JP2022166190A5 - - Google Patents

Info

Publication number

JP2022166190A5

JP2022166190A5 JP2022129635A JP2022129635A JP2022166190A5 JP 2022166190 A5 JP2022166190 A5 JP 2022166190A5 JP 2022129635 A JP2022129635 A JP 2022129635A JP 2022129635 A JP2022129635 A JP 2022129635A JP 2022166190 A5 JP2022166190 A5 JP 2022166190A5

Authority

JP

Japan

Prior art keywords

rebaudioside

product

crude product

supersaturation

degree

Prior art date

2022-08-16

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Granted

Links

• Espacenet
• Global Dossier
• Discuss

• RPYRMTHVSUWHSV-CUZJHZIBSA-N rebaudioside D Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O RPYRMTHVSUWHSV-CUZJHZIBSA-N 0.000 claims 28
• 238000004519 manufacturing process Methods 0.000 claims 13
• 239000012043 crude product Substances 0.000 claims 8
• 239000000047 product Substances 0.000 claims 8
• 239000001512 FEMA 4601 Substances 0.000 claims 6
• OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 6
• HELXLJCILKEWJH-SEAGSNCFSA-N Rebaudioside A Natural products O=C(O[C@H]1[C@@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1)[C@@]1(C)[C@@H]2[C@](C)([C@H]3[C@@]4(CC(=C)[C@@](O[C@H]5[C@H](O[C@H]6[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O6)[C@@H](O[C@H]6[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O6)[C@H](O)[C@@H](CO)O5)(C4)CC3)CC2)CCC1 HELXLJCILKEWJH-SEAGSNCFSA-N 0.000 claims 6
• HELXLJCILKEWJH-UHFFFAOYSA-N entered according to Sigma 01432 Natural products C1CC2C3(C)CCCC(C)(C(=O)OC4C(C(O)C(O)C(CO)O4)O)C3CCC2(C2)CC(=C)C21OC(C1OC2C(C(O)C(O)C(CO)O2)O)OC(CO)C(O)C1OC1OC(CO)C(O)C(O)C1O HELXLJCILKEWJH-UHFFFAOYSA-N 0.000 claims 6
• HELXLJCILKEWJH-NCGAPWICSA-N rebaudioside A Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O HELXLJCILKEWJH-NCGAPWICSA-N 0.000 claims 6
• 235000019203 rebaudioside A Nutrition 0.000 claims 6
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 4
• 238000002425 crystallisation Methods 0.000 claims 3
• 230000008025 crystallization Effects 0.000 claims 3
• 238000000034 method Methods 0.000 claims 3
• 241000544066 Stevia Species 0.000 claims 2
• 238000001816 cooling Methods 0.000 claims 2
• 239000011549 crystallization solution Substances 0.000 claims 2
• 238000002156 mixing Methods 0.000 claims 2
• 238000007670 refining Methods 0.000 claims 2
• 239000000243 solution Substances 0.000 claims 2
• 239000002904 solvent Substances 0.000 claims 2
• 238000003756 stirring Methods 0.000 claims 2
• 239000004383 Steviol glycoside Substances 0.000 claims 1
• 235000013361 beverage Nutrition 0.000 claims 1
• 239000013078 crystal Substances 0.000 claims 1
• 239000000463 material Substances 0.000 claims 1
• 238000000746 purification Methods 0.000 claims 1
• 229930182488 steviol glycoside Natural products 0.000 claims 1
• 235000019411 steviol glycoside Nutrition 0.000 claims 1
• 150000008144 steviol glycosides Chemical class 0.000 claims 1
• 235000019202 steviosides Nutrition 0.000 claims 1