JP5250986B2 - プリプレグおよび繊維強化複合材料 - Google Patents
プリプレグおよび繊維強化複合材料 Download PDFInfo
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- JP5250986B2 JP5250986B2 JP2007072399A JP2007072399A JP5250986B2 JP 5250986 B2 JP5250986 B2 JP 5250986B2 JP 2007072399 A JP2007072399 A JP 2007072399A JP 2007072399 A JP2007072399 A JP 2007072399A JP 5250986 B2 JP5250986 B2 JP 5250986B2
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- JP
- Japan
- Prior art keywords
- prepreg
- fiber
- polyarylene sulfide
- weight
- resin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000003733 fiber-reinforced composite Substances 0.000 title claims description 30
- 229920000412 polyarylene Polymers 0.000 claims description 55
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims description 50
- 125000004122 cyclic group Chemical group 0.000 claims description 34
- 239000000463 material Substances 0.000 claims description 30
- 239000012783 reinforcing fiber Substances 0.000 claims description 22
- 239000011342 resin composition Substances 0.000 claims description 22
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 8
- 239000004917 carbon fiber Substances 0.000 claims description 8
- 230000000379 polymerizing effect Effects 0.000 claims description 6
- 239000004734 Polyphenylene sulfide Substances 0.000 description 43
- 229920000069 polyphenylene sulfide Polymers 0.000 description 43
- 229920005989 resin Polymers 0.000 description 29
- 239000011347 resin Substances 0.000 description 29
- 238000000034 method Methods 0.000 description 25
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 description 22
- 239000000203 mixture Substances 0.000 description 21
- 239000000835 fiber Substances 0.000 description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 19
- 239000002002 slurry Substances 0.000 description 14
- 238000005470 impregnation Methods 0.000 description 13
- 229920000642 polymer Polymers 0.000 description 12
- 239000000843 powder Substances 0.000 description 12
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 11
- 238000010438 heat treatment Methods 0.000 description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 235000012970 cakes Nutrition 0.000 description 9
- 238000000465 moulding Methods 0.000 description 9
- 239000007787 solid Substances 0.000 description 9
- 238000005452 bending Methods 0.000 description 7
- 239000011521 glass Substances 0.000 description 7
- 239000011159 matrix material Substances 0.000 description 7
- 238000012360 testing method Methods 0.000 description 7
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 6
- 238000006116 polymerization reaction Methods 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 229910052757 nitrogen Inorganic materials 0.000 description 5
- -1 polyethylene Polymers 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 239000000758 substrate Substances 0.000 description 5
- 238000000967 suction filtration Methods 0.000 description 5
- 150000004763 sulfides Chemical class 0.000 description 5
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 239000002612 dispersion medium Substances 0.000 description 4
- 238000003475 lamination Methods 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 4
- 239000002798 polar solvent Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 229920001187 thermosetting polymer Polymers 0.000 description 4
- OCJBOOLMMGQPQU-UHFFFAOYSA-N 1,4-dichlorobenzene Chemical compound ClC1=CC=C(Cl)C=C1 OCJBOOLMMGQPQU-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 229920001400 block copolymer Polymers 0.000 description 3
- 229910001873 dinitrogen Inorganic materials 0.000 description 3
- 239000012943 hotmelt Substances 0.000 description 3
- 229920005604 random copolymer Polymers 0.000 description 3
- 229920005992 thermoplastic resin Polymers 0.000 description 3
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 2
- XWUCFAJNVTZRLE-UHFFFAOYSA-N 7-thiabicyclo[2.2.1]hepta-1,3,5-triene Chemical group C1=C(S2)C=CC2=C1 XWUCFAJNVTZRLE-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 2
- 229920000459 Nitrile rubber Polymers 0.000 description 2
- 239000004952 Polyamide Substances 0.000 description 2
- 239000004698 Polyethylene Substances 0.000 description 2
- 238000000862 absorption spectrum Methods 0.000 description 2
- 229910001508 alkali metal halide Inorganic materials 0.000 description 2
- 229910052977 alkali metal sulfide Inorganic materials 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 150000001491 aromatic compounds Chemical class 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- 239000003822 epoxy resin Substances 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000003365 glass fiber Substances 0.000 description 2
- 238000004128 high performance liquid chromatography Methods 0.000 description 2
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 2
- 238000012844 infrared spectroscopy analysis Methods 0.000 description 2
- 150000002576 ketones Chemical class 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 229920002647 polyamide Polymers 0.000 description 2
- 239000004417 polycarbonate Substances 0.000 description 2
- 229920000515 polycarbonate Polymers 0.000 description 2
- 229920000647 polyepoxide Polymers 0.000 description 2
- 229920000728 polyester Polymers 0.000 description 2
- 229920000573 polyethylene Polymers 0.000 description 2
- HYHCSLBZRBJJCH-UHFFFAOYSA-M sodium hydrosulfide Chemical compound [Na+].[SH-] HYHCSLBZRBJJCH-UHFFFAOYSA-M 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 150000003457 sulfones Chemical class 0.000 description 2
- 150000003505 terpenes Chemical class 0.000 description 2
- 235000007586 terpenes Nutrition 0.000 description 2
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
- 229920001169 thermoplastic Polymers 0.000 description 2
- 239000004416 thermosoftening plastic Substances 0.000 description 2
- 229920006337 unsaturated polyester resin Polymers 0.000 description 2
- 229920001567 vinyl ester resin Polymers 0.000 description 2
- 229920002554 vinyl polymer Polymers 0.000 description 2
- JTPNRXUCIXHOKM-UHFFFAOYSA-N 1-chloronaphthalene Chemical compound C1=CC=C2C(Cl)=CC=CC2=C1 JTPNRXUCIXHOKM-UHFFFAOYSA-N 0.000 description 1
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 1
- 239000004696 Poly ether ether ketone Substances 0.000 description 1
- 239000004962 Polyamide-imide Substances 0.000 description 1
- 239000004695 Polyether sulfone Substances 0.000 description 1
- 239000004697 Polyetherimide Substances 0.000 description 1
- 239000004642 Polyimide Substances 0.000 description 1
- 239000004721 Polyphenylene oxide Substances 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 1
- 238000000944 Soxhlet extraction Methods 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 description 1
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229920006231 aramid fiber Polymers 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000007334 copolymerization reaction Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 150000001923 cyclic compounds Chemical class 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 229940117389 dichlorobenzene Drugs 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 235000021463 dry cake Nutrition 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229920006244 ethylene-ethyl acrylate Polymers 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 239000011256 inorganic filler Substances 0.000 description 1
- 229910003475 inorganic filler Inorganic materials 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 238000010030 laminating Methods 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 238000001840 matrix-assisted laser desorption--ionisation time-of-flight mass spectrometry Methods 0.000 description 1
- 229920006284 nylon film Polymers 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000013001 point bending Methods 0.000 description 1
- 229920001643 poly(ether ketone) Polymers 0.000 description 1
- 229920002492 poly(sulfone) Polymers 0.000 description 1
- 229920002312 polyamide-imide Polymers 0.000 description 1
- 229920006393 polyether sulfone Polymers 0.000 description 1
- 229920002530 polyetherether ketone Polymers 0.000 description 1
- 229920001601 polyetherimide Polymers 0.000 description 1
- 229920001721 polyimide Polymers 0.000 description 1
- 229920006380 polyphenylene oxide Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920003225 polyurethane elastomer Polymers 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000011403 purification operation Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007660 shear property test Methods 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 239000001632 sodium acetate Substances 0.000 description 1
- 235000017281 sodium acetate Nutrition 0.000 description 1
- 229940048181 sodium sulfide nonahydrate Drugs 0.000 description 1
- WMDLZMCDBSJMTM-UHFFFAOYSA-M sodium;sulfanide;nonahydrate Chemical compound O.O.O.O.O.O.O.O.O.[Na+].[SH-] WMDLZMCDBSJMTM-UHFFFAOYSA-M 0.000 description 1
- 238000010183 spectrum analysis Methods 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 239000003017 thermal stabilizer Substances 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
Landscapes
- Reinforced Plastic Materials (AREA)
Priority Applications (12)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2007072399A JP5250986B2 (ja) | 2007-03-20 | 2007-03-20 | プリプレグおよび繊維強化複合材料 |
| KR1020097021740A KR101438248B1 (ko) | 2007-03-20 | 2008-02-22 | 성형 재료 |
| ES08711788.3T ES2624694T3 (es) | 2007-03-20 | 2008-02-22 | Material de moldeo, preimpregnado, material compuesto reforzado con fibras y proceso para la producción de un material de base de moldeo reforzado con fibras |
| KR1020127034006A KR101449232B1 (ko) | 2007-03-20 | 2008-02-22 | 프리프레그 및 섬유 강화 복합 재료, 및 섬유 강화 성형 기재의 제조 방법 |
| EP16202686.8A EP3156439B1 (en) | 2007-03-20 | 2008-02-22 | Molding material, prepreg, fiber-reinforced composite material, and process for production of fiber-reinforced molding base material |
| EP08711788.3A EP2138530B1 (en) | 2007-03-20 | 2008-02-22 | Molding material, prepreg, fiber-reinforced composite material, and process for production of fiber-reinforced molding base material |
| PCT/JP2008/053014 WO2008114573A1 (ja) | 2007-03-20 | 2008-02-22 | 成形材料、プリプレグおよび繊維強化複合材料、ならびに繊維強化成形基材の製造方法 |
| CN2008800166156A CN101679654B (zh) | 2007-03-20 | 2008-02-22 | 模塑材料，预浸料和纤维增强复合材料，以及生产纤维增强模塑基材的方法 |
| US12/531,621 US7824770B2 (en) | 2007-03-20 | 2008-02-22 | Molding material, prepreg and fiber-reinforced composite material, and method for producing fiber-reinforced molding substrate |
| CN201210171559.1A CN102660118B (zh) | 2007-03-20 | 2008-02-22 | 模塑材料，预浸料和纤维增强复合材料，以及生产纤维增强模塑基材的方法 |
| TW102138006A TWI488889B (zh) | 2007-03-20 | 2008-03-19 | 預浸漬物、纖維強化複合材料及纖維強化複合材料積層體與纖維強化成型基材之製法 |
| TW97109572A TWI417179B (zh) | 2007-03-20 | 2008-03-19 | 成型材料 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2007072399A JP5250986B2 (ja) | 2007-03-20 | 2007-03-20 | プリプレグおよび繊維強化複合材料 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2008231237A JP2008231237A (ja) | 2008-10-02 |
| JP2008231237A5 JP2008231237A5 (enExample) | 2010-04-30 |
| JP5250986B2 true JP5250986B2 (ja) | 2013-07-31 |
Family
ID=39904437
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2007072399A Expired - Fee Related JP5250986B2 (ja) | 2007-03-20 | 2007-03-20 | プリプレグおよび繊維強化複合材料 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP5250986B2 (enExample) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2011162767A (ja) * | 2010-01-14 | 2011-08-25 | Toray Ind Inc | 炭素繊維強化ポリフェニレンスルフィド樹脂組成物、ならびにそれを用いた成形材料および成形品 |
| KR101717165B1 (ko) | 2010-12-13 | 2017-03-16 | 도레이 카부시키가이샤 | 수지 조성물, 그것을 사용한 복합 경화물 및 그 제조방법 |
| ES2552215T3 (es) | 2011-01-14 | 2015-11-26 | Toray Industries, Inc. | Material de moldeo, material preimpregnado, material compuesto reforzado con fibra, laminado de material compuesto reforzado con fibra y proceso para la producción de material de base de moldeo reforzado con fibra |
| CN103608386B (zh) | 2011-06-24 | 2015-09-30 | 东丽株式会社 | 成型材料和使用其的成型方法、成型材料的制造方法以及纤维强化复合材料的制造方法 |
| JP5589973B2 (ja) * | 2011-06-24 | 2014-09-17 | 東レ株式会社 | 成形材料の製造方法 |
| JP5589971B2 (ja) * | 2011-06-24 | 2014-09-17 | 東レ株式会社 | 成形材料 |
| JP5589974B2 (ja) * | 2011-06-24 | 2014-09-17 | 東レ株式会社 | 繊維強化複合材料の製造方法 |
| JP5589972B2 (ja) * | 2011-06-24 | 2014-09-17 | 東レ株式会社 | 成形材料およびそれを用いた成形方法 |
| JP6561507B2 (ja) * | 2014-03-27 | 2019-08-21 | 東レ株式会社 | 成形材料ならびにそれを用いた成形品の製造方法および成形品 |
| FR3079163B1 (fr) | 2018-03-23 | 2021-10-15 | Arkema France | Nappe de materiau fibreux impregne, son procede de fabrication et son utilisation pour la fabrication de pieces composites en trois dimensions |
| FR3079164B1 (fr) | 2018-03-23 | 2021-10-22 | Arkema France | Materiau fibreux impregne de polymere thermoplastique d'epaisseur inferieure ou egale a 100μm et son procede de preparation |
| JPWO2020017288A1 (ja) * | 2018-07-17 | 2021-06-03 | 東レ株式会社 | 繊維強化樹脂基材 |
| JPWO2020017287A1 (ja) * | 2018-07-17 | 2021-06-03 | 東レ株式会社 | 繊維強化樹脂基材 |
| CN116855075B (zh) * | 2023-05-04 | 2024-06-28 | 国材(苏州)新材料科技有限公司 | 一种增加聚苯硫醚使用性能的复合制备方法 |
| WO2025197777A1 (ja) * | 2024-03-19 | 2025-09-25 | 東レ株式会社 | プリプレグ |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0413257A3 (en) * | 1989-08-14 | 1992-06-03 | The Dow Chemical Company | Cyclic poly(aryl ether) oligomers, a process for preparation thereof, and polymerization of cyclic poly (aryl ether) oligomers |
| JPH0539371A (ja) * | 1991-05-29 | 1993-02-19 | Dainippon Ink & Chem Inc | ポリアリーレンスルフイド系樹脂プリプレーグおよびその成形品 |
| JP3216228B2 (ja) * | 1991-08-06 | 2001-10-09 | 東ソー株式会社 | ポリアリーレンスルフィドの製造方法 |
| JP3774959B2 (ja) * | 1996-11-06 | 2006-05-17 | 東レ株式会社 | 成形材料およびその製造方法 |
-
2007
- 2007-03-20 JP JP2007072399A patent/JP5250986B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JP2008231237A (ja) | 2008-10-02 |
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