JP2020089302A - ポリフェノール類を含有する沈殿が抑制された液状組成物 - Google Patents
ポリフェノール類を含有する沈殿が抑制された液状組成物 Download PDFInfo
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- JP2020089302A JP2020089302A JP2018228161A JP2018228161A JP2020089302A JP 2020089302 A JP2020089302 A JP 2020089302A JP 2018228161 A JP2018228161 A JP 2018228161A JP 2018228161 A JP2018228161 A JP 2018228161A JP 2020089302 A JP2020089302 A JP 2020089302A
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Abstract
Description
項1.
ポリフェノール類、及び、沈殿を抑制するために有効な量のガティガム及び/又はアラビアガムを含有する、液状組成物。
項2.
前記ポリフェノール類が、植物抽出物に由来する、項1に記載の液状組成物。
項3.
前記植物抽出物由来の可溶性固形分が、0.35〜3質量%である、項2に記載の液状組成物。
項4.
前記ポリフェノール類の総含有量が0.05〜1.5質量%である、項1〜3のいずれか一項に記載の液状組成物。
項5.
ガティガム及びアラビアガムの総含有量が、1〜1000ppmである、項1〜4のいずれか一項に記載の液状組成物。
項6.
ガティガム及び/又はアラビアガムを含有する組成物を含有させることを含む、ポリフェノール類を含有する液状組成物の沈殿抑制方法。
項7.
ガティガム及び/又はアラビアガムを含有することを特徴とする、ポリフェノール類を含有する液状組成物の沈殿抑制用組成物。
項8.
さらに油性成分及び/又は油溶性香料を含有し、乳化物である、項7に記載の沈殿抑制用組成物。
項9.
乳化粒子のメジアン径が1μm以下である、項8に記載の沈殿抑制用組成物。
本発明の液状組成物は、ポリフェノール類、及び沈殿を抑制するために有効な量のガティガム及び/又はアラビアガムを含有する。
本発明の液状組成物は、ポリフェノール類を含有する。ポリフェノール類としては、例えば、カテキン類(カテキン、ガロカテキン、エピカテキン、エピガロカテキン、カテキンガレート、ガロカテキンガレート、エピカテキンガレート、エピガロカテキンガレート等);カテキン類重合体;フラボノール類(ケルセチン、ミリセチン、ケンフェロール等)及びその配糖体;フラボン類(アビゲニン、クリシン、ルテオリン等);イソフラボン類(ダイゼイン、ゲニステイン等)及びその配糖体;フラバノン類(ナリンゲニン、へスペレチン等)及びその配糖体;アントシアニジン類(シアニジン、デルフィニジン、ペラルゴニジン等)及びその配糖体;カルコン類;クルクミン類;リグナン類;クマリン類;フェニルカルボン酸類等を挙げることができる。即ち、ポリフェノール類には、非重合体のカテキン類とカテキン類重合物を包含する概念である「タンニン」が包含される。本発明の液状組成物には、これらのポリフェノール類が、1種単独で含有されても、2種以上が含有されていてもよいが、カテキン類及びカテキン類重合体から選択される1種以上の成分が含有されることがより好ましい。
本発明の液状組成物に用いられるガティガムは、シクンシ科ガティノキ(Anogeissus Latifolia)の樹液(分泌液)に由来する多糖類であり、増粘安定剤(食品添加物)として公知の多糖類である。本発明で使用するガティガムは商業的に入手可能であり、例えば、三栄源エフ・エフ・アイ株式会社の「ガティガムRD」を挙げることができる。
ム)であってもよい。低分子ガティガムの重量平均分子量は、限定はされないが、例えば
、0.020×106〜1.10×106とすることができる。なお、ガティガムの分子量の測定は、国際公開第2018/062554号公報に記載される、ゲル濾過クロマトグラフィー(GPC)を用いた方法により行われる。
また、アラビアガム及びガティガムの総含有量は、特に限定されないが、粘度を低く保つ観点から、液状組成物の全量に対して、好ましくは1000ppm以下、より好ましくは900ppm以下、更に好ましくは800ppm以下、特に好ましくは700ppm以下、最も好ましくは600ppm以下である。
本発明の液状組成物において、ガティガム及びアラビアガムの総含有量1質量部に対するポリフェノール類の総含有量は、特に限定されないが、本発明の効果を顕著に奏する観点から、好ましくは0.1〜15000質量部、より好ましくは1〜5000質量部、更に好ましくは5〜1000質量部、特に好ましくは10〜500質量部である。
本発明の液状組成物には、本発明の効果を損なわない限りにおいて、ポリフェノール類、ガティガム、及びアラビアガム以外の、飲料に用いられ得る公知の栄養成分(アミノ酸類、ビタミン類、ミネラル等);アルコール;酒類;塩類(食塩、塩化マグネシウム、酸性リン酸カリウム、酸性リン酸カルシウム、リン酸アンモニウム、硫酸マグネシウム、硫酸カルシウム、メタ重亜硫酸カリウム、塩化カルシウム、硝酸カリウム、硫酸アンモニウム等);呈味成分(塩味、うま味等を含む);果汁(濃縮物を含む);果肉;野菜;野菜汁(濃縮物を含む);ピューレ;エキス;甘味料(果糖ぶどう糖液糖、グルコース、スクロース、フルクトース、ガラクトース、マルトース、マンノース、ラクトース、ハチミツ、水飴等);糖アルコール(ソルビトール、キシリトール、マルチトール、還元パラチノース、ラクチトール等);高感度甘味料(スクラロース、アセスルファムK、アスパルテーム、ネオテーム、サッカリン、サッカリンナトリウム、ソーマチン、ステビア、グリチルリチン、モネリン、アリテーム、グリチルリチン酸二ナトリウム等);苦味料(イソ−α酸、ローホップ、ヘキサホップ、テトラホップ等);酸味料(リン酸、乳酸、グルコン酸カリウム、DL−リンゴ酸ナトリウム、クエン酸、アジピン酸、クエン酸三ナトリウム、グルコノデルタラクトン、グルコン酸、グルコン酸ナトリウム、コハク酸、コハク酸一ナトリウム、コハク酸二ナトリウム、酢酸ナトリウム、DL−酒石酸、L−酒石酸、DL−酒石酸ナトリウム、L−酒石酸ナトリウム、乳酸ナトリウム、氷酢酸、フマル酸、フマル酸一ナトリウム、DL−リンゴ酸等);香料;着色料(ベニバナ黄色素、カラメル色素、クチナシ色素、アントシアニン、果汁色素、野菜色素、合成色素等);食品添加物(食物繊維、乳化剤(ショ糖脂肪酸エステル、グリセリン脂肪酸エステル、レシチン、ポリソルベート、キラヤサポニン等)、ショ糖酢酸イソ酪酸エステル、多価アルコール(プロピレングリコール、グリセリン等)、pH調整剤、保存料、酸化防止剤(ビタミンC、ビタミンE、抽出トコフェロール等)、増粘剤、安定化剤、糊料等);医薬品、医薬部外品又は化粧品の有効成分又は添加剤、等を1種以上含有することができる。
本発明の液状組成物のpHは、特に限定されないが、風味を良好とする観点から、好ましくは2.0〜8.0、より好ましくは3.0〜7.5、更に好ましくは3.5〜7.0、特に好ましくは4.0〜7.0、最も好ましくは4.6〜6.5である。
本発明の液状組成物は、特に限定されず、食品、医薬品、医薬部外品、又は化粧品としてそのまま使用されるものであってもよく、あるいはこれらの製造に用いられてもよいが、例えば、還元濃縮飲料組成物等として、飲料の製造に用いることが好ましい。
本発明の液状組成物の容器は、特に限定されない。飲料としてそのまま供される場合は、例えば、瓶、アルミ缶、スチール缶、ボトル缶、PETボトル、紙パック(ゲーブルトップ、LL容器等)等に充填される。また、飲料の製造用途で供される場合は、上記の容器形態の他、例えば、一斗缶、ドラム缶等に充填される。さらに消費者又は飲食品の提供者が希釈して用いる用途で供される場合は、飲料と同様の容器形態のほか、プラスチックや紙等を材料とするポーションタイプのカートリッジ、アルミパウチ(スティック形状等)、ドレッシング容器やソース容器のようなキャップ付き狭口ボトル等に充填される。
本発明の液状組成物の保存温度は、特に限定されず、例えば40℃以下、30℃以下、25℃以下、20℃以下、15℃以下、10℃以下、8℃以下、5℃以下とすることができるが、本発明の効果を顕著に奏する観点から、好ましくは20℃以下であり、より好ましくは15℃以下であり、更に好ましくは10℃以下であり、特に好ましくは8℃以下であり、最も好ましくは5℃以下である。
本発明の液状組成物の製造方法は、ポリフェノール類、並びに沈殿を抑制するために有効な量のガティガム及び/又はアラビアガムを含有させる工程を含む。
本発明の沈殿抑制方法は、ポリフェノール類を含有する液状組成物に用いられるものであって、ガティガム及び/又はアラビアガムを含有する組成物を含有させることを含む。
本発明のポリフェノール類を含有する液状組成物の沈殿抑制用組成物は、ガティガム及び/又はアラビアガムを含有する。
本発明の沈殿抑制用組成物が乳化物である場合、沈殿抑制用組成物は、油性成分及び/又は油溶性香料をさらに含む。この場合の乳化物は、油性成分及び/又は油溶性香料が水相に対して乳化して得られるO/W型の乳化物が好ましい。
本発明の沈殿抑制用組成物のうち、固体形状の態様においては、さらに賦形剤を含有することが好ましい。賦形剤としては、例えば、澱粉分解物(デキストリン、粉飴等)、糖類(単糖(グルコース、フルクトース等)、二糖(例えば、ショ糖、乳糖、麦芽糖、トレハロース等)、オリゴ糖(セロオリゴ糖、マルトオリゴ糖、フラクトオリゴ糖等)、糖アルコール(キシリトール、ソルビトール、ラクチトール、マルチトール等)、還元糖化物等)、食物繊維(例えば、難消化性デキストリン、ポリデキストロース、グァーガム酵素分解物等)等が挙げられる。係る態様において、賦形剤の含有量は、特に限定されないが、沈殿抑制用組成物の全量に対して、例えば、1〜95質量%が挙げられ、好ましくは5〜95質量%、より好ましくは10〜90質量%、更に好ましくは20〜90質量%、特に好ましくは30〜90質量%である。
さらに、本発明の沈殿抑制用組成物には、その態様にかかわらず、その他成分として、本発明の効果を損なわない限りにおいて、ガティガム、アラビアガム、油性成分、油溶性香料、多価アルコール、乳化剤、及び賦形剤以外に、食品、医薬品、医薬部外品、又は化粧品に用いられ得る公知の栄養成分、アルコール、酒類、塩類、呈味成分、果汁、果肉、野菜、野菜汁、ピューレ、エキス、甘味料、糖アルコール、高感度甘味料、苦味料、酸味料、香料、着色料、食品添加物(食物繊維、pH調整剤、保存料、酸化防止剤、増粘剤、安定化剤等)、医薬品又は医薬部外品の有効成分又は添加剤、等を1種以上配合することができる。これらの成分の具体例は上記の[液状組成物]の項で記載したとおりである。
紅茶用フレーバーとしてコウチャフレーバーコンパウンド(*)、ガティガムとしてGATIFOLIA RD(*)、アラビアガムとしてアラビアガム SD(*)、カラギナン(κカラギナン)としてCSK−1(F)(*)、抽出トコフェロールとしてトコフェロール 70(s)(日清オイリオグループ社製)、食用油脂としてO.D.O(日清オイリオグループ社製)を以下の試験で用いた。
まず、紅茶エキスパウダー(DAMIN FOODSTUFF(ZANG ZHOU)社製、ポリフェノール類含有率約36質量%)を2kg、砂糖14kgを水に溶解し、100.0Lに調整した後で、85℃で30分間加熱殺菌することによって、紅茶シロップを調製した。このとき、紅茶シロップのpHは5.0、Brixは15.7°、比重は1.054、茶固形分は1.9質量%、ポリフェノール類は約0.72質量%であった。
<沈殿量の評価基準>(堆積した沈殿の厚さを目安として目視でスコアを決定)
スコア0:沈殿を認めない(沈殿厚さ0mm)
スコア1:沈殿を少量認める(沈殿厚さ0.1mm未満)
スコア2:沈殿がやや多い(沈殿厚さ0.1mm以上0.5mm未満)
スコア3:沈殿が多い(沈殿厚さ0.5mm以上1.0mm未満)
スコア4:沈殿が非常に多い(沈殿厚さ1.0mm以上)
表4、5の処方の乳化組成物を調製した。それぞれ、まず油溶性香料である紅茶用フレーバーと油性成分である食用油脂、抽出トコフェロール、ショ糖酢酸イソ酪酸エステルを均一に混合して油性溶液を得た。続いて、残りの原材料を水に溶解して調製した水溶液に、得られた油性溶液を添加して攪拌混合した。得られた混合物を高圧ホモジナイザー(APV Gaulin社製高圧ホモジナイザー15MR-8TA)を用いて、圧力350kg/cm2で4回乳化処理を行い、ガティガムを含有する乳化組成物(実施例2−1、表4)、アラビアガムを含有する乳化組成物(実施例2−2、表5)が得られた。
試験例2で得られたガティガム含有乳化組成物(実施例2−1)、アラビアガム含有乳化組成物(実施例2−2)、ガティガム含有粉末組成物(実施例2−3)を、試験例1と同じ紅茶シロップに、それぞれ終濃度で1000ppmとなるように添加したものを調製し、それぞれ実施例3−1〜3とした。即ち、実施例3−1、3−3にはガティガムが40ppm、実施例3−2にはアラビアガムが240ppm含まれる。
Claims (9)
- ポリフェノール類、及び、沈殿を抑制するために有効な量のガティガム及び/又はアラビアガムを含有する、液状組成物。
- 前記ポリフェノール類が、植物抽出物に由来する、請求項1に記載の液状組成物。
- 前記植物抽出物由来の可溶性固形分が、0.35〜3質量%である、請求項2に記載の液状組成物。
- 前記ポリフェノール類の総含有量が0.05〜1.5質量%である、請求項1〜3のいずれか一項に記載の液状組成物。
- ガティガム及びアラビアガムの総含有量が、1〜1000ppmである、請求項1〜4のいずれか一項に記載の液状組成物。
- ガティガム及び/又はアラビアガムを含有する組成物を含有させることを含む、ポリフェノール類を含有する液状組成物の沈殿抑制方法。
- ガティガム及び/又はアラビアガムを含有することを特徴とする、ポリフェノール類を含有する液状組成物の沈殿抑制用組成物。
- さらに油性成分及び/又は油溶性香料を含有し、乳化物である、請求項7に記載の沈殿抑制用組成物。
- 乳化粒子のメジアン径が1μm以下である、請求項8に記載の沈殿抑制用組成物。
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