JP2543919B2 - 冷凍機油組成物 - Google Patents

冷凍機油組成物

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Publication number
JP2543919B2
JP2543919B2 JP62312357A JP31235787A JP2543919B2 JP 2543919 B2 JP2543919 B2 JP 2543919B2 JP 62312357 A JP62312357 A JP 62312357A JP 31235787 A JP31235787 A JP 31235787A JP 2543919 B2 JP2543919 B2 JP 2543919B2
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Japan
Prior art keywords
fluorine
oil
substituted
group
alkyl group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP62312357A
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English (en)
Other versions
JPH01153792A (ja
Inventor
正人 金子
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Idemitsu Kosan Co Ltd
Original Assignee
Idemitsu Kosan Co Ltd
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Filing date
Publication date
Application filed by Idemitsu Kosan Co Ltd filed Critical Idemitsu Kosan Co Ltd
Priority to JP62312357A priority Critical patent/JP2543919B2/ja
Priority to US07/280,959 priority patent/US4946611A/en
Priority to KR1019880016614A priority patent/KR930010532B1/ko
Publication of JPH01153792A publication Critical patent/JPH01153792A/ja
Application granted granted Critical
Publication of JP2543919B2 publication Critical patent/JP2543919B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Description

【発明の詳細な説明】 〔産業上の利用分野〕 本発明は冷凍機油組成物に関し、詳しくは基油に特定
のフッ素化合物を添加してなり、各種のフロン系化合物
等の冷媒に対して安定で、しかも耐焼付性等の優れた冷
凍機油組成物に関する。
〔従来の技術及び発明が解決しようとする問題点〕
一般に、冷凍機油に要求される性能は、フロン等の冷
媒に対して安定であるとともに、耐焼付性や耐摩耗性等
の潤滑性に優れていることがあげられる。特に、最近に
至ってはコンプレッサーの回転数が高くなり、またイン
バーター化されるなど冷凍機が過酷な条件下で運転され
るようになってきており、潤滑性の一層の向上が必要不
可欠の条件になってきている。
従来、冷凍機油の潤滑性を向上させる方策としては、
基油にトリクレシルホスフェート（TCP）等のリン系化
合物やジアルキルスルフィド等のイオウ系化合物などが
配合されていたが、潤滑性の向上に限界があり、しか
も、冷媒に対する安定性が悪いという問題があった。
そこで、本発明者は上記従来の冷凍機油等の問題点を
解消し、耐焼付荷重が高く、しかも各種の冷媒に対して
安定性を有する冷凍機油組成物を開発すべく鋭意研究を
重ねた。
〔問題点を解決するための手段〕
その結果、特定のフッ素化合物を基油に添加すること
により上記目的を達成しうることを見出し、本発明を完
成するに至った。すなわち本発明は、鉱油及び／又は合
成油からなる基油に、 一般式 〔式中、R1,R2はそれぞれ炭素数１〜20のアルキル基，
炭素数６〜30のアリール基，炭素数６〜30のシクロアル
キル基，炭素数１〜20のフッ素置換アルキル基，炭素数
６〜30のフッ素置換アリール基あるいは炭素数６〜30の
フッ素置換シクロアルキル基を示し、R3〜R6はそれぞれ
炭素数１〜20のフッ素置換アルキル基，炭素数６〜30の
フッ素置換アリール基あるいは炭素数６〜30のフッ素置
換シクロアルキル基を示す。また、ｍは１〜100のいず
れかの数を示す。〕 で表わされるフッ素化合物を0.01〜50重量％の割合で配
合することを特徴とする冷凍機油組成物を提供するもの
である。
本発明の冷凍機油組成物は、上述の如く鉱油，合成油
を単独であるいは両者を混合したものを基油として用い
る。この基油の性状については特に制限はないが、通常
は40℃における動粘度が５〜500cSt、好ましくは10〜30
0cStである。ここで動粘度が5cSt未満のものでは、蒸発
により油消費量が多く、また油循環量が多くなり、さら
にシール性が悪いという問題がある。ここで基油として
用いる鉱油の例としては、パラフィン基系原油，中間基
系原油あるいはナフテン基系原油を常圧蒸留するかある
いは常圧蒸留の残渣油を減圧蒸留して得られる留出油、
またはこれを常法にしたがって精製することによって得
られる精製油、例えば溶剤精製油，水添精製油，脱ロウ
処理油，白土処理油等をあげることができる。
また、合成油としてはアルキルベンゼン，アルキルジ
フェニル，ポリα−オレフィン，エステル（ヒンダード
エステル，二塩基酸エステル，ポリオールエステル，リ
ン酸エステル），ポリエーテル（ポリフェニルエーテ
ル，ポリグリコールエーテル），シリコーンオイルなど
がある。
本発明の基油としては、上記の鉱油あるいは合成油を
用いることができるが、難溶性冷媒に対する溶解性（安
定性）を考慮すると、合成油を用いることが好ましく、
特にアルキルベンゼン，アルキルジフェニル，エステ
ル，ポリエーテルが好ましい。
本発明の組成物は、上記基油に前記一般式（Ｉ）で表
わされるフッ素化合物を添加する。ここで一般式（Ｉ）
で表わされるフッ素化合物としては、各種のものがある
が、一般式（Ｉ）中におけるR1,R2はそれぞれ炭素数１
〜20のアルキル基，炭素数６〜30のアリール基、炭素数
６〜30のシクロアルキル基，炭素数１〜20のフッ素置換
アルキル基，炭素数６〜30のフッ素置換アリール基ある
いは炭素数６〜30のフッ素置換シクロアルキル基を示
す。またR3〜R6はそれぞれ炭素数１〜20のフッ素置換ア
ルキル基，炭素数６〜30のフッ素置換アリール基あるい
は炭素数６〜30のフッ素置換シクロアルキル基を示す
が、好ましくは炭素数１〜４のフッ素置換アルキル基で
ある。ｍは１〜100、好ましくは３〜50のいずれかの数
を示す。
この一般式（Ｉ）の化合物の具体例としては、式 で表わされるポリフルオロアルキルシロキサンをあげる
ことができ、このような化合物の市販品としては、上記
式（Ｉ′）（但し、ｍは約10〜30）のポリフルオロアル
キルシロキサン（信越シリコーン（株）製,FL−100）を
充当すればよい。
本発明の組成物では、基油に対して上記一般式（Ｉ）
のフッ素化合物を0.0005〜50重量％、好ましくは0.001
〜30重量％、さらに好ましくは0.01〜10重量％の割合で
配合する。配合割合が0.0005重量％未満では、潤滑性の
向上効果がほとんど認められず、また50重量％を超える
と基油中にフッ素化合物が均一に分散しないなどの問題
が生ずる。
本発明の組成物では、さらに必要に応じて摩耗防止
剤，塩素捕捉剤，酸化防止剤，金属不活性化剤，消泡剤
等を適量配合すことも有効である。
〔実施例〕
次に、本発明を実施例および比較例により更に詳しく
説明する。
実施例１〜８および比較例１〜６ 第１表に示す鉱油，ポリα−オレフィン，アルキルベ
ンゼン，ヒンダードエステルあるいはポリグリコールを
基油とし、またフッ素化合物として一般式（Ｉ′）のフ
ッ素化シリコーン（式中のｍは約12（平均値）であり、
40℃の動粘度80cSt,粘度指数210）を用いて組成物を調
製し、下記の方法にしたがってその性能評価を行った。
結果を第2,3表に示す。
ファレックス焼付試験 ASTM Ｄ 3233に準拠し、焼付荷重（ポンド）で評価
した。
シールドチューブ試験 試料とフロン−22との2:1（重量）混合物を鉄，銅，
アルミニウムの触媒とともに、ガラス管に封入し、175
℃において720時間加熱後、その外観ならびに析出物の
有無を測定した。
第2,3表からわかるように、比較例では焼付荷重が小
さく、またシールドチューブ試験でも析出物が生じた。
これに対して、実施例では焼付荷重も大きく、耐熱性に
もすぐれている。
実施例９〜13 フッ素化合物として、式（Ｉ′）の化合物に代えて第
４表に示す化合物（式中のｍは約12（平均値））を用い
た以外は、実施例５と同様にして組成物を調製し、性能
評価を行った。結果を第４表に示す。
〔発明の効果〕 以上の如く、本発明の冷凍機油組成物は、各種の冷媒
に安定であり、特に一般に難溶性冷媒とされる冷媒に対
しても、相溶性が良好であり安定性にすぐれている。ま
た耐焼付性が高く、蒸発による油消費量も少なく、油循
環量も少なくすることができる。
したがって、本発明の冷凍機油組成物は、各種のフロ
ン化合物等を冷媒として用いる冷凍機，クーラー（特に
カーエアコン），ヒートポンプ等の潤滑剤として有効に
利用される。
───────────────────────────────────────────────────── フロントページの続き (51)Int.Cl.6 識別記号 庁内整理番号 ＦＩ 技術表示箇所 Ｃ１０Ｍ 155:02 105:06 107:12 105:32 105:74 107:34） (Ｃ１０Ｍ 169/04 139:04 105:06 107:12 105:74 107:34） Ｃ１０Ｎ 20:02 40:25

Claims (1)

    (57)【特許請求の範囲】
  1. 【請求項１】鉱油及び／又は合成油からなる基油に、 一般式 〔式中、R1,R2はそれぞれ炭素数１〜20のアルキル基，
    炭素数６〜30のアリール基、炭素数６〜30のシクロアル
    キル基，炭素数１〜20のフッ素置換アルキル基，炭素数
    ６〜30のフッ素置換アリール基あるいは炭素数６〜30の
    フッ素置換シクロアルキル基を示し、R3〜R6はそれぞれ
    炭素数１〜20のフッ素置換アルキル基，炭素数６〜30の
    フッ素置換アリール基あるいは炭素数６〜30のフッ素置
    換シクロアルキル基を示す。また、ｍは１〜100のいず
    れかの数を示す。〕 で表わされるフッ素化合物を0.01〜50重量％の割合で配
    合することを特徴とする冷凍機油組成物。
JP62312357A 1987-12-11 1987-12-11 冷凍機油組成物 Expired - Lifetime JP2543919B2 (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP62312357A JP2543919B2 (ja) 1987-12-11 1987-12-11 冷凍機油組成物
US07/280,959 US4946611A (en) 1987-12-11 1988-12-07 Refrigerator oil containing fluorinated siloxane compounds
KR1019880016614A KR930010532B1 (ko) 1987-12-11 1988-12-12 냉동기유

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP62312357A JP2543919B2 (ja) 1987-12-11 1987-12-11 冷凍機油組成物

Publications (2)

Publication Number Publication Date
JPH01153792A JPH01153792A (ja) 1989-06-15
JP2543919B2 true JP2543919B2 (ja) 1996-10-16

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ID=18028273

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Country Link
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JP (1) JP2543919B2 (ja)
KR (1) KR930010532B1 (ja)

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JP2020158786A (ja) * 2014-07-04 2020-10-01 Ｅｎｅｏｓ株式会社 耐摩耗添加剤、冷凍機油及び冷凍機用作動流体組成物
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JPH01153792A (ja) 1989-06-15
US4946611A (en) 1990-08-07
KR930010532B1 (ko) 1993-10-25
KR890010171A (ko) 1989-08-07

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