JP4121602B2 - 二種金属シアン化物触媒の製造方法 - Google Patents

二種金属シアン化物触媒の製造方法 Download PDF

Info

Publication number
JP4121602B2
JP4121602B2 JP04805698A JP4805698A JP4121602B2 JP 4121602 B2 JP4121602 B2 JP 4121602B2 JP 04805698 A JP04805698 A JP 04805698A JP 4805698 A JP4805698 A JP 4805698A JP 4121602 B2 JP4121602 B2 JP 4121602B2
Authority
JP
Japan
Prior art keywords
iii
ligand
catalyst
water
suspension
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP04805698A
Other languages
English (en)
Japanese (ja)
Other versions
JPH10277398A5 (enExample
JPH10277398A (ja
Inventor
ゲオルク、ハインリヒ、グロシュ
ハーラルト、ラルビッヒ
ディーター、ユンゲ
ダニーラ、ゲーレン
ペーター、デ、フォクト
ゲルト、ヘプナー
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=26034540&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=JP4121602(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by BASF SE filed Critical BASF SE
Publication of JPH10277398A publication Critical patent/JPH10277398A/ja
Publication of JPH10277398A5 publication Critical patent/JPH10277398A5/ja
Application granted granted Critical
Publication of JP4121602B2 publication Critical patent/JP4121602B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4866—Polyethers having a low unsaturation value
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24—Nitrogen compounds
    • B01J27/26—Cyanides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyethers (AREA)
  • Catalysts (AREA)
JP04805698A 1997-03-06 1998-02-27 二種金属シアン化物触媒の製造方法 Expired - Fee Related JP4121602B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19709031A DE19709031A1 (de) 1997-03-06 1997-03-06 Verfahren zur Herstellung von Doppelmetallcyanidkatalysatoren
DE19709031.1 1997-03-06
US09/035,601 US6303533B1 (en) 1997-03-06 1998-03-05 Process for preparing two-metal cyanide catalysts

Publications (3)

Publication Number Publication Date
JPH10277398A JPH10277398A (ja) 1998-10-20
JPH10277398A5 JPH10277398A5 (enExample) 2005-09-02
JP4121602B2 true JP4121602B2 (ja) 2008-07-23

Family

ID=26034540

Family Applications (1)

Application Number Title Priority Date Filing Date
JP04805698A Expired - Fee Related JP4121602B2 (ja) 1997-03-06 1998-02-27 二種金属シアン化物触媒の製造方法

Country Status (6)

Country Link
US (1) US6303533B1 (enExample)
EP (1) EP0862947B2 (enExample)
JP (1) JP4121602B2 (enExample)
CA (1) CA2228651A1 (enExample)
DE (2) DE19709031A1 (enExample)
ES (1) ES2198610T5 (enExample)

Families Citing this family (46)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19742978A1 (de) 1997-09-29 1999-04-01 Basf Ag Multimetallcyanidkomplexe als Katalysatoren
US6051680A (en) * 1998-06-08 2000-04-18 Arco Chemical Technology, L.P. Silylated double metal cyanide complex catalysts
DE19917897A1 (de) † 1999-04-20 2000-10-26 Basf Ag Verfahren zur Herstellung von Polyurethanen
DE19919267A1 (de) 1999-04-28 2000-11-02 Bayer Ag Kristallisierende Polyetherpolyole, ein Verfahren zu deren Herstellung sowie deren Verwendung
ES2244446T3 (es) * 1999-06-02 2005-12-16 Basf Aktiengesellschaft Procedimiento para la preparacion de polieterpolioles con empleo de catalizadores cristalinos de cianuros polimetalicos.
US6800583B2 (en) * 1999-06-02 2004-10-05 Basf Aktiengesellschaft Suspension of multimetal cyanide compounds, their preparation and their use
US6613714B2 (en) * 1999-06-02 2003-09-02 Basf Aktiengesellschaft Multimetal cyanide compounds, their preparation and their use
JP2003504461A (ja) * 1999-07-09 2003-02-04 ザ ダウ ケミカル カンパニー スルホン化合物またはスルホキシド化合物で錯化された金属触媒
US6376645B1 (en) * 1999-07-09 2002-04-23 The Dow Chemical Company Complexing agent-modified hexacyanometallate hexanitrometallate catalysts
US6358877B1 (en) 1999-09-10 2002-03-19 The Dow Chemical Company Metal catalysts complexed with sulfone or sulfoxide compounds
DE19949091A1 (de) 1999-10-12 2001-04-26 Basf Ag Polyester-Polyetherblockcopolymere
US6429166B1 (en) * 2000-05-19 2002-08-06 Dow Global Technologies Inc. Method for preparing metal cyanide catalyst/polyol initiator slurries
US6436867B1 (en) * 2000-08-01 2002-08-20 Basf Corporation One-step synthesis of double metal cyanides
DE10137628A1 (de) * 2001-08-03 2003-02-27 Basf Ag Verfahren zur Herstellung von Polyurethan-Weichschaumstoffen
DE10141122A1 (de) * 2001-08-22 2003-03-13 Basf Ag Verfahren zur Erhöhung der katalytischen Aktivität von Multimetallcyanidverbindungen
US6696383B1 (en) * 2002-09-20 2004-02-24 Bayer Polymers Llc Double-metal cyanide catalysts which can be used to prepare polyols and the processes related thereto
US6806348B2 (en) * 2003-02-11 2004-10-19 Basf Corporation Process for removing and regenerating a double metal cyanide (DMC) catalyst from a polymer polyol
CN1867609A (zh) * 2003-03-07 2006-11-22 陶氏环球技术公司 制备聚醚多元醇的连续方法和设备
US6855658B1 (en) 2003-08-26 2005-02-15 Bayer Antwerp, N.V. Hydroxide containing double metal cyanide (DMC) catalysts
DE102004013408A1 (de) 2004-03-18 2005-10-06 Basf Ag Polyetheralkohole und Verfahren zur Herstellung von Polyetheralkoholen zur Polyurethansynthese
EP1983010A3 (de) 2007-04-19 2009-07-29 Basf Se Verfahren zur Herstellung von Polyurethanen
EP2003156A1 (de) 2007-04-19 2008-12-17 Basf Se Urethangruppen und Isocyanatgruppen enthaltende Prepolymere
DE102008042715A1 (de) 2007-10-12 2009-04-16 Basf Se Polyetherpolyole
PT2238195E (pt) 2008-01-29 2015-04-02 Basf Se Método para a produção de poliéter álcoois
CN101684184A (zh) 2008-09-27 2010-03-31 巴斯夫欧洲公司 可通过使用可再生的原料获得的聚氨酯鞋底
DE102009045651A1 (de) 2008-10-17 2010-04-29 Basf Se Textilien und Verfahren zu ihrer Herstellung
BR112012000634A2 (pt) 2009-07-10 2016-02-10 Basf Se processo para a produção de polióis, poliol, uso de polióis, e, processo para a produção de poliuretanos
WO2011085772A1 (en) 2010-01-15 2011-07-21 Basf Se "process for the dmc-catalyzed preparation of polyols"
DE102010039090A1 (de) 2010-08-09 2012-02-09 Basf Se Verfahren zur Herstellung von Polyetheralkoholen
CN105189719B (zh) 2013-03-11 2018-05-29 巴斯夫欧洲公司 聚烷氧基化物在润滑剂组合物中的用途
AU2014267528B2 (en) 2013-05-17 2017-05-18 Basf Se The use of polytetrahydrofuranes in lubricating oil compositions
KR102220786B1 (ko) * 2013-07-18 2021-03-02 에스케이이노베이션 주식회사 이중금속 시아나이드(ｄｍｃ) 촉매 및 이를 통해 제조된 에폭사이드/이산화탄소 공중합체
US20150113867A1 (en) 2013-10-24 2015-04-30 Basf Se Use of an alkoxylated polytetrahydrofuran to reduce fuel consumption
WO2015113850A1 (en) 2014-01-28 2015-08-06 Basf Se The use of alkoxylated polyethylene glycols in lubricating oil compositions
EP3146028B1 (en) 2014-05-22 2018-07-11 Basf Se Lubricant compositions containing beta-glucans
EP3029087A1 (de) 2014-12-05 2016-06-08 Evonik Degussa GmbH Verfahren zur Herstellung von niedrigviskosen Polyethersiloxanen
US9562135B1 (en) 2015-12-21 2017-02-07 Covestro Llc Polyether carbonates by DMC catalysis
EP3315591A1 (en) 2016-10-28 2018-05-02 Basf Se Energy efficient lubricant compositions
PL3700956T3 (pl) 2017-10-27 2025-06-23 Huntsman International Llc Katalizatory do wytwarzania materiałów oksazolidynonowych
US10479862B2 (en) 2017-12-07 2019-11-19 Covestro Llc Amine based polymer polyol stabilizers
US10526484B2 (en) 2017-12-20 2020-01-07 Covestro Llc Dithiocarbonate containing polyols as polymer polyol stabilizers
ES2941289T3 (es) * 2018-12-21 2023-05-19 Dow Global Technologies Llc Proceso de polimerización de poliéter
US11566145B2 (en) 2019-03-14 2023-01-31 Covestro Llc Polyurethane coating compositions and their use as gel coats
US10544158B1 (en) 2019-03-14 2020-01-28 Covestro Llc Process for producing polycyclic polyether polyols
KR102717144B1 (ko) * 2021-07-15 2024-10-11 아주대학교산학협력단 하이드로젠 헥사시아노코발테이트와 아연 카복실레이트의 조합으로 제조된 더블메탈시아나이드 촉매 및 이를 이용한 프로필렌 옥사이드 중합
CN116376001A (zh) * 2023-04-10 2023-07-04 浙江皇马科技股份有限公司 一种改性双金属氰化物合成宽分子量分布脂肪醇聚醚的方法

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DD148957A1 (de) * 1980-01-31 1981-06-17 Gerhard Behrendt Verfahren zur herstellung von hochmolekularen polyetheralkoholen
US4764567A (en) 1986-11-20 1988-08-16 Basf Corporation Process for the preparation of polyoxyalkylene block polyethers having enhanced properties
CA2138063C (en) * 1993-12-23 2007-02-20 Bi Le-Khac Polyurethane foam-supported double metal cyanide catalysts for polyol synthesis
US5482908A (en) * 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5627122A (en) 1995-07-24 1997-05-06 Arco Chemical Technology, L.P. Highly active double metal cyanide complex catalysts
US5639705A (en) * 1996-01-19 1997-06-17 Arco Chemical Technology, L.P. Double metal cyanide catalysts and methods for making them

Also Published As

Publication number Publication date
DE19709031A1 (de) 1998-09-10
ES2198610T3 (es) 2004-02-01
ES2198610T5 (es) 2008-02-16
EP0862947B1 (de) 2003-04-23
US6303533B1 (en) 2001-10-16
EP0862947B2 (de) 2007-09-05
DE59808009D1 (de) 2003-05-28
EP0862947A1 (de) 1998-09-09
JPH10277398A (ja) 1998-10-20
CA2228651A1 (en) 1998-09-06

Similar Documents

Publication Publication Date Title
JP4121602B2 (ja) 二種金属シアン化物触媒の製造方法
JP4471492B2 (ja) 触媒としての複数シアン化金属錯体
US5789626A (en) Highly active double metal cyanide catalysts
KR100355336B1 (ko) 고활성이중금속시안나이드촉매
JP4043061B2 (ja) 改良されたポリエーテル含有二重金属シアン化物触媒並びにその製法および用途
ES2199712T3 (es) Nuevos catalizadores de cianuro bimetalico para la fabricacion de polioleteres.
CA2179946A1 (en) Highly active double metal cyanide complex catalysts
JPH0480933B2 (enExample)
US6596842B2 (en) Polymerizing alkylene oxide with sound or radiation treated DMC
HUP0103774A2 (hu) Kettős fém-cianid katalizátorok poliéter-poliolok előállítására
US6624286B2 (en) Double-metal cyanide catalysts containing polyester for preparing polyether polyols
KR100589580B1 (ko) 폴리에테르 폴리올의 제조에 사용되는 이중 금속시아나이드 촉매
CA2306386C (en) Double metal cyanide catalysts containing polyester for preparing polyether polyols
KR20010101746A (ko) 폴리에테르 폴리올의 제조 방법
HU223381B1 (hu) Kettős fémcianid-katalizátorok alkalmazása poliéter-poliolok előállítására
JP2005509051A (ja) ポリエーテルポリオールを製造するための複金属シアン化物触媒
CN1326614C (zh) 用零价金属制备金属氰化物催化剂的方法
JP2005501947A (ja) ポリエーテルポリオールを製造するための複金属シアン化物触媒
US6358877B1 (en) Metal catalysts complexed with sulfone or sulfoxide compounds
RU2237515C2 (ru) Двойной металлцианидный катализатор, способ его получения и способ получения полиэфирполиолов
MXPA98001797A (en) Process for the preparation of two-metal cyanide catalysts
MXPA00003563A (en) Crystalline double metal cyanide catalysts for producing polyether polyols
MXPA00003447A (en) Double metal cyanide catalysts containing polyester for preparing polyether polyoles
JP2003504461A (ja) スルホン化合物またはスルホキシド化合物で錯化された金属触媒

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20050225

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20050225

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20061219

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20061221

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20070301

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20070828

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20071126

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20080401

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20080430

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20110509

Year of fee payment: 3

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

LAPS Cancellation because of no payment of annual fees