JP2018524376A5 - - Google Patents
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- JP2018524376A5 JP2018524376A5 JP2018502143A JP2018502143A JP2018524376A5 JP 2018524376 A5 JP2018524376 A5 JP 2018524376A5 JP 2018502143 A JP2018502143 A JP 2018502143A JP 2018502143 A JP2018502143 A JP 2018502143A JP 2018524376 A5 JP2018524376 A5 JP 2018524376A5
- Authority
- JP
- Japan
- Prior art keywords
- process according
- composition
- reaction
- product stream
- dehydrofluorination
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000000203 mixture Substances 0.000 claims description 16
- FXRLMCRCYDHQFW-UHFFFAOYSA-N 2,3,3,3-tetrafluoropropene Chemical compound FC(=C)C(F)(F)F FXRLMCRCYDHQFW-UHFFFAOYSA-N 0.000 claims description 13
- 238000004821 distillation Methods 0.000 claims description 9
- 238000000746 purification Methods 0.000 claims description 7
- 238000005201 scrubbing Methods 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 claims 21
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims 10
- 229910000040 hydrogen fluoride Inorganic materials 0.000 claims 9
- 238000006243 chemical reaction Methods 0.000 claims 7
- 238000005796 dehydrofluorination reaction Methods 0.000 claims 7
- 238000007033 dehydrochlorination reaction Methods 0.000 claims 4
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 3
- 239000003054 catalyst Substances 0.000 claims 3
- QDOXWKRWXJOMAK-UHFFFAOYSA-N dichromium trioxide Chemical compound O=[Cr]O[Cr]=O QDOXWKRWXJOMAK-UHFFFAOYSA-N 0.000 claims 3
- 229910052725 zinc Inorganic materials 0.000 claims 3
- 239000011701 zinc Substances 0.000 claims 3
- 238000005191 phase separation Methods 0.000 claims 2
- FDOPVENYMZRARC-UHFFFAOYSA-N 1,1,1,2,2-pentafluoropropane Chemical compound CC(F)(F)C(F)(F)F FDOPVENYMZRARC-UHFFFAOYSA-N 0.000 claims 1
- OQISUJXQFPPARX-UHFFFAOYSA-N 2-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)C(Cl)=C OQISUJXQFPPARX-UHFFFAOYSA-N 0.000 claims 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
- 230000003197 catalytic effect Effects 0.000 claims 1
- 229910052804 chromium Inorganic materials 0.000 claims 1
- 239000011651 chromium Substances 0.000 claims 1
- 238000001035 drying Methods 0.000 claims 1
- 238000003682 fluorination reaction Methods 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 238000004064 recycling Methods 0.000 claims 1
- 239000012808 vapor phase Substances 0.000 claims 1
- 238000009835 boiling Methods 0.000 description 5
- 239000012535 impurity Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1512593.3 | 2015-07-17 | ||
| GB1512593.3A GB2540427B (en) | 2015-07-17 | 2015-07-17 | Process for the preparation of 2,3,3,3-tetrafluoropropene (1234yf) |
| PCT/GB2016/052145 WO2017013406A1 (en) | 2015-07-17 | 2016-07-14 | Process for the preparation of 2,3,3,3-tetrafluoropropene (1234yf) |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2018524376A JP2018524376A (ja) | 2018-08-30 |
| JP2018524376A5 true JP2018524376A5 (cg-RX-API-DMAC7.html) | 2019-12-26 |
| JP6688383B2 JP6688383B2 (ja) | 2020-04-28 |
Family
ID=54013203
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2018502143A Active JP6688383B2 (ja) | 2015-07-17 | 2016-07-14 | ２，３，３，３−テトラフルオロプロペン（１２３４ｙｆ）の調製プロセス |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US10899686B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP3325435B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JP6688383B2 (cg-RX-API-DMAC7.html) |
| KR (1) | KR102676107B1 (cg-RX-API-DMAC7.html) |
| CN (1) | CN107848916B (cg-RX-API-DMAC7.html) |
| ES (1) | ES2864023T3 (cg-RX-API-DMAC7.html) |
| GB (1) | GB2540427B (cg-RX-API-DMAC7.html) |
| WO (1) | WO2017013406A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP6115550B2 (ja) | 2014-11-17 | 2017-04-19 | ダイキン工業株式会社 | ＨＦＣ−２４５ｃｂと（Ｅ）−ＨＦＯ−１２３４ｚｅとを含有する組成物から両化合物を分離する方法 |
| GB201712775D0 (en) * | 2017-08-09 | 2017-09-20 | Mexichem Fluor Sa De Cv | Compositions and uses thereof |
| US10233137B1 (en) * | 2017-10-13 | 2019-03-19 | Honeywell International Inc. | Method for removing unsaturated halogenated impurities from 2,3,3,3-tetrafluoropropene (HFO-1234yf) |
| BR112021022059A2 (pt) | 2018-10-26 | 2021-12-28 | Chemours Co Fc Llc | Composições de fluoropropeno, métodos de produção de uma mistura e de resfriamento, processos para transferência de calor, para tratamento de uma superfície e para formação de uma composição, sistema de refrigeração, aparelhos de refrigeração, uso da composição de fluoropropeno e método para substituição de um refrigerante |
| US11209196B2 (en) | 2018-10-26 | 2021-12-28 | The Chemours Company Fc, Llc | HFO-1234ZE, HFO-1225ZC and HFO-1234YF compositions and processes for producing and using the compositions |
| CN109438170B (zh) * | 2018-11-27 | 2022-02-01 | 浙江三美化工股份有限公司 | 一种2，3，3，3-四氟丙烯的制备方法 |
| GB2582364A (en) * | 2019-03-21 | 2020-09-23 | Mexichem Fluor Sa De Cv | Methods |
| JP7287965B2 (ja) | 2019-11-13 | 2023-06-06 | フジアン ヨンジン テクノロジー カンパニー リミテッド | ２，３，３，３－テトラフルオロプロペン（１２３４ｙｆ）および２，３－ジクロロ－１，１，１－トリフルオロプロパン（２４３ｄｂ）の新しい合成方法 |
Family Cites Families (48)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9104775D0 (en) | 1991-03-07 | 1991-04-17 | Ici Plc | Fluorination catalyst and process |
| FR2740994B1 (fr) | 1995-11-10 | 1997-12-05 | Atochem Elf Sa | Catalyseurs massiques a base d'oxyde de chrome, leur procede de preparation et leur application a la fluoration d'hydrocarbures halogenes |
| US6403524B2 (en) | 1996-09-10 | 2002-06-11 | Imperial Chemical Industries Plc | Fluorination catalyst and process |
| TW499363B (en) | 1998-06-26 | 2002-08-21 | Sinco Ricerche Spa | Recyclable multi-layer material in polyester resin |
| US8058486B2 (en) | 2004-04-29 | 2011-11-15 | Honeywell International Inc. | Integrated process to produce 2,3,3,3-tetrafluoropropene |
| US7897823B2 (en) | 2004-10-29 | 2011-03-01 | E. I. Du Pont De Nemours And Company | Process for production of azeotrope compositions comprising hydrofluoroolefin and hydrogen fluoride and uses of said azeotrope compositions in separation processes |
| GB0507139D0 (en) | 2005-04-08 | 2005-05-18 | Ineos Fluor Holdings Ltd | Catalyst |
| US7476771B2 (en) | 2005-11-01 | 2009-01-13 | E.I. Du Pont De Nemours + Company | Azeotrope compositions comprising 2,3,3,3-tetrafluoropropene and hydrogen fluoride and uses thereof |
| US7560602B2 (en) | 2005-11-03 | 2009-07-14 | Honeywell International Inc. | Process for manufacture of fluorinated olefins |
| EP2546220A3 (en) | 2006-01-03 | 2013-05-08 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
| CN101395109B (zh) | 2006-01-03 | 2013-09-18 | 霍尼韦尔国际公司 | 制备氟化有机化合物的方法 |
| JP5764291B2 (ja) | 2006-07-13 | 2015-08-19 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーＥ．Ｉ．Ｄｕ Ｐｏｎｔ Ｄｅ Ｎｅｍｏｕｒｓ Ａｎｄ Ｃｏｍｐａｎｙ | テトラフルオロプロペンおよびペンタフルオロプロペンを製造するための触媒製造方法 |
| GB0806422D0 (en) * | 2008-04-09 | 2008-05-14 | Ineos Fluor Holdings Ltd | Process |
| EP2129644B1 (en) | 2006-10-03 | 2020-07-01 | Mexichem Fluor S.A. de C.V. | Dehydrogenationhalogenation process for the production of c3-c6-(hydro)fluoroalkenes |
| USRE49849E1 (en) | 2006-10-31 | 2024-02-27 | The Chemours Company Fc, Llc | Processes for the production of fluoropropanes and halopropenes |
| US8398882B2 (en) | 2006-10-31 | 2013-03-19 | E I Du Pont De Nemours And Company | Processes for the production of fluoropropanes and halopropenes and azeotropic compositions of 2-chloro-3,3,3-trifluoro-1-propene with HF and of 1,1,1,2,2-pentafluoropropane with HF |
| GB0625214D0 (en) | 2006-12-19 | 2007-01-24 | Ineos Fluor Holdings Ltd | Process |
| US8563789B2 (en) | 2007-06-27 | 2013-10-22 | Arkema Inc. | Process for the manufacture of hydrofluoroolefins |
| CN101687732A (zh) | 2007-06-27 | 2010-03-31 | 阿科玛股份有限公司 | 用于制造氢氟烯烃的两步法 |
| WO2009003084A1 (en) | 2007-06-27 | 2008-12-31 | Arkema Inc. | Process for the manufacture of hydrofluoroolefins |
| US9035111B2 (en) * | 2007-08-22 | 2015-05-19 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
| CN101952230B (zh) | 2008-02-21 | 2015-07-22 | 纳幕尔杜邦公司 | 通过共沸蒸馏使2,3,3,3-四氟丙烯与氟化氢分离的方法 |
| FR2933402B1 (fr) | 2008-07-03 | 2010-07-30 | Arkema France | Procede de purification de 2,3,3,3-tetrafluoro-1-propene (hfo1234yf) |
| WO2010059493A1 (en) * | 2008-11-19 | 2010-05-27 | Arkema Inc. | Process for the manufacture of hydrofluoroolefins |
| GB0906191D0 (en) | 2009-04-09 | 2009-05-20 | Ineos Fluor Holdings Ltd | Process |
| ES2598484T3 (es) * | 2009-04-23 | 2017-01-27 | Daikin Industries, Ltd. | Procedimiento para la preparación de 2,3,3,3-tetrafluoropropeno |
| HUE031899T2 (en) | 2009-12-23 | 2017-08-28 | Arkema France | Catalytic gas phase fluorination of 1233XF to 1234YF |
| WO2011077191A1 (en) | 2009-12-23 | 2011-06-30 | Arkema France | Catalytic gas phase fluorination of 1230xa to 1234yf |
| PL2516367T3 (pl) | 2009-12-23 | 2016-08-31 | Arkema France | Katalityczne fluorowanie w fazie gazowej 243db do 1234yf |
| CN102753506A (zh) | 2010-02-12 | 2012-10-24 | 大金工业株式会社 | 用于制备含氟烯烃的方法 |
| JP5569589B2 (ja) * | 2010-02-12 | 2014-08-13 | ダイキン工業株式会社 | 含フッ素アルケン化合物の製造方法 |
| US8927791B2 (en) | 2010-04-29 | 2015-01-06 | Honeywell International Inc. | Method for producing tetrafluoropropenes |
| CN102884031B (zh) | 2010-05-03 | 2016-04-06 | 阿科玛股份有限公司 | 用于形成四氟烯烃的五氟烷的脱氟化氢作用 |
| EP3363776B1 (en) | 2010-10-22 | 2020-01-01 | Arkema France | Process for the preparation of 2,3,3,3-tetrafluoropropene |
| WO2012057367A1 (en) | 2010-10-27 | 2012-05-03 | Daikin Industries, Ltd. | Process for producing 2,3,3,3-tetrafluoropropene |
| US9890096B2 (en) | 2011-01-19 | 2018-02-13 | Honeywell International Inc. | Methods of making 2,3,3,3-tetrafluoro-2-propene |
| MX343621B (es) | 2011-01-21 | 2016-11-11 | Arkema France | Fluoracion catalitica en fase gas. |
| EP2665693B1 (en) | 2011-01-21 | 2017-07-19 | Arkema France | Catalytic gas phase fluorination |
| US8741828B2 (en) | 2011-02-23 | 2014-06-03 | Honeywell International Inc. | Azeotrope and azeotrope-like compositions useful for the production of haloolefins |
| JP5704264B2 (ja) | 2011-07-26 | 2015-04-22 | ダイキン工業株式会社 | ２，３，３，３−テトラフルオロプロペンの製造方法 |
| FR2980474B1 (fr) | 2011-09-27 | 2013-08-30 | Arkema France | Procede de fabrication du 2,3,3,3-tetrafluoropropene |
| JP6518869B2 (ja) | 2011-11-04 | 2019-05-29 | ハネウェル・インターナショナル・インコーポレーテッドＨｏｎｅｙｗｅｌｌ Ｉｎｔｅｒｎａｔｉｏｎａｌ Ｉｎｃ． | ２，３，３，３−テトラフルオロプロペンの製造方法 |
| CN106397103A (zh) | 2011-11-04 | 2017-02-15 | 塞尔马·贝克特什维克 | 用于制造2,3,3,3‑四氟丙烯的方法 |
| US9334208B2 (en) * | 2011-12-14 | 2016-05-10 | Arkema France | Process for the preparation of 2,3,3,3 tetrafluoropropene |
| EP2819978A4 (en) | 2012-02-29 | 2015-11-04 | Honeywell Int Inc | PROCESS FOR PRODUCTION OF 2,3,3,3-TETRAFLUOROPROPENE |
| GB201207666D0 (en) | 2012-05-02 | 2012-06-13 | Mexichem Amanco Holding Sa | Process |
| KR20150021551A (ko) | 2012-06-06 | 2015-03-02 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 플루오로올레핀 중 RfCCX 불순물의 감소 방법 |
| CN103055643A (zh) | 2012-12-11 | 2013-04-24 | 上海巴安水务股份有限公司 | 一种多管微旋流过滤分离器 |
-
2015
- 2015-07-17 GB GB1512593.3A patent/GB2540427B/en active Active
-
2016
- 2016-07-14 US US15/745,505 patent/US10899686B2/en active Active
- 2016-07-14 WO PCT/GB2016/052145 patent/WO2017013406A1/en not_active Ceased
- 2016-07-14 JP JP2018502143A patent/JP6688383B2/ja active Active
- 2016-07-14 ES ES16750478T patent/ES2864023T3/es active Active
- 2016-07-14 KR KR1020187004683A patent/KR102676107B1/ko active Active
- 2016-07-14 EP EP16750478.6A patent/EP3325435B1/en active Active
- 2016-07-14 CN CN201680041643.8A patent/CN107848916B/zh active Active
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