JP2016507545A5 - - Google Patents
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- Publication number
- JP2016507545A5 JP2016507545A5 JP2015556518A JP2015556518A JP2016507545A5 JP 2016507545 A5 JP2016507545 A5 JP 2016507545A5 JP 2015556518 A JP2015556518 A JP 2015556518A JP 2015556518 A JP2015556518 A JP 2015556518A JP 2016507545 A5 JP2016507545 A5 JP 2016507545A5
- Authority
- JP
- Japan
- Prior art keywords
- acid
- alkyl
- hydroxycarboxylic acid
- cyclic ester
- hydroxycarboxylic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 15
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims 8
- -1 cyclic ester Chemical class 0.000 claims 6
- KXDHJXZQYSOELW-UHFFFAOYSA-N Carbamic acid Chemical compound NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 claims 4
- 229910021536 Zeolite Inorganic materials 0.000 claims 4
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 4
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims 4
- 239000010457 zeolite Substances 0.000 claims 4
- 125000000217 alkyl group Chemical group 0.000 claims 3
- 125000000882 C2-C6 alkenyl group Chemical group 0.000 claims 2
- 125000003601 C2-C6 alkynyl group Chemical group 0.000 claims 2
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 claims 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 2
- JVTAAEKCZFNVCJ-REOHCLBHSA-N L-lactic acid Chemical compound C[C@H](O)C(O)=O JVTAAEKCZFNVCJ-REOHCLBHSA-N 0.000 claims 2
- 125000003545 alkoxy group Chemical group 0.000 claims 2
- 125000003118 aryl group Chemical group 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 150000003950 cyclic amides Chemical class 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- 235000014655 lactic acid Nutrition 0.000 claims 2
- 239000004310 lactic acid Substances 0.000 claims 2
- 125000001424 substituent group Chemical group 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 claims 1
- VBWPSWWDYVWZKA-UHFFFAOYSA-N 2-hydroxybut-3-enoic acid Chemical compound C=CC(O)C(O)=O VBWPSWWDYVWZKA-UHFFFAOYSA-N 0.000 claims 1
- AFENDNXGAFYKQO-UHFFFAOYSA-N 2-hydroxybutyric acid Chemical compound CCC(O)C(O)=O AFENDNXGAFYKQO-UHFFFAOYSA-N 0.000 claims 1
- NYHNVHGFPZAZGA-UHFFFAOYSA-N 2-hydroxyhexanoic acid Chemical compound CCCCC(O)C(O)=O NYHNVHGFPZAZGA-UHFFFAOYSA-N 0.000 claims 1
- JJTUDXZGHPGLLC-IMJSIDKUSA-N 4511-42-6 Chemical group C[C@@H]1OC(=O)[C@H](C)OC1=O JJTUDXZGHPGLLC-IMJSIDKUSA-N 0.000 claims 1
- IWHLYPDWHHPVAA-UHFFFAOYSA-N 6-hydroxyhexanoic acid Chemical compound OCCCCCC(O)=O IWHLYPDWHHPVAA-UHFFFAOYSA-N 0.000 claims 1
- 229930182843 D-Lactic acid Natural products 0.000 claims 1
- JVTAAEKCZFNVCJ-UWTATZPHSA-N D-lactic acid Chemical compound C[C@@H](O)C(O)=O JVTAAEKCZFNVCJ-UWTATZPHSA-N 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 230000002378 acidificating effect Effects 0.000 claims 1
- 238000010533 azeotropic distillation Methods 0.000 claims 1
- 229940022769 d- lactic acid Drugs 0.000 claims 1
- 150000002148 esters Chemical class 0.000 claims 1
- JJTUDXZGHPGLLC-UHFFFAOYSA-N lactide Chemical group CC1OC(=O)C(C)OC1=O JJTUDXZGHPGLLC-UHFFFAOYSA-N 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP13154707 | 2013-02-08 | ||
| EP13154707.7 | 2013-02-08 | ||
| PCT/EP2014/052493 WO2014122294A1 (en) | 2013-02-08 | 2014-02-07 | Process for preparing cyclic esters and cyclic amides |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2016507545A JP2016507545A (ja) | 2016-03-10 |
| JP2016507545A5 true JP2016507545A5 (enExample) | 2017-03-16 |
| JP6422893B2 JP6422893B2 (ja) | 2018-11-14 |
Family
ID=47681787
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015556518A Expired - Fee Related JP6422893B2 (ja) | 2013-02-08 | 2014-02-07 | 環状エステルおよび環状アミドの製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US9573924B2 (enExample) |
| EP (1) | EP2941422B1 (enExample) |
| JP (1) | JP6422893B2 (enExample) |
| KR (1) | KR20150115792A (enExample) |
| CN (1) | CN104981464B (enExample) |
| BR (1) | BR112015016103A2 (enExample) |
| EA (1) | EA027829B1 (enExample) |
| ES (1) | ES2628803T3 (enExample) |
| WO (1) | WO2014122294A1 (enExample) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20190020746A (ko) * | 2016-06-20 | 2019-03-04 | 토탈 리서치 앤드 테크놀로지 펠루이 | 용매에 대해 별도의 유입을 이용한 단일 단계 락티드 제조 방법 |
| CN109563068A (zh) * | 2016-06-20 | 2019-04-02 | 道达尔研究技术弗吕公司 | 通过滗析回收水的单步骤丙交酯生产工艺 |
| CN110402246A (zh) | 2017-03-15 | 2019-11-01 | 巴斯夫欧洲公司 | 通过使羟基羧酸或酰胺与酸性BEA(H-β多晶型A)型沸石反应而制备环状二酯或环状二酰胺的方法 |
| CN106831700B (zh) * | 2017-03-28 | 2019-05-24 | 南京大学 | 一种全绿色封闭循环工艺生产光学纯l-/d-丙交酯的方法 |
| JP6952303B2 (ja) * | 2017-08-02 | 2021-10-20 | 日本曹達株式会社 | 環状エステル類の製造方法 |
| US10266512B2 (en) | 2017-08-10 | 2019-04-23 | Novus International, Inc. | Processes for preparing heteroatom containing cyclic dimers |
| WO2020081836A1 (en) | 2018-10-17 | 2020-04-23 | The Regents Of The University Of California | Prodrugs of alpha-ketoglutarate, alpha-ketobutyrate, alpha-ketoisovalerate, and alpha-ketoisohexanoate, and uses thereof |
| WO2022006023A1 (en) * | 2020-06-29 | 2022-01-06 | Zymergen Inc. | Dimers from bioreachable molecules as copolymers |
| CN116113634A (zh) * | 2020-06-29 | 2023-05-12 | 齐默尔根公司 | 模量改性剂及其薄膜 |
| CN111995611A (zh) * | 2020-08-18 | 2020-11-27 | 青岛科技大学 | 一种己内酯的合成工艺 |
| CN114437017A (zh) * | 2020-10-31 | 2022-05-06 | 中国石油化工股份有限公司 | 一种乳酸制备丙交酯的方法 |
| CN112574165B (zh) * | 2020-12-30 | 2022-01-07 | 安徽丰原生物技术股份有限公司 | 一步转化生成丙交酯的方法 |
| EP4134365A1 (en) * | 2021-08-12 | 2023-02-15 | Sulzer Management AG | A plant and an efficient process for producing lactide from lactic acid |
| CN115028615B (zh) * | 2022-07-27 | 2024-01-09 | 万华化学(四川)有限公司 | 一种l,l-丙交酯及其制备方法和应用 |
| CN120004848A (zh) * | 2025-02-17 | 2025-05-16 | 中国科学院长春应用化学研究所 | 一种用分子筛催化剂合成的丙交酯衍生物及其合成方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5326887A (en) * | 1991-02-27 | 1994-07-05 | E. I. Du Pont De Nemours And Company | Process for the preparation of 1,4-dioxane-2,5-diones |
| JPH05138022A (ja) * | 1991-11-22 | 1993-06-01 | Japan Tobacco Inc | ラクトンの製造方法 |
| PT1883665T (pt) * | 2005-04-22 | 2017-11-14 | Univ Geneve | Composições polilactídeo e usos das mesmas |
| KR20100110830A (ko) * | 2007-12-21 | 2010-10-13 | 바스프 에스이 | ε-카프로락톤의 제조 방법 |
| KR101683110B1 (ko) * | 2008-08-29 | 2016-12-07 | 우데 인벤타-피셔 게엠바하 | 락티드 유도체의 혼합물의 생성 방법 |
| KR101154029B1 (ko) * | 2009-05-20 | 2012-06-07 | 한국화학연구원 | 젖산에스테르로부터 락타이드의 직접 전환용 촉매 및 이를 이용한 락타이드의 제조방법 |
| EP2407463A1 (en) * | 2010-07-14 | 2012-01-18 | Solvay SA | Process for the manufacture of a cyclic diester of an apha-hydroxyacid |
| KR101886434B1 (ko) * | 2012-02-29 | 2018-08-07 | 현대자동차주식회사 | 유산으로부터 락타이드의 제조방법 |
| KR101459819B1 (ko) * | 2012-04-04 | 2014-11-07 | 현대자동차주식회사 | 유산염으로부터 락타이드의 제조방법 |
| WO2013160485A1 (de) * | 2012-04-28 | 2013-10-31 | Uhde Inventa-Fischer Gmbh | Verfahren zur kontinuierlichen herstellung von lactid direkt aus konzentrierter milchsäure |
-
2014
- 2014-02-07 EP EP14703824.4A patent/EP2941422B1/en active Active
- 2014-02-07 BR BR112015016103A patent/BR112015016103A2/pt active Search and Examination
- 2014-02-07 EA EA201591022A patent/EA027829B1/ru not_active IP Right Cessation
- 2014-02-07 US US14/765,703 patent/US9573924B2/en active Active
- 2014-02-07 WO PCT/EP2014/052493 patent/WO2014122294A1/en not_active Ceased
- 2014-02-07 JP JP2015556518A patent/JP6422893B2/ja not_active Expired - Fee Related
- 2014-02-07 CN CN201480008213.7A patent/CN104981464B/zh active Active
- 2014-02-07 KR KR1020157021473A patent/KR20150115792A/ko not_active Abandoned
- 2014-02-07 ES ES14703824.4T patent/ES2628803T3/es active Active
-
2017
- 2017-01-05 US US15/399,189 patent/US9862700B2/en active Active
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