JP5527860B2 - ステンレスの不動態化方法 - Google Patents
ステンレスの不動態化方法 Download PDFInfo
- Publication number
- JP5527860B2 JP5527860B2 JP2012504338A JP2012504338A JP5527860B2 JP 5527860 B2 JP5527860 B2 JP 5527860B2 JP 2012504338 A JP2012504338 A JP 2012504338A JP 2012504338 A JP2012504338 A JP 2012504338A JP 5527860 B2 JP5527860 B2 JP 5527860B2
- Authority
- JP
- Japan
- Prior art keywords
- treatment
- stainless steel
- nitric acid
- acid
- molybdenum
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229910001220 stainless steel Inorganic materials 0.000 title claims description 33
- 239000010935 stainless steel Substances 0.000 title claims description 32
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 31
- 229910017604 nitric acid Inorganic materials 0.000 claims description 31
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 24
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 20
- 235000015393 sodium molybdate Nutrition 0.000 claims description 14
- 239000011684 sodium molybdate Substances 0.000 claims description 14
- TVXXNOYZHKPKGW-UHFFFAOYSA-N sodium molybdate (anhydrous) Chemical compound [Na+].[Na+].[O-][Mo]([O-])(=O)=O TVXXNOYZHKPKGW-UHFFFAOYSA-N 0.000 claims description 14
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 4
- 238000005498 polishing Methods 0.000 claims description 4
- 238000005260 corrosion Methods 0.000 description 25
- 230000007797 corrosion Effects 0.000 description 25
- 239000000243 solution Substances 0.000 description 22
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 20
- 229910052750 molybdenum Inorganic materials 0.000 description 20
- 239000011733 molybdenum Substances 0.000 description 20
- 238000002474 experimental method Methods 0.000 description 18
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 14
- 238000010586 diagram Methods 0.000 description 10
- 238000005868 electrolysis reaction Methods 0.000 description 10
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 8
- 229910052804 chromium Inorganic materials 0.000 description 8
- 239000011651 chromium Substances 0.000 description 8
- VLAPMBHFAWRUQP-UHFFFAOYSA-L molybdic acid Chemical compound O[Mo](O)(=O)=O VLAPMBHFAWRUQP-UHFFFAOYSA-L 0.000 description 8
- 238000012360 testing method Methods 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 7
- 229910052742 iron Inorganic materials 0.000 description 7
- 229910052751 metal Inorganic materials 0.000 description 7
- 239000002184 metal Substances 0.000 description 7
- 239000005078 molybdenum compound Substances 0.000 description 6
- 150000002752 molybdenum compounds Chemical class 0.000 description 6
- 238000004544 sputter deposition Methods 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 5
- 238000002161 passivation Methods 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 description 3
- AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 description 3
- 239000011259 mixed solution Substances 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000004070 electrodeposition Methods 0.000 description 2
- 238000000921 elemental analysis Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 230000001954 sterilising effect Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- RMXTYBQNQCQHEU-UHFFFAOYSA-N ac1lawpn Chemical compound [Cr]#[Cr] RMXTYBQNQCQHEU-UHFFFAOYSA-N 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- -1 chlorine ions Chemical class 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000002845 discoloration Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000002659 electrodeposit Substances 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- MEFBJEMVZONFCJ-UHFFFAOYSA-N molybdate Chemical compound [O-][Mo]([O-])(=O)=O MEFBJEMVZONFCJ-UHFFFAOYSA-N 0.000 description 1
- 150000002751 molybdenum Chemical class 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25F—PROCESSES FOR THE ELECTROLYTIC REMOVAL OF MATERIALS FROM OBJECTS; APPARATUS THEREFOR
- C25F3/00—Electrolytic etching or polishing
- C25F3/16—Polishing
- C25F3/22—Polishing of heavy metals
- C25F3/24—Polishing of heavy metals of iron or steel
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/40—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing molybdates, tungstates or vanadates
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Electrochemistry (AREA)
- Chemical Treatment Of Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012504338A JP5527860B2 (ja) | 2010-03-12 | 2011-03-10 | ステンレスの不動態化方法 |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2010056706 | 2010-03-12 | ||
| JP2010056706 | 2010-03-12 | ||
| PCT/JP2011/001400 WO2011111391A1 (ja) | 2010-03-12 | 2011-03-10 | ステンレスの不動態化方法 |
| JP2012504338A JP5527860B2 (ja) | 2010-03-12 | 2011-03-10 | ステンレスの不動態化方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPWO2011111391A1 JPWO2011111391A1 (ja) | 2013-06-27 |
| JP5527860B2 true JP5527860B2 (ja) | 2014-06-25 |
Family
ID=44563222
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012504338A Active JP5527860B2 (ja) | 2010-03-12 | 2011-03-10 | ステンレスの不動態化方法 |
Country Status (3)
| Country | Link |
|---|---|
| JP (1) | JP5527860B2 (zh) |
| CN (1) | CN102762769B (zh) |
| WO (1) | WO2011111391A1 (zh) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPWO2014103703A1 (ja) * | 2012-12-28 | 2017-01-12 | マルイ鍍金工業株式会社 | ステンレス鋼の不動態化方法 |
| JP6196064B2 (ja) * | 2013-04-25 | 2017-09-13 | 株式会社Ihi | ステンレス鋼部品の不動態化処理方法 |
| JP6505498B2 (ja) * | 2014-05-21 | 2019-04-24 | マルイ鍍金工業株式会社 | ステンレス鋼の不動態化方法 |
| DE102014111779A1 (de) * | 2014-08-18 | 2016-02-18 | Iva Industrieöfen Gmbh | Verfahren zur Herstellung einer Retorte für einen Nitrierofen sowie Retorte |
| CN105543937B (zh) * | 2015-12-23 | 2018-01-16 | 江门市安诺特炊具制造有限公司 | 一种不锈钢炊具电解钝化液及其钝化处理工艺 |
| CN106435585B (zh) * | 2016-08-16 | 2019-07-12 | 深圳市诚达科技股份有限公司 | 一种不锈钢件的表面cts抗腐蚀处理方法 |
| CN106086996B (zh) * | 2016-08-24 | 2017-12-26 | 厦门双瑞船舶涂料有限公司 | 一种修复已生锈不锈钢钝化状态的复合表面处理方法 |
| CN106835241A (zh) * | 2016-12-26 | 2017-06-13 | 安徽宝恒新材料科技有限公司 | 一种耐磨型不锈钢的制备方法 |
| JP7108291B2 (ja) * | 2018-06-25 | 2022-07-28 | マルイ鍍金工業株式会社 | ステンレスの表面処理方法 |
| CN114107970B (zh) * | 2021-11-29 | 2024-04-12 | 深圳市诚达科技股份有限公司 | 一种不锈钢表面抗腐蚀膜层的常温制备方法 |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09250000A (ja) * | 1996-03-14 | 1997-09-22 | Okuno Chem Ind Co Ltd | ステンレス鋼電解研摩液用添加剤およびステンレス鋼電解研摩液 |
| JP2002081451A (ja) * | 2000-05-31 | 2002-03-22 | Nsk Ltd | 転がり支持装置 |
| JP2005089804A (ja) * | 2003-09-16 | 2005-04-07 | Kyodo Yushi Co Ltd | 水素含有環境下で使用されるトライボロジー金属部材及び潤滑剤 |
| JP2007516772A (ja) * | 2003-12-30 | 2007-06-28 | ボストン サイエンティフィック リミテッド | 金属合金の洗浄および研磨方法、ならびにそれにより洗浄または研磨された製品 |
| JP2008091225A (ja) * | 2006-10-03 | 2008-04-17 | Nisshin Steel Co Ltd | 固体高分子型燃料電池用セパレータ及びその製造方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5847477B2 (ja) * | 1980-07-24 | 1983-10-22 | 日本金属株式会社 | ステンレス鋼の表面処理方法 |
| JPH03153247A (ja) * | 1989-11-10 | 1991-07-01 | Fuji Photo Film Co Ltd | 感光材料処理装置 |
| JP4777098B2 (ja) * | 2006-03-07 | 2011-09-21 | 日本ペイント株式会社 | 新規な複合化成皮膜を含む複層塗膜 |
-
2011
- 2011-03-10 WO PCT/JP2011/001400 patent/WO2011111391A1/ja active Application Filing
- 2011-03-10 CN CN201180010016.5A patent/CN102762769B/zh active Active
- 2011-03-10 JP JP2012504338A patent/JP5527860B2/ja active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09250000A (ja) * | 1996-03-14 | 1997-09-22 | Okuno Chem Ind Co Ltd | ステンレス鋼電解研摩液用添加剤およびステンレス鋼電解研摩液 |
| JP2002081451A (ja) * | 2000-05-31 | 2002-03-22 | Nsk Ltd | 転がり支持装置 |
| JP2005089804A (ja) * | 2003-09-16 | 2005-04-07 | Kyodo Yushi Co Ltd | 水素含有環境下で使用されるトライボロジー金属部材及び潤滑剤 |
| JP2007516772A (ja) * | 2003-12-30 | 2007-06-28 | ボストン サイエンティフィック リミテッド | 金属合金の洗浄および研磨方法、ならびにそれにより洗浄または研磨された製品 |
| JP2008091225A (ja) * | 2006-10-03 | 2008-04-17 | Nisshin Steel Co Ltd | 固体高分子型燃料電池用セパレータ及びその製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPWO2011111391A1 (ja) | 2013-06-27 |
| CN102762769A (zh) | 2012-10-31 |
| CN102762769B (zh) | 2014-10-29 |
| WO2011111391A1 (ja) | 2011-09-15 |
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