) 1997-09-03 1999-03-04 Basf Ag Verwendung von Formkörpern als Katalysator zur Herstellung von Caprolactam
DE10128249A1 (de) * 2001-06-11 2002-12-12 Basf Ag Verfahren zur Entfernung von Ameisensäure aus wässrigen Lösungen
DE10313702A1 (de) 2003-03-27 2004-10-07 Basf Ag Katalysator und Verfahren zur Hydrierung von Carbonylverbindungen
DE102004033557A1 (de) 2004-07-09 2006-02-16 Basf Ag Verfahren zur Herstellung von 1,6-Hexandiol in einer Reinheit von über 99,5%
DE102004054047A1 (de) * 2004-11-05 2006-05-11 Basf Ag Verfahren zur Herstellung von 1,6-Hexandiol
KR20100020036A (ko) 2007-06-14 2010-02-19 바스프 에스이 ε-카프로락톤의 제법
US8247580B2 (en) 2007-11-05 2012-08-21 Basf Se Process for preparing ε-caprolactone
EP2225220B1 (de) 2007-12-21 2013-05-22 Basf Se Verfahren zur Herstellung von epsilon-Caprolacton
JP2011512339A (ja) 2008-02-15 2011-04-21 ビーエーエスエフ ソシエタス・ヨーロピア ６−ヒドロキシカプロン酸エステルの製造方法
KR20120004513A (ko) * 2009-04-07 2012-01-12 바스프 에스이 1,6-헥산디올 및 카프로락톤을 제조하기 위한 방법
DE102009047194A1 (de) 2009-11-26 2011-06-01 Basf Se Verfahren zur Herstellung von Kunststoffen mit 1,6-Hexandiol mit einem Aldehydanteil von kleiner 500ppm
DE102009047193A1 (de) 2009-11-26 2011-06-01 Basf Se Verfahren zur Herstellung von Diolen durch Hydrierung eines Carbonsäure enthaltenden Gemisches mittels Kobalt enthaltenden Katalysatoren

Also Published As

Publication number Publication date
ES2415156T3 (es) 2013-07-24
EP2417088B1 (de) 2013-05-29
CA2755696A1 (en) 2010-10-14
SG174392A1 (en) 2011-11-28
US20120022298A1 (en) 2012-01-26
CN102388009B (zh) 2014-11-05
KR20120005018A (ko) 2012-01-13
JP2012522819A (ja) 2012-09-27
CN102388009A (zh) 2012-03-21
EP2417088A1 (de) 2012-02-15
US8629306B2 (en) 2014-01-14
WO2010115738A1 (de) 2010-10-14

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