JP5190194B2 - 精製装置 - Google Patents
精製装置 Download PDFInfo
- Publication number
- JP5190194B2 JP5190194B2 JP2006315110A JP2006315110A JP5190194B2 JP 5190194 B2 JP5190194 B2 JP 5190194B2 JP 2006315110 A JP2006315110 A JP 2006315110A JP 2006315110 A JP2006315110 A JP 2006315110A JP 5190194 B2 JP5190194 B2 JP 5190194B2
- Authority
- JP
- Japan
- Prior art keywords
- purification
- tube
- end portion
- unit
- inner diameter
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000000746 purification Methods 0.000 title claims description 855
- 239000007789 gas Substances 0.000 claims description 50
- 239000000126 substance Substances 0.000 claims description 30
- 238000007670 refining Methods 0.000 claims description 20
- 239000011521 glass Substances 0.000 claims description 16
- 239000010453 quartz Substances 0.000 claims description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 11
- 230000008016 vaporization Effects 0.000 claims description 8
- 239000011261 inert gas Substances 0.000 claims description 5
- 239000013076 target substance Substances 0.000 description 114
- 239000007788 liquid Substances 0.000 description 33
- 239000007787 solid Substances 0.000 description 33
- 239000012535 impurity Substances 0.000 description 22
- 238000000859 sublimation Methods 0.000 description 18
- 230000008022 sublimation Effects 0.000 description 18
- 239000000463 material Substances 0.000 description 14
- 238000002474 experimental method Methods 0.000 description 13
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 12
- 238000011109 contamination Methods 0.000 description 10
- 230000007423 decrease Effects 0.000 description 10
- 238000000034 method Methods 0.000 description 10
- 239000012264 purified product Substances 0.000 description 10
- 238000010438 heat treatment Methods 0.000 description 8
- 239000000203 mixture Substances 0.000 description 7
- 239000011368 organic material Substances 0.000 description 7
- 238000005160 1H NMR spectroscopy Methods 0.000 description 6
- 229910052786 argon Inorganic materials 0.000 description 6
- 239000012159 carrier gas Substances 0.000 description 6
- 238000011084 recovery Methods 0.000 description 6
- VIJYEGDOKCKUOL-UHFFFAOYSA-N 9-phenylcarbazole Chemical compound C1=CC=CC=C1N1C2=CC=CC=C2C2=CC=CC=C21 VIJYEGDOKCKUOL-UHFFFAOYSA-N 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 5
- 238000004821 distillation Methods 0.000 description 5
- 239000000314 lubricant Substances 0.000 description 4
- 230000001681 protective effect Effects 0.000 description 4
- NAWXUBYGYWOOIX-SFHVURJKSA-N (2s)-2-[[4-[2-(2,4-diaminoquinazolin-6-yl)ethyl]benzoyl]amino]-4-methylidenepentanedioic acid Chemical compound C1=CC2=NC(N)=NC(N)=C2C=C1CCC1=CC=C(C(=O)N[C@@H](CC(=C)C(O)=O)C(O)=O)C=C1 NAWXUBYGYWOOIX-SFHVURJKSA-N 0.000 description 3
- 230000003247 decreasing effect Effects 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 150000002894 organic compounds Chemical class 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- 238000009835 boiling Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000011491 glass wool Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- COVCYOMDZRYBNM-UHFFFAOYSA-N n-naphthalen-1-yl-9-phenyl-n-(9-phenylcarbazol-3-yl)carbazol-3-amine Chemical compound C1=CC=CC=C1N1C2=CC=C(N(C=3C=C4C5=CC=CC=C5N(C=5C=CC=CC=5)C4=CC=3)C=3C4=CC=CC=C4C=CC=3)C=C2C2=CC=CC=C21 COVCYOMDZRYBNM-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 238000001646 magnetic resonance method Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Images
Landscapes
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2006315110A JP5190194B2 (ja) | 2005-12-02 | 2006-11-22 | 精製装置 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2005348659 | 2005-12-02 | ||
| JP2005348659 | 2005-12-02 | ||
| JP2006315110A JP5190194B2 (ja) | 2005-12-02 | 2006-11-22 | 精製装置 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2007175698A JP2007175698A (ja) | 2007-07-12 |
| JP2007175698A5 JP2007175698A5 (enrdf_load_stackoverflow) | 2009-12-24 |
| JP5190194B2 true JP5190194B2 (ja) | 2013-04-24 |
Family
ID=38301408
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2006315110A Expired - Fee Related JP5190194B2 (ja) | 2005-12-02 | 2006-11-22 | 精製装置 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP5190194B2 (enrdf_load_stackoverflow) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101129449B1 (ko) | 2011-05-23 | 2012-03-26 | (주)씨에스엘쏠라 | 분리형 유기재료의 승화 정제용 내부관 |
| JP6096144B2 (ja) * | 2014-03-26 | 2017-03-15 | 出光興産株式会社 | 搬送治具、装填方法、および精製方法 |
| KR101649620B1 (ko) * | 2016-03-18 | 2016-08-19 | 임아영 | 패럴린 코팅장치 |
| JP6432874B1 (ja) * | 2018-06-26 | 2018-12-05 | 株式会社奥本研究所 | 精製装置 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6036304A (ja) * | 1983-08-08 | 1985-02-25 | Nippon Telegr & Teleph Corp <Ntt> | 薬品の精製装置 |
| JP2583306B2 (ja) * | 1989-02-10 | 1997-02-19 | 日本電信電話株式会社 | 試薬の精製装置とその精製方法 |
| JPH03143506A (ja) * | 1989-10-27 | 1991-06-19 | Nippon Telegr & Teleph Corp <Ntt> | 精製装置及び精製方法 |
| JP3246060B2 (ja) * | 1993-04-14 | 2002-01-15 | 日本電信電話株式会社 | フッ化物原料の精製方法 |
| JP3828090B2 (ja) * | 2003-04-15 | 2006-09-27 | 勝華科技股▲ふん▼有限公司 | 昇華純化方法 |
| JP2005111303A (ja) * | 2003-10-03 | 2005-04-28 | Sony Corp | 昇華管及びその製造方法、並びに昇華精製装置 |
-
2006
- 2006-11-22 JP JP2006315110A patent/JP5190194B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JP2007175698A (ja) | 2007-07-12 |
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