JP5219372B2 - 高純度液化塩素の製造方法 - Google Patents
高純度液化塩素の製造方法 Download PDFInfo
- Publication number
- JP5219372B2 JP5219372B2 JP2006537657A JP2006537657A JP5219372B2 JP 5219372 B2 JP5219372 B2 JP 5219372B2 JP 2006537657 A JP2006537657 A JP 2006537657A JP 2006537657 A JP2006537657 A JP 2006537657A JP 5219372 B2 JP5219372 B2 JP 5219372B2
- Authority
- JP
- Japan
- Prior art keywords
- chlorine
- photolysis
- purity liquefied
- purity
- oxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000460 chlorine Substances 0.000 title claims description 102
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 title claims description 92
- 229910052801 chlorine Inorganic materials 0.000 title claims description 89
- 238000004519 manufacturing process Methods 0.000 title claims description 28
- OSVXSBDYLRYLIG-UHFFFAOYSA-N dioxidochlorine(.) Chemical group O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 claims description 94
- 238000006303 photolysis reaction Methods 0.000 claims description 60
- 239000004155 Chlorine dioxide Substances 0.000 claims description 47
- 235000019398 chlorine dioxide Nutrition 0.000 claims description 47
- 230000015843 photosynthesis, light reaction Effects 0.000 claims description 46
- 229910001902 chlorine oxide Inorganic materials 0.000 claims description 40
- MAYPHUUCLRDEAZ-UHFFFAOYSA-N chlorine peroxide Chemical compound ClOOCl MAYPHUUCLRDEAZ-UHFFFAOYSA-N 0.000 claims description 35
- 239000012535 impurity Substances 0.000 claims description 33
- 238000000034 method Methods 0.000 claims description 33
- 238000004821 distillation Methods 0.000 claims description 24
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 22
- 239000001301 oxygen Substances 0.000 claims description 22
- 229910052760 oxygen Inorganic materials 0.000 claims description 22
- 239000007789 gas Substances 0.000 claims description 18
- 238000009835 boiling Methods 0.000 claims description 15
- 239000002994 raw material Substances 0.000 claims description 13
- 230000001678 irradiating effect Effects 0.000 claims description 7
- 239000006200 vaporizer Substances 0.000 claims description 4
- 238000007670 refining Methods 0.000 claims description 3
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 claims 2
- NHYCGSASNAIGLD-UHFFFAOYSA-N Chlorine monoxide Chemical class Cl[O] NHYCGSASNAIGLD-UHFFFAOYSA-N 0.000 description 16
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 14
- 238000000354 decomposition reaction Methods 0.000 description 10
- 239000012071 phase Substances 0.000 description 10
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 8
- 238000010521 absorption reaction Methods 0.000 description 8
- XTEGARKTQYYJKE-UHFFFAOYSA-M Chlorate Chemical compound [O-]Cl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-M 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 6
- 239000011521 glass Substances 0.000 description 6
- 239000007791 liquid phase Substances 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 238000005868 electrolysis reaction Methods 0.000 description 4
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 4
- 229910052753 mercury Inorganic materials 0.000 description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000003463 adsorbent Substances 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- -1 chlorine dioxide Chemical compound 0.000 description 3
- 238000011049 filling Methods 0.000 description 3
- 239000011261 inert gas Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 239000011780 sodium chloride Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- BZSXEZOLBIJVQK-UHFFFAOYSA-N 2-methylsulfonylbenzoic acid Chemical compound CS(=O)(=O)C1=CC=CC=C1C(O)=O BZSXEZOLBIJVQK-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000003421 catalytic decomposition reaction Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- RCJVRSBWZCNNQT-UHFFFAOYSA-N dichloridooxygen Chemical compound ClOCl RCJVRSBWZCNNQT-UHFFFAOYSA-N 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 230000031700 light absorption Effects 0.000 description 2
- 229910001507 metal halide Inorganic materials 0.000 description 2
- 150000005309 metal halides Chemical class 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000005033 Fourier transform infrared spectroscopy Methods 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- TVWHTOUAJSGEKT-UHFFFAOYSA-N chlorine trioxide Chemical compound [O]Cl(=O)=O TVWHTOUAJSGEKT-UHFFFAOYSA-N 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000001784 detoxification Methods 0.000 description 1
- SAUMVKNLVQDHMJ-UHFFFAOYSA-N dichlorine trioxide Inorganic materials ClOCl(=O)=O SAUMVKNLVQDHMJ-UHFFFAOYSA-N 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000013307 optical fiber Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 238000002627 tracheal intubation Methods 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/07—Purification ; Separation
- C01B7/075—Purification ; Separation of liquid chlorine
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2006537657A JP5219372B2 (ja) | 2004-09-29 | 2005-08-29 | 高純度液化塩素の製造方法 |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004283475 | 2004-09-29 | ||
| JP2004283475 | 2004-09-29 | ||
| PCT/JP2005/016157 WO2006035571A1 (ja) | 2004-09-29 | 2005-08-29 | 高純度液化塩素の製造方法 |
| JP2006537657A JP5219372B2 (ja) | 2004-09-29 | 2005-08-29 | 高純度液化塩素の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPWO2006035571A1 JPWO2006035571A1 (ja) | 2008-05-15 |
| JP5219372B2 true JP5219372B2 (ja) | 2013-06-26 |
Family
ID=36118723
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006537657A Active JP5219372B2 (ja) | 2004-09-29 | 2005-08-29 | 高純度液化塩素の製造方法 |
Country Status (4)
| Country | Link |
|---|---|
| JP (1) | JP5219372B2 (zh) |
| KR (1) | KR100849656B1 (zh) |
| TW (1) | TWI391326B (zh) |
| WO (1) | WO2006035571A1 (zh) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5544696B2 (ja) * | 2008-09-24 | 2014-07-09 | 東亞合成株式会社 | 液化塩素の製造方法 |
| KR101203490B1 (ko) * | 2011-11-29 | 2012-11-21 | 홍인화학 주식회사 | 고순도 염화수소 제조방법 및 제조 시스템 |
| MY156181A (en) * | 2011-10-11 | 2016-01-15 | Hong In Chemical Co Ltd | Method and system for producing high-purity hydrogen chloride |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5120092A (ja) * | 1974-08-12 | 1976-02-17 | Asahi Denka Kogyo Kk | Gasunoseiseiho |
| JPS5632301A (en) * | 1979-08-13 | 1981-04-01 | Shell Int Research | Method of improving quality of chlorine |
| JPH028683A (ja) * | 1988-02-16 | 1990-01-12 | Mitsui Toatsu Chem Inc | 塩素の分離回収方法 |
| JPH0338218A (ja) * | 1989-06-30 | 1991-02-19 | Daikin Ind Ltd | 悪臭ガス除去装置 |
| US5908532A (en) * | 1996-10-30 | 1999-06-01 | Eka Chemicals, Inc. | Method of converting chlorine dioxide present in a gaseous stream from a pulp bleach plant by irradiation to chlorine |
| JP2002316804A (ja) * | 2001-04-19 | 2002-10-31 | Sumitomo Chem Co Ltd | 塩素精製法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5528195Y2 (zh) | 1974-08-01 | 1980-07-05 | ||
| US5944962A (en) * | 1995-10-03 | 1999-08-31 | Laroche Industries, Inc. | Process for photochlorination |
-
2005
- 2005-08-29 KR KR1020077001846A patent/KR100849656B1/ko active IP Right Grant
- 2005-08-29 WO PCT/JP2005/016157 patent/WO2006035571A1/ja active Application Filing
- 2005-08-29 JP JP2006537657A patent/JP5219372B2/ja active Active
- 2005-09-19 TW TW94132335A patent/TWI391326B/zh active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5120092A (ja) * | 1974-08-12 | 1976-02-17 | Asahi Denka Kogyo Kk | Gasunoseiseiho |
| JPS5632301A (en) * | 1979-08-13 | 1981-04-01 | Shell Int Research | Method of improving quality of chlorine |
| JPH028683A (ja) * | 1988-02-16 | 1990-01-12 | Mitsui Toatsu Chem Inc | 塩素の分離回収方法 |
| JPH0338218A (ja) * | 1989-06-30 | 1991-02-19 | Daikin Ind Ltd | 悪臭ガス除去装置 |
| US5908532A (en) * | 1996-10-30 | 1999-06-01 | Eka Chemicals, Inc. | Method of converting chlorine dioxide present in a gaseous stream from a pulp bleach plant by irradiation to chlorine |
| JP2002316804A (ja) * | 2001-04-19 | 2002-10-31 | Sumitomo Chem Co Ltd | 塩素精製法 |
Also Published As
| Publication number | Publication date |
|---|---|
| TW200621636A (en) | 2006-07-01 |
| WO2006035571A1 (ja) | 2006-04-06 |
| KR20070028586A (ko) | 2007-03-12 |
| KR100849656B1 (ko) | 2008-08-01 |
| JPWO2006035571A1 (ja) | 2008-05-15 |
| TWI391326B (zh) | 2013-04-01 |
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