JP5558830B2 - 硫化水素を製造するための反応器および方法 - Google Patents
硫化水素を製造するための反応器および方法 Download PDFInfo
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- JP5558830B2 JP5558830B2 JP2009545890A JP2009545890A JP5558830B2 JP 5558830 B2 JP5558830 B2 JP 5558830B2 JP 2009545890 A JP2009545890 A JP 2009545890A JP 2009545890 A JP2009545890 A JP 2009545890A JP 5558830 B2 JP5558830 B2 JP 5558830B2
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- Prior art keywords
- reactor
- hydrogen
- sulfur
- distributor
- distribution plate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/16—Hydrogen sulfides
- C01B17/161—Preparation from elemental sulfur
- C01B17/162—Preparation from elemental sulfur from elemental sulfur and hydrogen
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
- B01J10/005—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out at high temperatures in the presence of a molten material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2415—Tubular reactors
- B01J19/242—Tubular reactors in series
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
- B01J8/065—Feeding reactive fluids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
- B01J8/067—Heating or cooling the reactor
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Hydrogen, Water And Hydrids (AREA)
Description
Claims (11)
- ガス状の水素を少なくとも反応器の下部中に含まれている硫黄溶融液(9)中に分配するための分配装置(15)を含む、H2Sを水素および硫黄から連続的に製造するための反応器(1)において、
分配装置(15)が硫黄溶融液(9)中に配置されており、縁部範囲(18)を有する下向きに延在する縁部(17)を備えた、反応器(1)中に配置された分配板(16)を有し、この場合水素は、分配板(16)の下方で形成される水素気泡から縁部範囲(18)を介して硫黄溶融液(9)中に分配可能であり、
反応器(1)が、反応器(1)中へのガス状の水素のための供給装置(11)を有し、該供給装置(11)は、反応器(1)中で垂直に配置された開口管(13)を備え、この管を通じて、分配板(16)の下方で水素気泡を形成し、ガス状の水素が分配板(16)の下方で硫黄溶融液中に導入可能であることを特徴とする、H2Sを水素および硫黄から連続的に製造するための反応器。 - 分配板(16)が通過開口(19)を有し、この通過開口を通じて水素は水素気泡から分配板(16)を介して硫黄溶融液(9)中に分配可能である、請求項1記載の反応器(1)。
- 分配板(16)の通過開口(19)の全開口面積が分配板(16)の面積に対して0.001〜5%である、請求項2記載の反応器(1)。
- 0.2〜3cmの直径を有する分配板(16)の円形の通過開口(19)または0.2〜3cmのスリット幅を有する分配板(16)のスリット状の通過開口を有する、請求項2または3記載の反応器(1)。
- 下向きに延在する縁部(17)が鋸刃状縁部範囲(18)を有し、この縁部範囲を介して水素が水素気泡から縁部(17)と反応器(1)の反応器ジャケット(25)との間の間隙(20)を通じて硫黄溶融液中に導入可能である、請求項1から4までのいずれか1項に記載の反応器(1)。
- 反応器(1)が少なくとも1つの接触管(21)を備え、この接触管中でH2Sへのガス状の硫黄と水素との反応が行なわれ、この場合少なくとも1つの接触管(21)は、硫黄溶融液(9)と部分的に接触している、請求項1から5までのいずれか1項に記載の反応器(1)。
- 少なくとも1つの接触管(21)が分配装置(15)の分配板(16)と結合されている、請求項6記載の反応器(1)。
- 少なくとも反応器の下部中に含まれている硫黄溶融液中へのガス状水素の導入を含む、H2Sを水素および硫黄から連続的に製造する方法において、
ガス状の水素を、硫黄溶融液中に配置された、分配板(16)の下方で水素気泡を形成させるために下向きに延在する縁部(17)を有する、反応器(1)中に配置された分配板(16)を備えた分配装置(15)を介して硫黄溶融液中に分配し、この場合水素は、水素気泡から分配装置(15)を通じて硫黄溶融液(9)中に分配され、
ここで、水素は、反応器(1)中で垂直方向に配置された、分配装置(15)の下方にある、水素気泡に向かって突出する開口管(13)を介して反応器(1)に供給されることを特徴とする、H2Sを水素および硫黄から連続的に製造する方法。 - ガス状の水素を水素気泡から分配板(16)の下方で分配装置(15)の下向きに延在する縁部(17)を介して縁部(17)と反応器(1)の反応器ジャケット(25)との間の間隙(20)を通じて硫黄溶融液(9)中に分配する、請求項8記載の方法。
- ガス状の水素を、水素気泡から分配板(16)の下方で下向きに延在する縁部(17)の鋸刃状縁部範囲(18)を介して分配する、請求項8または9記載の方法。
- ガス状の水素を水素気泡から分配板(16)の下方で分配板(16)中に設けられた通過開口(19)を通じて分配板(16)の上方に存在する硫黄溶融液(9)中に分配する、請求項8から10までのいずれか1項に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP07100588 | 2007-01-16 | ||
EP07100588.8 | 2007-01-16 | ||
PCT/EP2008/050231 WO2008087086A1 (de) | 2007-01-16 | 2008-01-10 | Reaktor und verfahren zur herstellung von schwefelwasserstoff |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2010515657A JP2010515657A (ja) | 2010-05-13 |
JP5558830B2 true JP5558830B2 (ja) | 2014-07-23 |
Family
ID=39429990
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2009545890A Expired - Fee Related JP5558830B2 (ja) | 2007-01-16 | 2008-01-10 | 硫化水素を製造するための反応器および方法 |
Country Status (10)
Country | Link |
---|---|
US (2) | US7871594B2 (ja) |
EP (1) | EP2125611B1 (ja) |
JP (1) | JP5558830B2 (ja) |
CN (1) | CN101610976B (ja) |
CA (1) | CA2674276C (ja) |
CL (1) | CL2008000131A1 (ja) |
ES (1) | ES2612956T3 (ja) |
PE (2) | PE20121273A1 (ja) |
PL (1) | PL2125611T3 (ja) |
WO (1) | WO2008087086A1 (ja) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101610976B (zh) * | 2007-01-16 | 2012-12-05 | 巴斯夫欧洲公司 | 生产硫化氢的反应器和方法 |
US20110259552A1 (en) * | 2008-09-05 | 2011-10-27 | Flagsol Gmbh | Use of modified, low-viscosity sulfur as heat transfer and heat storage fluid |
MX2012007394A (es) | 2010-01-05 | 2012-07-23 | Basf Se | Fluidos de transferencia de calor y fluidos de almacenamiento de calor para temperaturas extremadamente altas basados en polisulfuros. |
WO2013027431A1 (ja) * | 2011-08-23 | 2013-02-28 | 日揮株式会社 | 硫化水素合成反応器、硫化水素製造装置、硫化水素ナトリウム製造装置、及びそれらの方法 |
CN105169936A (zh) * | 2015-09-30 | 2015-12-23 | 苏州韵蓝环保科技有限公司 | 一种气液洗涤塔 |
CA3020740A1 (en) | 2016-05-31 | 2017-12-07 | Novus International Inc. | Process for producing methyl mercaptan from dimethyl sulfide |
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-
2008
- 2008-01-10 CN CN2008800023970A patent/CN101610976B/zh not_active Expired - Fee Related
- 2008-01-10 US US12/523,227 patent/US7871594B2/en not_active Expired - Fee Related
- 2008-01-10 PL PL08701382T patent/PL2125611T3/pl unknown
- 2008-01-10 JP JP2009545890A patent/JP5558830B2/ja not_active Expired - Fee Related
- 2008-01-10 EP EP08701382.7A patent/EP2125611B1/de not_active Not-in-force
- 2008-01-10 ES ES08701382.7T patent/ES2612956T3/es active Active
- 2008-01-10 CA CA2674276A patent/CA2674276C/en not_active Expired - Fee Related
- 2008-01-10 WO PCT/EP2008/050231 patent/WO2008087086A1/de active Application Filing
- 2008-01-16 PE PE2012000176A patent/PE20121273A1/es not_active Application Discontinuation
- 2008-01-16 CL CL2008000131A patent/CL2008000131A1/es unknown
- 2008-01-16 PE PE2008000143A patent/PE20081328A1/es not_active Application Discontinuation
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- 2010-12-09 US US12/963,827 patent/US8580208B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP2125611A1 (de) | 2009-12-02 |
PE20081328A1 (es) | 2008-11-12 |
CL2008000131A1 (es) | 2009-01-23 |
CN101610976B (zh) | 2012-12-05 |
CA2674276C (en) | 2016-07-19 |
US8580208B2 (en) | 2013-11-12 |
US20110081278A1 (en) | 2011-04-07 |
ES2612956T3 (es) | 2017-05-19 |
CA2674276A1 (en) | 2008-07-24 |
US20100015036A1 (en) | 2010-01-21 |
PE20121273A1 (es) | 2012-10-22 |
PL2125611T3 (pl) | 2017-04-28 |
US7871594B2 (en) | 2011-01-18 |
WO2008087086A1 (de) | 2008-07-24 |
CN101610976A (zh) | 2009-12-23 |
JP2010515657A (ja) | 2010-05-13 |
EP2125611B1 (de) | 2016-11-02 |
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