JP3126032B2 - 気体−固体反応システムによるアンモニウムグリホセートの製造 - Google Patents

気体−固体反応システムによるアンモニウムグリホセートの製造

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Publication number
JP3126032B2
JP3126032B2 JP09500437A JP50043797A JP3126032B2 JP 3126032 B2 JP3126032 B2 JP 3126032B2 JP 09500437 A JP09500437 A JP 09500437A JP 50043797 A JP50043797 A JP 50043797A JP 3126032 B2 JP3126032 B2 JP 3126032B2
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JP
Japan
Prior art keywords
temperature
glyphosate
reaction
reactor
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP09500437A
Other languages
English (en)
Japanese (ja)
Other versions
JPH10511688A (ja
Inventor
デイ，トーマス・マクケイブ
ギレスピ，ジエーン・ローラ
クラマー，リチヤード・メルビン
Original Assignee
モンサント・カンパニー
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by モンサント・カンパニー filed Critical モンサント・カンパニー
Publication of JPH10511688A publication Critical patent/JPH10511688A/ja
Application granted granted Critical
Publication of JP3126032B2 publication Critical patent/JP3126032B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
    • A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
    • C07F9/3804—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)] not used, see subgroups
    • C07F9/3808—Acyclic saturated acids which can have further substituents on alkyl
    • C07F9/3813—N-Phosphonomethylglycine; Salts or complexes thereof

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Dentistry (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
JP09500437A 1995-06-07 1996-03-05 気体−固体反応システムによるアンモニウムグリホセートの製造 Expired - Lifetime JP3126032B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US485,316 1995-06-07
US08/485,316 US5633397A (en) 1995-06-07 1995-06-07 Preparation of ammonium glyphosate via a gas-solid reaction system
PCT/US1996/003082 WO1996040697A1 (en) 1995-06-07 1996-03-05 Preparation of ammonium glyphosate via a gas-solid reaction system

Publications (2)

Publication Number Publication Date
JPH10511688A JPH10511688A (ja) 1998-11-10
JP3126032B2 true JP3126032B2 (ja) 2001-01-22

Family

ID=23927683

Family Applications (1)

Application Number Title Priority Date Filing Date
JP09500437A Expired - Lifetime JP3126032B2 (ja) 1995-06-07 1996-03-05 気体−固体反応システムによるアンモニウムグリホセートの製造

Country Status (21)

Country Link
US (1) US5633397A (en:Method)
EP (1) EP0832086B1 (en:Method)
JP (1) JP3126032B2 (en:Method)
KR (1) KR100257283B1 (en:Method)
CN (1) CN1068008C (en:Method)
AR (1) AR002087A1 (en:Method)
AT (1) ATE196908T1 (en:Method)
AU (1) AU704518B2 (en:Method)
BR (1) BR9608561A (en:Method)
CA (1) CA2221299C (en:Method)
DE (1) DE69610629T2 (en:Method)
ES (1) ES2152019T3 (en:Method)
HU (1) HUP9802088A3 (en:Method)
IL (1) IL118576A (en:Method)
MY (1) MY134658A (en:Method)
NZ (1) NZ306043A (en:Method)
RU (1) RU2164518C2 (en:Method)
TW (1) TW300159B (en:Method)
UA (1) UA48972C2 (en:Method)
WO (1) WO1996040697A1 (en:Method)
ZA (1) ZA964774B (en:Method)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5614468A (en) * 1995-06-07 1997-03-25 Monsanto Company Preparation of ammonium glyphosate using aqueous ammonium hydroxide in a liquid-solid reaction system
MY120452A (en) * 1997-07-22 2005-10-31 Monsanto Technology Llc High- loaded ammonium glyphosate formulations
MXPA02000979A (es) 1999-07-28 2003-07-21 Monsanto Technology Llc Metodo para fabricar una pasta de glifosato de amonio que se puede procesar corriente abajo.
US6448434B1 (en) 1999-07-29 2002-09-10 Monsanto Technology Llc Process for making ammonium glyphosate powder
US6599858B1 (en) 1999-07-29 2003-07-29 Monsanto Technology Llc Process for making ammonium glyphosate flakes
CN1072672C (zh) * 1999-11-08 2001-10-10 浙江新安化工集团股份有限公司 草甘膦酸铵的制备方法
US6734142B2 (en) 2001-04-23 2004-05-11 Monsanto Technology Llc Ammonium glyphosate compositions and process for their preparation
KR100456288B1 (ko) * 2001-12-20 2004-11-09 (주)한백 반도체/평판 디스플레이 제조용 기판의 온도 안정화 장치
EP2172107A2 (en) * 2002-08-31 2010-04-07 Monsanto Technology LLC Process for the preparation of a dry pesticidal composition containing a dicarboxylate component
BR0313970A (pt) 2002-08-31 2005-09-06 Monsanto Technology Llc Composições pesticidas contendo ácidos dicarboxìlicos
US20050037924A1 (en) * 2002-08-31 2005-02-17 Monsanto Technology Llc Sodium glyphosate compositions and process for their preparation
CN1244587C (zh) * 2002-09-05 2006-03-08 浙江新安化工集团股份有限公司 气－液－固三相反应及溶剂萃取制备草甘膦酸铵
AR037559A1 (es) * 2002-11-19 2004-11-17 Atanor S A Una formulacion herbicida solida de n-fosfonometilglicina, bajo la forma de polvo, granulos o escamas, soluble o dispersable en agua, y el procedimiento para preparar dicha composicion
ITMI20051138A1 (it) * 2005-06-17 2006-12-18 Sipcam Spa Processo per preparare granuli di glifosate ammonico
CN100389116C (zh) * 2006-06-12 2008-05-21 江苏好收成韦恩农药化工有限公司 用草甘膦二、三价盐生产草甘膦一价盐的方法
CN1958594B (zh) * 2006-11-17 2011-08-10 浙江新安化工集团股份有限公司 一种制备草甘膦异丙胺盐固体的方法
US20110071027A1 (en) * 2009-09-18 2011-03-24 Volker Heide High strength aqueous glyphosate salt concentrates and methods
EP3278668A1 (en) 2009-12-08 2018-02-07 Eureka! Agresearch (Vic) Pty Ltd Novel glyphosate formulation
CN103980308B (zh) * 2014-05-27 2016-04-06 湘潭大学 一种双甘膦氧化反应液的后处理方法
CN115594712B (zh) * 2022-10-08 2023-12-19 湖北泰盛化工有限公司 一种气固非均相草甘膦连续氨化的方法

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3671612A (en) * 1968-04-05 1972-06-20 Knapsack Ag Process for the manufacture of ammonium dialkyldithiophosphates
BR8600462A (pt) * 1986-02-04 1987-09-01 Monsanto Brasil Formulacao herbicida
ZA871571B (en) * 1986-03-20 1987-08-24 Uniroyal Chemical Company, Inc. Dry reactive processing
US5070197A (en) * 1986-03-20 1991-12-03 Uniroyal Chemical Company, Inc. Dry reactive processing
US5047079A (en) * 1986-08-18 1991-09-10 Ici Americas Inc. Method of preparation and use of solid, phytoactive compositions
DK170456B1 (da) * 1986-08-18 1995-09-11 Stauffer Chemical Co Fremgangsmåde til fremstilling af faste, fytoaktive midler
NZ231897A (en) * 1988-12-30 1992-09-25 Monsanto Co Dry water-soluble granular composition comprising glyphosate and a liquid surfactant
NO901662L (no) * 1989-04-17 1990-12-21 Monsanto Co Toert herbicid preparat med forbedret vannopploeselighet.
EP0568635B1 (en) * 1991-01-24 1997-03-19 Monsanto Company Improved glyphosate formulations
IL101539A (en) * 1991-04-16 1998-09-24 Monsanto Europe Sa Non-hygroscopic mono-ammonium salts of n-phosphonomethyl glycine derivatives their preparation and pesticidal compositons containing them
US5266553A (en) * 1991-10-21 1993-11-30 Riverdale Chemical Company Method of manufacturing a dry water-soluble herbicidal salt composition
FR2692439A1 (fr) * 1992-05-26 1993-12-24 Osa Sacifia Prod Produit applicable, comme agent phytotoxique comprenant un sel d'ammonium de (N-Phosphonométhyl)glycine, composition concentrée et préparation phytotoxique le contenant.
MY111437A (en) * 1992-07-31 2000-05-31 Monsanto Co Improved glyphosate herbicide formulation.
CA2148840A1 (en) * 1992-11-06 1994-05-26 Jim F. Stewart Dry water-dispersible glyphosate phytoactive formulation
US5614468A (en) * 1995-06-07 1997-03-25 Monsanto Company Preparation of ammonium glyphosate using aqueous ammonium hydroxide in a liquid-solid reaction system

Also Published As

Publication number Publication date
TW300159B (en) 1997-03-11
US5633397A (en) 1997-05-27
AU704518B2 (en) 1999-04-22
BR9608561A (pt) 1999-07-06
DE69610629D1 (de) 2000-11-16
EP0832086B1 (en) 2000-10-11
WO1996040697A1 (en) 1996-12-19
AR002087A1 (es) 1998-01-07
KR19990022560A (ko) 1999-03-25
EP0832086A1 (en) 1998-04-01
HUP9802088A3 (en) 1999-03-29
CN1068008C (zh) 2001-07-04
ZA964774B (en) 1997-01-08
KR100257283B1 (ko) 2000-05-15
CA2221299C (en) 2001-06-05
MY134658A (en) 2007-12-31
RU2164518C2 (ru) 2001-03-27
AU5419596A (en) 1996-12-30
NZ306043A (en) 1998-12-23
HUP9802088A2 (hu) 1998-12-28
IL118576A (en) 2000-09-28
ES2152019T3 (es) 2001-01-16
ATE196908T1 (de) 2000-10-15
IL118576A0 (en) 1996-10-16
CN1192742A (zh) 1998-09-09
MX9709428A (es) 1998-07-31
DE69610629T2 (de) 2001-05-03
CA2221299A1 (en) 1996-12-19
UA48972C2 (uk) 2002-09-16
JPH10511688A (ja) 1998-11-10

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JP3126032B2 (ja) 気体−固体反応システムによるアンモニウムグリホセートの製造
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EP0845000B1 (en) Preparation of ammonium glyphosate using aqueous ammonium hydroxiye in a liquid-solid reaction system
KR20020029079A (ko) 다운스트림 공정이 가능한 암모늄글리포세이트 페이스트의제조방법
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