JP2015007188A - ポリカーボネートの製造方法 - Google Patents
ポリカーボネートの製造方法 Download PDFInfo
- Publication number
- JP2015007188A JP2015007188A JP2013132910A JP2013132910A JP2015007188A JP 2015007188 A JP2015007188 A JP 2015007188A JP 2013132910 A JP2013132910 A JP 2013132910A JP 2013132910 A JP2013132910 A JP 2013132910A JP 2015007188 A JP2015007188 A JP 2015007188A
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- Japan
- Prior art keywords
- dihydroxy compound
- polycarbonate
- compound
- reaction
- dihydroxy
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 150000005690 diesters Chemical class 0.000 claims abstract description 5
- 238000006243 chemical reaction Methods 0.000 claims description 128
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- 238000004090 dissolution Methods 0.000 claims description 86
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- 150000004650 carbonic acid diesters Chemical class 0.000 claims description 44
- 125000004432 carbon atom Chemical group C* 0.000 claims description 26
- 239000007787 solid Substances 0.000 claims description 21
- 125000003118 aryl group Chemical group 0.000 claims description 13
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- 150000004292 cyclic ethers Chemical group 0.000 claims description 10
- 229910052799 carbon Inorganic materials 0.000 claims description 9
- 125000000217 alkyl group Chemical group 0.000 claims description 8
- 238000009835 boiling Methods 0.000 claims description 6
- 150000001721 carbon Chemical class 0.000 claims description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
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- ROORDVPLFPIABK-UHFFFAOYSA-N diphenyl carbonate Chemical compound C=1C=CC=CC=1OC(=O)OC1=CC=CC=C1 ROORDVPLFPIABK-UHFFFAOYSA-N 0.000 description 44
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- NQXNYVAALXGLQT-UHFFFAOYSA-N 2-[4-[9-[4-(2-hydroxyethoxy)phenyl]fluoren-9-yl]phenoxy]ethanol Chemical compound C1=CC(OCCO)=CC=C1C1(C=2C=CC(OCCO)=CC=2)C2=CC=CC=C2C2=CC=CC=C21 NQXNYVAALXGLQT-UHFFFAOYSA-N 0.000 description 6
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- NIHNNTQXNPWCJQ-UHFFFAOYSA-N fluorene Chemical compound C1=CC=C2CC3=CC=CC=C3C2=C1 NIHNNTQXNPWCJQ-UHFFFAOYSA-N 0.000 description 6
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- WGTYBPLFGIVFAS-UHFFFAOYSA-M tetramethylammonium hydroxide Chemical compound [OH-].C[N+](C)(C)C WGTYBPLFGIVFAS-UHFFFAOYSA-M 0.000 description 6
- BXGYYDRIMBPOMN-UHFFFAOYSA-N 2-(hydroxymethoxy)ethoxymethanol Chemical compound OCOCCOCO BXGYYDRIMBPOMN-UHFFFAOYSA-N 0.000 description 5
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 5
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 5
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 5
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical class OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 5
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical class OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 5
- 125000003368 amide group Chemical group 0.000 description 5
- 239000003963 antioxidant agent Substances 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
- 238000000354 decomposition reaction Methods 0.000 description 5
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- 125000004185 ester group Chemical group 0.000 description 5
- 229910052744 lithium Inorganic materials 0.000 description 5
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- 230000009257 reactivity Effects 0.000 description 5
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- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical class [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
- 150000003868 ammonium compounds Chemical class 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 4
- 125000002029 aromatic hydrocarbon group Chemical group 0.000 description 4
- 239000012298 atmosphere Substances 0.000 description 4
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 4
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- 239000003795 chemical substances by application Substances 0.000 description 4
- OEYIOHPDSNJKLS-UHFFFAOYSA-N choline Chemical compound C[N+](C)(C)CCO OEYIOHPDSNJKLS-UHFFFAOYSA-N 0.000 description 4
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- 125000001142 dicarboxylic acid group Chemical group 0.000 description 4
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- 229920000728 polyester Polymers 0.000 description 4
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- UBQKCCHYAOITMY-UHFFFAOYSA-N pyridin-2-ol Chemical compound OC1=CC=CC=N1 UBQKCCHYAOITMY-UHFFFAOYSA-N 0.000 description 4
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical class C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 description 4
- VDZOOKBUILJEDG-UHFFFAOYSA-M tetrabutylammonium hydroxide Chemical compound [OH-].CCCC[N+](CCCC)(CCCC)CCCC VDZOOKBUILJEDG-UHFFFAOYSA-M 0.000 description 4
- GXURZKWLMYOCDX-UHFFFAOYSA-N 2,2-bis(hydroxymethyl)propane-1,3-diol;dihydroxyphosphanyl dihydrogen phosphite Chemical compound OP(O)OP(O)O.OCC(CO)(CO)CO GXURZKWLMYOCDX-UHFFFAOYSA-N 0.000 description 3
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- QSRFYFHZPSGRQX-UHFFFAOYSA-N benzyl(tributyl)azanium Chemical compound CCCC[N+](CCCC)(CCCC)CC1=CC=CC=C1 QSRFYFHZPSGRQX-UHFFFAOYSA-N 0.000 description 2
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- SXVFRTBMWHHATP-UHFFFAOYSA-M butyl(triphenyl)azanium;hydroxide Chemical compound [OH-].C=1C=CC=CC=1[N+](C=1C=CC=CC=1)(CCCC)C1=CC=CC=C1 SXVFRTBMWHHATP-UHFFFAOYSA-M 0.000 description 2
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2017074980A (ja) * | 2015-10-16 | 2017-04-20 | 三菱瓦斯化学株式会社 | 粒状物の貯蔵方法、粒状物貯蔵及び輸送容器、及びそれらを用いた押出成形方法 |
| JP2017082038A (ja) * | 2015-10-23 | 2017-05-18 | 帝人株式会社 | ポリカーボネート樹脂及び光学部材 |
| JP2020090677A (ja) * | 2020-01-22 | 2020-06-11 | 帝人株式会社 | ポリカーボネート樹脂および光学フィルム |
| WO2023085340A1 (ja) * | 2021-11-12 | 2023-05-19 | 三菱瓦斯化学株式会社 | ポリカーボネート樹脂、ならびにそれを用いた光学レンズおよび光学フィルム |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JP2010150540A (ja) * | 2008-11-28 | 2010-07-08 | Mitsubishi Chemicals Corp | ポリカーボネート原料用ジヒドロキシ化合物の保存方法、ポリカーボネート原料の調製方法及びポリカーボネートの製造方法 |
| JP2013010965A (ja) * | 2011-03-31 | 2013-01-17 | Mitsubishi Chemicals Corp | ポリカーボネート樹脂の製造方法 |
| JP2013018979A (ja) * | 2011-06-16 | 2013-01-31 | Mitsubishi Chemicals Corp | ポリカーボネートジオール含有組成物およびその製造方法、並びにポリカーボネートジオール含有組成物を用いたポリウレタン |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JP2010150540A (ja) * | 2008-11-28 | 2010-07-08 | Mitsubishi Chemicals Corp | ポリカーボネート原料用ジヒドロキシ化合物の保存方法、ポリカーボネート原料の調製方法及びポリカーボネートの製造方法 |
| JP2013010965A (ja) * | 2011-03-31 | 2013-01-17 | Mitsubishi Chemicals Corp | ポリカーボネート樹脂の製造方法 |
| JP2013018979A (ja) * | 2011-06-16 | 2013-01-31 | Mitsubishi Chemicals Corp | ポリカーボネートジオール含有組成物およびその製造方法、並びにポリカーボネートジオール含有組成物を用いたポリウレタン |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2017074980A (ja) * | 2015-10-16 | 2017-04-20 | 三菱瓦斯化学株式会社 | 粒状物の貯蔵方法、粒状物貯蔵及び輸送容器、及びそれらを用いた押出成形方法 |
| JP2017082038A (ja) * | 2015-10-23 | 2017-05-18 | 帝人株式会社 | ポリカーボネート樹脂及び光学部材 |
| JP2020090677A (ja) * | 2020-01-22 | 2020-06-11 | 帝人株式会社 | ポリカーボネート樹脂および光学フィルム |
| WO2023085340A1 (ja) * | 2021-11-12 | 2023-05-19 | 三菱瓦斯化学株式会社 | ポリカーボネート樹脂、ならびにそれを用いた光学レンズおよび光学フィルム |
| EP4431544A4 (en) * | 2021-11-12 | 2025-02-26 | Mitsubishi Gas Chemical Company, Inc. | Polycarbonate resin, and optical lens and optical film using same |
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