JP4233121B2 - 希薄水性溶液からの発酵塩類の回収 - Google Patents

希薄水性溶液からの発酵塩類の回収 Download PDF

Info

Publication number
JP4233121B2
JP4233121B2 JP50557499A JP50557499A JP4233121B2 JP 4233121 B2 JP4233121 B2 JP 4233121B2 JP 50557499 A JP50557499 A JP 50557499A JP 50557499 A JP50557499 A JP 50557499A JP 4233121 B2 JP4233121 B2 JP 4233121B2
Authority
JP
Japan
Prior art keywords
water
extractant
amine
mixture
carboxylate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP50557499A
Other languages
English (en)
Japanese (ja)
Other versions
JP2002510972A5 (enExample
JP2002510972A (ja
Inventor
ホルトザップル,マーク・ティー
デイヴィソン,リチャード・アール
ルエティッヒ,トルステン
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Texas A&M University
Original Assignee
Texas A&M University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Texas A&M University filed Critical Texas A&M University
Publication of JP2002510972A publication Critical patent/JP2002510972A/ja
Publication of JP2002510972A5 publication Critical patent/JP2002510972A5/ja
Application granted granted Critical
Publication of JP4233121B2 publication Critical patent/JP4233121B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/042Breaking emulsions by changing the temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/04Solvent extraction of solutions which are liquid
    • B01D11/0446Juxtaposition of mixers-settlers
    • B01D11/0457Juxtaposition of mixers-settlers comprising rotating mechanisms, e.g. mixers, mixing pumps
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/0208Separation of non-miscible liquids by sedimentation
    • B01D17/0211Separation of non-miscible liquids by sedimentation with baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/0208Separation of non-miscible liquids by sedimentation
    • B01D17/0214Separation of non-miscible liquids by sedimentation with removal of one of the phases
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/041Breaking emulsions with moving devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/044Breaking emulsions by changing the pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/045Breaking emulsions with coalescers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/047Breaking emulsions with separation aids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/04Breaking emulsions
    • B01D17/048Breaking emulsions by changing the state of aggregation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Apparatus Associated With Microorganisms And Enzymes (AREA)
JP50557499A 1997-06-30 1998-06-12 希薄水性溶液からの発酵塩類の回収 Expired - Fee Related JP4233121B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US08/885,841 1997-06-30
US08/885,841 US5986133A (en) 1997-06-30 1997-06-30 Recovery of fermentation salts from dilute aqueous solutions
PCT/US1998/012202 WO1999000352A1 (en) 1997-06-30 1998-06-12 Recovery of fermentation salts from dilute aqueous solutions

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2008240071A Division JP2009000686A (ja) 1997-06-30 2008-09-18 希薄水性溶液からの発酵塩類の回収

Publications (3)

Publication Number Publication Date
JP2002510972A JP2002510972A (ja) 2002-04-09
JP2002510972A5 JP2002510972A5 (enExample) 2005-12-22
JP4233121B2 true JP4233121B2 (ja) 2009-03-04

Family

ID=25387809

Family Applications (2)

Application Number Title Priority Date Filing Date
JP50557499A Expired - Fee Related JP4233121B2 (ja) 1997-06-30 1998-06-12 希薄水性溶液からの発酵塩類の回収
JP2008240071A Pending JP2009000686A (ja) 1997-06-30 2008-09-18 希薄水性溶液からの発酵塩類の回収

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2008240071A Pending JP2009000686A (ja) 1997-06-30 2008-09-18 希薄水性溶液からの発酵塩類の回収

Country Status (6)

Country Link
US (2) US5986133A (enExample)
EP (1) EP0994842A1 (enExample)
JP (2) JP4233121B2 (enExample)
AU (1) AU756707B2 (enExample)
CA (1) CA2294615C (enExample)
WO (1) WO1999000352A1 (enExample)

Families Citing this family (53)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2133385C1 (ru) * 1998-01-27 1999-07-20 Попов Сергей Анатольевич Насосно-эжекторная установка
US6509180B1 (en) 1999-03-11 2003-01-21 Zeachem Inc. Process for producing ethanol
US7074603B2 (en) * 1999-03-11 2006-07-11 Zeachem, Inc. Process for producing ethanol from corn dry milling
US7684786B2 (en) * 2003-08-26 2010-03-23 Nokia Corporation Method and system for establishing a connection between network elements
CA2470978A1 (en) * 2002-01-03 2003-07-24 A.E. Staley Manufacturing Co. Process for purifying an organic acid
US6641734B2 (en) * 2002-01-03 2003-11-04 A. E. Staley Manufacturing Co. Process for purifying an organic acid
DE10251191A1 (de) * 2002-11-04 2004-05-13 Bayer Ag Verfahren zur Trennung von m- und p-Dichlorbenzol enthaltenden Gemischen
AU2005207970B2 (en) 2004-01-29 2011-04-28 Zeachem Inc. Recovery of organic acids
CA2562467C (en) * 2004-04-13 2012-07-31 Iogen Energy Corporation Recovery of inorganic salt during processing of lignocellulosic feedstocks
WO2006007406A2 (en) * 2004-06-16 2006-01-19 The Texas A & M University System Methods and systems for biomass conversion to carboxylic acids and alcohols
JP4734425B2 (ja) * 2006-01-27 2011-07-27 ユニバーシティ オブ マサチューセッツ バイオ燃料および関連材料を製造するためのシステムおよび方法
US9499635B2 (en) 2006-10-13 2016-11-22 Sweetwater Energy, Inc. Integrated wood processing and sugar production
US8323923B1 (en) 2006-10-13 2012-12-04 Sweetwater Energy, Inc. Method and system for producing ethanol
US7670813B2 (en) * 2006-10-25 2010-03-02 Iogen Energy Corporation Inorganic salt recovery during processing of lignocellulosic feedstocks
JP2010517581A (ja) 2007-02-09 2010-05-27 ジーケム インコーポレイテッド 良好なエネルギー効率で生成物を生成するための方法
US8153850B2 (en) 2007-05-11 2012-04-10 The Texas A&M University System Integrated biofuel production system
DE102007059389A1 (de) 2007-07-21 2009-06-10 Universität Dortmund Verfahren zur Aufarbeitung von koaleszenzgehemmten Emulsionen aus Ganzzell-Biotransformationen mit komprimierten oder überkritischen Gasen
JP2011519344A (ja) * 2007-12-31 2011-07-07 ユニヴァーシティー オブ ノースダコタ バイオマスから短鎖カルボン酸とエステルを生産する方法並びにその生成物
US8076504B2 (en) * 2007-12-31 2011-12-13 The University Of North Dakota Method for production of short chain carboxylic acids and esters from biomass and product of same
MX2010008587A (es) * 2008-02-07 2010-09-28 Zeachem Inc Produccion indirecta de butanol y hexanol.
CN101981199A (zh) * 2008-02-27 2011-02-23 奎特罗斯公司 通过两种微生物的顺序作用将植物材料转化为燃料和化学产品的方法
JP2011519578A (ja) * 2008-05-07 2011-07-14 ジーケム インコーポレイテッド 有機酸の回収
MX2011004912A (es) * 2008-11-26 2011-05-30 Univ North Dakota Metodo para producir compuestos organicos ciclicos a partir de aceites de cultivo.
EP2597077A3 (en) * 2008-12-02 2013-09-25 The Texas A&M University System Alternative paths to alcohols and hydrocarbons from biomass
WO2010068637A1 (en) * 2008-12-09 2010-06-17 Jerry Wayne Horton Ensiling biomass and multiple phase apparatus for hydrolyzation of ensiled biomass
JP5536341B2 (ja) 2009-01-06 2014-07-02 住友重機械工業株式会社 減速装置
BRPI1013829A2 (pt) * 2009-04-20 2019-09-24 Qteros Inc composições e métodos para fermentação de biomassa
BRPI1007109A2 (pt) * 2009-04-20 2018-02-20 Greenfield Ethanol Inc "pré- tratamento de biomassa lignocelulósica através da remoção de compostos inibitórios"
US20120329116A1 (en) * 2009-04-20 2012-12-27 Greenfield Ethanol Inc. Pretreatment of lignocellulosic biomass through removal of inhibitory compounds
EP2429976A4 (en) * 2009-05-14 2013-03-06 Univ North Dakota METHOD FOR PRODUCING PRODUCTS HAVING HIGH CARBON OF BIOMASS OIL
PL3199511T3 (pl) 2009-06-04 2020-05-18 Genomatica, Inc. Sposób oddzielania składników brzeczki fermentacyjnej
US9662594B2 (en) * 2009-06-22 2017-05-30 Ng Innovations, Inc. Systems and methods for treating fractionated water
US8409442B2 (en) 2009-08-20 2013-04-02 Ng Innovations, Inc. Water separation method and apparatus
US8470139B2 (en) * 2009-12-11 2013-06-25 Nginnovations, Inc. Systems and method for low temperature recovery of fractionated water
WO2012021956A1 (pt) * 2010-08-19 2012-02-23 Companhia Refinadora Da Amazônia Processo de obtenção de ácido lático com elevado grau de pureza a partir de licor fermentativo
JP2013537541A (ja) 2010-08-19 2013-10-03 コンパニア レフィナドラ ダ アマゾニア 発酵液から高純度の乳酸を得る方法
JP2014518558A (ja) 2011-04-22 2014-07-31 ユニヴァーシティー オブ ノースダコタ 非接触分解された脂肪酸に基づく油からの芳香族化合物の製造
GB2496599A (en) * 2011-08-26 2013-05-22 Tha Ni Ind E Gmbh Two tank fermentation system and method of operation
KR20140127218A (ko) * 2011-12-21 2014-11-03 인비스타 테크놀러지스 에스.에이 알.엘. 안정한 에멀젼을 감소시키기 위한 추출 용매 제어
KR20140108683A (ko) 2011-12-21 2014-09-12 인비스타 테크놀러지스 에스.에이 알.엘. 안정한 에멀젼을 감소시키기 위한 추출 용매 제어
CN103402595B (zh) * 2011-12-21 2016-02-03 因温斯特技术公司 用于减少稳定乳液的萃取溶剂控制
HK1199630A1 (en) 2011-12-21 2015-07-10 因温斯特技术公司 Extraction solvent control for reducing stable emulsions
US8765430B2 (en) 2012-02-10 2014-07-01 Sweetwater Energy, Inc. Enhancing fermentation of starch- and sugar-based feedstocks
LT2836602T (lt) 2012-04-13 2019-04-10 Sweetwater Energy, Inc. Biomasės cukrinimo būdai ir sistemos
US8563277B1 (en) 2012-04-13 2013-10-22 Sweetwater Energy, Inc. Methods and systems for saccharification of biomass
EP2970068B1 (en) 2013-03-15 2021-07-28 Genomatica, Inc. Process and systems for obtaining 1,4-butanediol from fermentation broths
US9809867B2 (en) 2013-03-15 2017-11-07 Sweetwater Energy, Inc. Carbon purification of concentrated sugar streams derived from pretreated biomass
AU2013397905B2 (en) 2013-08-15 2017-11-23 Hatch Ltd. Multi-compartment reactor and method for controlling retention time in a multi-compartment reactor
AU2015360513B2 (en) 2014-12-09 2020-03-12 Apalta Patents OÜ Rapid pretreatment
EP3583223A4 (en) 2017-02-16 2020-12-23 Sweetwater Energy, Inc. HIGH PRESSURE ZONE TRAINING FOR PRETREATMENT
CN109384666B (zh) 2018-11-26 2021-06-22 广州楹鼎生物科技有限公司 一种联动回收有机酸水溶液中有机酸的方法
US11692000B2 (en) 2019-12-22 2023-07-04 Apalta Patents OÜ Methods of making specialized lignin and lignin products from biomass
CN116062829B (zh) * 2022-12-12 2024-10-08 内蒙古鄂尔多斯电力冶金集团股份有限公司 一种非变温的萃取结晶脱盐方法

Family Cites Families (40)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1442306A (en) * 1923-01-16 Oil-elotation apparatus
GB277975A (en) 1926-09-23 1929-01-21 Fernand Germain Process for the production of butyrone
FR642698A (fr) 1927-03-23 1928-09-01 H Gouthiere Et Cie Soc Procédé de fabrication des cétones
CH132022A (fr) 1928-03-07 1929-03-31 Ketol Sa L Procédé pour la décomposition continue de substances par la chaleur.
GB445108A (en) 1934-10-02 1936-04-02 British Celanese Improvements in the recovery of acidic and basic reagents
FR1064614A (fr) 1949-06-21 1954-05-17 Procédé et dispositif pour la production de gaz méthane, dane les installations septiques rurales en particulier
US2845936A (en) * 1955-05-09 1958-08-05 Hercules Powder Co Ltd Countercurrent contacting apparatus
US3079705A (en) 1959-01-20 1963-03-05 Bauer Bros Co Peanut cooler
US3088909A (en) * 1961-02-09 1963-05-07 Richard R Davison Mixed solvents for saline water extraction
US3424675A (en) * 1965-08-25 1969-01-28 Us Interior Vapor compression solvent extractor desalination
GB1140224A (en) 1966-02-16 1969-01-15 Inst Gornogo Dela Sibirskogo O Vibration magnetometer
NL6801614A (enExample) * 1968-02-05 1969-08-07
DE7138603U (de) * 1971-10-12 1972-06-15 Passavant Werke Vorrichtung zur mechanisch-chemischen Wasseraufbereitung und Abwasserbehandlung
BE793060A (fr) * 1971-12-24 1973-04-16 Metallgesellschaft Ag Dispositif pour separer des liquides
FR2227830A1 (en) 1973-05-04 1974-11-29 Guttridge Ltd David Portable pellet processing appts - with air drying columns and screens for farm animal feed
US4132651A (en) * 1976-02-19 1979-01-02 Dejong Leendert W C Separating device to separate two liquids of different specific gravity
DE2710241A1 (de) * 1976-03-11 1977-09-22 Krebs & Co Ag Verfahren zum vermengen und trennen von zwei nicht mischbaren fluessigkeiten
US4131651A (en) * 1977-10-25 1978-12-26 Barnes-Hind Pharmaceuticals, Inc. Treatment of dry eye
FI57059C (fi) * 1978-06-28 1980-06-10 Outokumpu Oy Extraktionsenhet foer vaetske-vaetske-extraktion
JPS6027441Y2 (ja) * 1980-03-17 1985-08-19 住友金属鉱山株式会社 液々抽出装置
AU7279981A (en) 1980-08-21 1982-02-25 Koppers Company, Inc. Method + apparatus for cooling pellets
US4444881A (en) 1981-10-26 1984-04-24 Cpc International Inc. Recovery of organic acids from a fermentation broth
US4469582A (en) * 1982-03-22 1984-09-04 Combustion Engineering, Inc. Electrically enhanced inclined plate separator
JPS597131A (ja) * 1982-07-06 1984-01-14 Daicel Chem Ind Ltd 酢酸の回収法
JPS5912706A (ja) * 1982-07-13 1984-01-23 Daicel Chem Ind Ltd ミキサ−セトラ−の運転方法
DE3312579A1 (de) 1983-04-08 1984-10-11 Bayer Ag, 5090 Leverkusen Verfahren zur durchfuehrung von mikrobiologischen umsetzungen bei enger verweilzeitverteilung
SE445710B (sv) * 1984-11-01 1986-07-14 Hyosong M Lee Anordning for kontinuerlig separering av en vetskeblandning, innehallande en lettare och en tyngre fas
US4978616A (en) 1985-02-28 1990-12-18 Verax Corporation Fluidized cell cultivation process
EP0355159B1 (de) * 1987-12-23 1992-08-12 Institut Khimii I Tekhnologii Redkikh Elementov I Mineralnogo Syrya Kolskogo Filiala Akademii Nauk Sssr Misch- und absetzapparat für die flüssig-flüssig-extraktion
EP0444338B1 (en) 1990-03-01 1993-06-02 Cominco Ltd. Method and apparatus for cooling particulate solids
US5046856A (en) * 1989-09-12 1991-09-10 Dowell Schlumberger Incorporated Apparatus and method for mixing fluids
US5132456A (en) 1991-05-07 1992-07-21 The Regents Of The University Of California Sorption of carboxylic acid from carboxylic salt solutions at PHS close to or above the pKa of the acid, with regeneration with an aqueous solution of ammonia or low-molecular-weight alkylamine
US5326474A (en) * 1992-11-13 1994-07-05 The United States Of America As Represented By The Secretary Of The Navy Low flow fluid separator
US5264623A (en) * 1993-01-04 1993-11-23 Energy Mines & Resources Canada Method of producing calcium salts from biomass
TW360636B (en) * 1993-07-12 1999-06-11 Glitsch Method and apparatus for recovering acetic acid from aqueous streams
US5554301A (en) * 1995-05-08 1996-09-10 Universal Environmental Technologies, Inc. Water clarification system
DE19624268C2 (de) 1995-09-30 2001-09-27 Herhof Umwelttechnik Gmbh Verfahren und Vorrichtung zur Verwertung organischer Abfälle
US5874263A (en) 1996-07-31 1999-02-23 The Texas A&M University System Method and apparatus for producing organic acids
US5795478A (en) * 1997-01-15 1998-08-18 Hirs; Gene Oil extraction system
US6043392A (en) * 1997-06-30 2000-03-28 Texas A&M University System Method for conversion of biomass to chemicals and fuels

Also Published As

Publication number Publication date
US6478965B1 (en) 2002-11-12
CA2294615A1 (en) 1999-01-07
EP0994842A1 (en) 2000-04-26
WO1999000352A1 (en) 1999-01-07
JP2002510972A (ja) 2002-04-09
AU7961898A (en) 1999-01-19
CA2294615C (en) 2009-07-14
JP2009000686A (ja) 2009-01-08
US5986133A (en) 1999-11-16
AU756707B2 (en) 2003-01-23

Similar Documents

Publication Publication Date Title
JP4233121B2 (ja) 希薄水性溶液からの発酵塩類の回収
Wasewar SeparationofLacticAcid: RecentAdvances
JP4272345B2 (ja) バイオマスを化学品及び燃料に転化する方法
KR102237801B1 (ko) 발효액 성분들의 분리 방법
JP2003511360A (ja) 精製乳酸溶液の製造方法
CN109665661B (zh) 一种从糠醛废水中分离硫酸、醋酸和糠醛的方法
EP2470491A1 (en) Recovery of volatile carboxylic acids by extractive evaporation
CN109294893B (zh) 一种白酒酿造副产物黄水的资源化利用系统及方法
CN103012104A (zh) 一种处理丁辛醇废碱液回收丁酸的方法
CN102911854A (zh) 一种分离纯化丁醇和丙酮的装置及方法
CN215799238U (zh) 乙醛酸精制的工艺装置
CN115974204B (zh) 醇醛缩合反应废碱液的处理方法
CN115028530B (zh) 一种长链二元酸的提取工艺及长链二元酸产品
CN112898148B (zh) 乙醛酸精制的工艺方法和装置
MXPA00000128A (en) Recovery of fermentation salts from dilute aqueous solutions
CN1275931C (zh) 从青霉素发酵液萃余相废水中分离乙酸丁酯的方法及设备
CN111411019A (zh) 一种高epa含量的深海鱼油及其加工工艺
CN1185206C (zh) 一种含4-氨基二苯胺组合物的分离方法及其设备
CN116332749A (zh) 从有机固废厌氧发酵液中绿色回收高浓度乙酸的方法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20050610

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20050610

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20080318

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20080617

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20080728

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20080918

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20081111

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20081209

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20111219

Year of fee payment: 3

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20111219

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20121219

Year of fee payment: 4

LAPS Cancellation because of no payment of annual fees