JP2014504278A5 - - Google Patents
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- Publication number
- JP2014504278A5 JP2014504278A5 JP2013540038A JP2013540038A JP2014504278A5 JP 2014504278 A5 JP2014504278 A5 JP 2014504278A5 JP 2013540038 A JP2013540038 A JP 2013540038A JP 2013540038 A JP2013540038 A JP 2013540038A JP 2014504278 A5 JP2014504278 A5 JP 2014504278A5
- Authority
- JP
- Japan
- Prior art keywords
- drying column
- reaction
- drying
- column
- produce
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000001035 drying Methods 0.000 claims 25
- 238000000034 method Methods 0.000 claims 18
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical group OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 6
- 239000007795 chemical reaction product Substances 0.000 claims 6
- 238000006243 chemical reaction Methods 0.000 claims 5
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims 4
- 239000012043 crude product Substances 0.000 claims 4
- 238000004821 distillation Methods 0.000 claims 4
- 239000000376 reactant Substances 0.000 claims 4
- 239000012429 reaction media Substances 0.000 claims 4
- 239000012264 purified product Substances 0.000 claims 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims 2
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 claims 2
- 229910002091 carbon monoxide Inorganic materials 0.000 claims 2
- 239000003054 catalyst Substances 0.000 claims 2
- 230000002496 gastric effect Effects 0.000 claims 2
- 229910052736 halogen Inorganic materials 0.000 claims 2
- 150000002367 halogens Chemical class 0.000 claims 2
- 239000007788 liquid Substances 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims 2
- TZIHFWKZFHZASV-UHFFFAOYSA-N methyl formate Chemical compound COC=O TZIHFWKZFHZASV-UHFFFAOYSA-N 0.000 claims 2
- 239000000203 mixture Substances 0.000 claims 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims 1
- 230000006315 carbonylation Effects 0.000 claims 1
- 238000005810 carbonylation reaction Methods 0.000 claims 1
- 235000019253 formic acid Nutrition 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- 239000000047 product Substances 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US12/950,520 US8637698B2 (en) | 2010-11-19 | 2010-11-19 | Production of acetic acid with an increased production rate |
| US12/950,520 | 2010-11-19 | ||
| PCT/US2011/061316 WO2012068429A2 (en) | 2010-11-19 | 2011-11-18 | Production of acetic acid with an increased production rate |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015158397A Division JP6208722B2 (ja) | 2010-11-19 | 2015-08-10 | 増加した製造速度での酢酸の製造 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2014504278A JP2014504278A (ja) | 2014-02-20 |
| JP2014504278A5 true JP2014504278A5 (enExample) | 2015-01-15 |
| JP5873101B2 JP5873101B2 (ja) | 2016-03-01 |
Family
ID=45099204
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013540038A Expired - Fee Related JP5873101B2 (ja) | 2010-11-19 | 2011-11-18 | 増加した製造速度での酢酸の製造 |
| JP2015158397A Active JP6208722B2 (ja) | 2010-11-19 | 2015-08-10 | 増加した製造速度での酢酸の製造 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015158397A Active JP6208722B2 (ja) | 2010-11-19 | 2015-08-10 | 増加した製造速度での酢酸の製造 |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US8637698B2 (enExample) |
| EP (1) | EP2640685A2 (enExample) |
| JP (2) | JP5873101B2 (enExample) |
| CN (2) | CN103221375A (enExample) |
| AR (1) | AR083929A1 (enExample) |
| BR (1) | BR112013012246A2 (enExample) |
| CA (1) | CA2816898A1 (enExample) |
| MX (1) | MX355557B (enExample) |
| RU (1) | RU2013127674A (enExample) |
| SG (1) | SG190328A1 (enExample) |
| TW (1) | TWI606037B (enExample) |
| WO (1) | WO2012068429A2 (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20150014150A1 (en) * | 2013-07-11 | 2015-01-15 | Celanese Acetate Llc | Process for Energy Recovery in Purifying Carboxylic Anhydride for Manufacturing Cellulose Esters |
| US20150014148A1 (en) * | 2013-07-11 | 2015-01-15 | Celanese Acetate Llc | Process for Energy Recovery in Manufacturing Cellulose Esters |
| CN103864595B (zh) * | 2014-03-07 | 2015-11-25 | 中石化上海工程有限公司 | 醋酸装置能量利用的方法 |
| KR20190039518A (ko) * | 2016-08-17 | 2019-04-12 | 코베스트로 도이칠란트 아게 | 통합 생산으로 이소시아네이트 및 적어도 1종의 추가의 화학 생성물을 제조하는 방법 |
| CN111646890A (zh) * | 2019-09-10 | 2020-09-11 | 上海浦景化工技术股份有限公司 | 反应器与精馏塔热耦合的甲醇羰基化制醋酸的工艺方法 |
Family Cites Families (49)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3190912A (en) | 1962-05-02 | 1965-06-22 | Nat Distillers Chem Corp | Process for preparing esters |
| US3637819A (en) | 1967-12-30 | 1972-01-25 | Knapsack Ag | Process for the manufacture of unsaturated esters of carboxylic acids |
| US3769329A (en) | 1970-03-12 | 1973-10-30 | Monsanto Co | Production of carboxylic acids and esters |
| US4039395A (en) | 1975-08-11 | 1977-08-02 | Monsanto Company | Purification of acetic acid |
| DE2811115A1 (de) | 1978-03-15 | 1979-09-27 | Hoechst Ag | Traeger-katalysator fuer die herstellung von vinylacetat aus ethylen, essigsaeure und sauerstoff in der gasphase |
| EP0055622B1 (en) | 1980-12-26 | 1985-05-29 | Mitsubishi Gas Chemical Company, Inc. | Process for producing acetic anhydride |
| US5001259A (en) | 1984-05-03 | 1991-03-19 | Hoechst Celanese Corporation | Methanol carbonylation process |
| US5026908A (en) | 1984-05-03 | 1991-06-25 | Hoechst Celanese Corporation | Methanol carbonylation process |
| US5144068A (en) | 1984-05-03 | 1992-09-01 | Hoechst Celanese Corporation | Methanol carbonylation process |
| US4615806B1 (en) | 1985-03-07 | 1994-05-03 | Hoechst Co American | Removal of iodide compounds from non-aqueous organic media |
| CA1299195C (en) | 1986-06-16 | 1992-04-21 | G. Paull Torrence | Addition of hydrogen to carbon monoxide feed gas in producing acetic acid by carbonylation of methanol |
| US4894477A (en) | 1986-10-14 | 1990-01-16 | Hoechst Celanese Corporation | Process for regenerating a carbonylation catalyst solution to remove corrosion metals and carbonylation of methanol to acetic acid |
| DE3803900A1 (de) | 1988-02-09 | 1989-08-17 | Hoechst Ag | Verfahren zur herstellung von vinylacetat |
| US5185308A (en) | 1991-05-06 | 1993-02-09 | Bp Chemicals Limited | Catalysts and processes for the manufacture of vinyl acetate |
| US5334755A (en) | 1992-04-24 | 1994-08-02 | Chiyoda Corporation | Process for the production of acetic acid from methanol and carbon monoxide using supported rhodium catalyst |
| US5672743A (en) | 1993-09-10 | 1997-09-30 | Bp Chemicals Limited | Process for the production of acetic acid |
| US5364963A (en) | 1993-04-30 | 1994-11-15 | Chiyoda Corporation | Supported rhodium catalyst, method of preparing same and process of producing acetic acid by methanol carbonylation using same |
| US5352415A (en) * | 1993-09-29 | 1994-10-04 | Hoechst Celanese Corporation | Control system for acetic acid manufacturing process |
| DE4342042A1 (de) * | 1993-12-09 | 1995-06-14 | Hoechst Ag | Verfahren und Vorrichtung zur Reinigung von Vinylchlorid |
| US5696284A (en) | 1995-06-21 | 1997-12-09 | Bp Chemicals Limited | Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof |
| IN189249B (enExample) | 1995-10-27 | 2003-01-18 | Hoechst Celanese Corp | |
| US6339171B1 (en) | 1996-10-18 | 2002-01-15 | Celanese International Corporation | Removal or reduction of permanganate reducing compounds and alkyl iodides from a carbonylation process stream |
| IN192600B (enExample) | 1996-10-18 | 2004-05-08 | Hoechst Celanese Corp | |
| GB9625335D0 (en) | 1996-12-05 | 1997-01-22 | Bp Chem Int Ltd | Process |
| GB9626317D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| GB9626428D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| GB9626429D0 (en) | 1996-12-19 | 1997-02-05 | Bp Chem Int Ltd | Process |
| US6114576A (en) | 1997-12-18 | 2000-09-05 | Uop Llc | Carbonylation process with integrated heat exchange |
| GB9816385D0 (en) * | 1998-07-29 | 1998-09-23 | Bp Chem Int Ltd | Process |
| DE69915417T2 (de) | 1998-08-06 | 2005-01-27 | Haldor Topsoe A/S | Reaktiv Distillierungsverfahren zur Herstellung von Essigsäure auf der Basis von DME/Methanol Carbonylierung |
| US6225498B1 (en) | 2000-03-24 | 2001-05-01 | Celanese International Corporation | Method of removing organic iodides from organic media |
| US6627770B1 (en) * | 2000-08-24 | 2003-09-30 | Celanese International Corporation | Method and apparatus for sequesting entrained and volatile catalyst species in a carbonylation process |
| US6657078B2 (en) | 2001-02-07 | 2003-12-02 | Celanese International Corporation | Low energy carbonylation process |
| US7005541B2 (en) | 2002-12-23 | 2006-02-28 | Celanese International Corporation | Low water methanol carbonylation process for high acetic acid production and for water balance control |
| US7223886B2 (en) | 2004-03-02 | 2007-05-29 | Celanese International Corporation | Removal of permanganate reducing compounds from methanol carbonylation process stream |
| US7271293B2 (en) | 2004-03-02 | 2007-09-18 | Celanese International Corporation | Control method for process of removing permanganate reducing compounds from methanol carbonylation process |
| US7465823B2 (en) | 2004-03-17 | 2008-12-16 | Celanese International Corporation | Utilization of acetic acid reaction heat in other process plants |
| US7199263B2 (en) | 2004-08-18 | 2007-04-03 | Celanese International Corporation | Acetic anhydride and acetate ester co-production |
| US7855306B2 (en) | 2005-04-28 | 2010-12-21 | Celanese International Corporation | Process for the production of acetic acid |
| EP1966115B1 (en) * | 2005-12-21 | 2011-04-20 | BP Chemicals Limited | Carbonylation process |
| CN100363321C (zh) * | 2005-12-29 | 2008-01-23 | 西南化工研究设计院 | 甲醇低压羰基合成醋酸工艺中的精馏方法 |
| JP5148578B2 (ja) * | 2007-03-15 | 2013-02-20 | 三菱重工業株式会社 | 脱水システム |
| US7989659B2 (en) | 2007-05-17 | 2011-08-02 | Celanese International Corporation | Method and apparatus for making acetic acid with improved light ends column productivity |
| US8017802B2 (en) | 2007-05-21 | 2011-09-13 | Celanese International Corporation | Control of impurities in reaction product of rhodium-catalyzed methanol carbonylation |
| US7902397B2 (en) * | 2007-10-11 | 2011-03-08 | Celanese International Corporation | Method and apparatus for making acetic acid with improved productivity |
| US8062482B2 (en) | 2007-10-30 | 2011-11-22 | Celanese International Corporation | Acetaldehyde removal from methyl acetate by distillation at elevated pressure |
| JP5325418B2 (ja) * | 2007-12-28 | 2013-10-23 | 三菱重工業株式会社 | 脱水システム及び脱水方法 |
| US7820855B2 (en) | 2008-04-29 | 2010-10-26 | Celanese International Corporation | Method and apparatus for carbonylating methanol with acetic acid enriched flash stream |
| MX2010011850A (es) | 2008-04-29 | 2010-11-30 | Celanese Int Corp | Sistema de carbonilacion de metanol que tiene un absorbedor con multiples opciones de disolvente. |
-
2010
- 2010-11-19 US US12/950,520 patent/US8637698B2/en active Active
-
2011
- 2011-11-10 TW TW100140994A patent/TWI606037B/zh active
- 2011-11-18 CN CN2011800553733A patent/CN103221375A/zh active Pending
- 2011-11-18 BR BR112013012246A patent/BR112013012246A2/pt not_active IP Right Cessation
- 2011-11-18 AR ARP110104317A patent/AR083929A1/es not_active Application Discontinuation
- 2011-11-18 JP JP2013540038A patent/JP5873101B2/ja not_active Expired - Fee Related
- 2011-11-18 CA CA2816898A patent/CA2816898A1/en not_active Abandoned
- 2011-11-18 WO PCT/US2011/061316 patent/WO2012068429A2/en not_active Ceased
- 2011-11-18 MX MX2013005586A patent/MX355557B/es active IP Right Grant
- 2011-11-18 CN CN201711016610.0A patent/CN107673963A/zh active Pending
- 2011-11-18 EP EP11791709.6A patent/EP2640685A2/en not_active Withdrawn
- 2011-11-18 SG SG2013038294A patent/SG190328A1/en unknown
- 2011-11-18 RU RU2013127674/04A patent/RU2013127674A/ru not_active Application Discontinuation
-
2015
- 2015-08-10 JP JP2015158397A patent/JP6208722B2/ja active Active
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