JP2009539835A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2009539835A5 JP2009539835A5 JP2009514302A JP2009514302A JP2009539835A5 JP 2009539835 A5 JP2009539835 A5 JP 2009539835A5 JP 2009514302 A JP2009514302 A JP 2009514302A JP 2009514302 A JP2009514302 A JP 2009514302A JP 2009539835 A5 JP2009539835 A5 JP 2009539835A5
- Authority
- JP
- Japan
- Prior art keywords
- acetic anhydride
- acetic acid
- liquid
- evaporation
- product effluent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- WFDIJRYMOXRFFG-UHFFFAOYSA-N acetic acid anhydride Natural products CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 claims 192
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 132
- 238000001704 evaporation Methods 0.000 claims 62
- 230000008020 evaporation Effects 0.000 claims 62
- 239000000047 product Substances 0.000 claims 51
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 39
- 239000007788 liquid Substances 0.000 claims 29
- 230000006315 carbonylation Effects 0.000 claims 24
- 238000005810 carbonylation reaction Methods 0.000 claims 24
- 239000003054 catalyst Substances 0.000 claims 22
- 239000012263 liquid product Substances 0.000 claims 21
- 239000002994 raw material Substances 0.000 claims 21
- INQOMBQAUSQDDS-UHFFFAOYSA-N iodomethane Chemical compound IC INQOMBQAUSQDDS-UHFFFAOYSA-N 0.000 claims 20
- 150000001875 compounds Chemical class 0.000 claims 19
- 238000000034 method Methods 0.000 claims 12
- 239000000203 mixture Substances 0.000 claims 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 11
- 238000006243 chemical reaction Methods 0.000 claims 10
- 238000000746 purification Methods 0.000 claims 6
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims 4
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims 4
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 claims 4
- 238000004519 manufacturing process Methods 0.000 claims 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims 2
- 229910002091 carbon monoxide Inorganic materials 0.000 claims 2
- 229910052741 iridium Inorganic materials 0.000 claims 2
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 claims 2
- 239000011541 reaction mixture Substances 0.000 claims 2
- 229910052703 rhodium Inorganic materials 0.000 claims 2
- 239000010948 rhodium Substances 0.000 claims 2
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 claims 2
- 238000009835 boiling Methods 0.000 claims 1
- 239000007791 liquid phase Substances 0.000 claims 1
- 239000007858 starting material Substances 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/423,383 | 2006-06-09 | ||
| US11/423,383 US7737298B2 (en) | 2006-06-09 | 2006-06-09 | Production of acetic acid and mixtures of acetic acid and acetic anhydride |
| PCT/US2007/012457 WO2007145795A2 (en) | 2006-06-09 | 2007-05-25 | Production of acetic acid and mixtures of acetic acid and acetic anhydride |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009539835A JP2009539835A (ja) | 2009-11-19 |
| JP2009539835A5 true JP2009539835A5 (enExample) | 2010-05-27 |
| JP5281000B2 JP5281000B2 (ja) | 2013-09-04 |
Family
ID=38564364
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009514302A Expired - Fee Related JP5281000B2 (ja) | 2006-06-09 | 2007-05-25 | 酢酸および酢酸と無水酢酸との混合物の製造 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US7737298B2 (enExample) |
| EP (1) | EP2029514B1 (enExample) |
| JP (1) | JP5281000B2 (enExample) |
| CN (1) | CN101466659B (enExample) |
| TW (1) | TWI398435B (enExample) |
| WO (1) | WO2007145795A2 (enExample) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101659607B (zh) * | 2008-08-29 | 2013-04-10 | 上海焦化有限公司 | 制备乙酸、乙酸酐或同时制备乙酸和乙酸酐的方法 |
| US9012683B2 (en) * | 2010-11-12 | 2015-04-21 | Eastman Chemical Company | Coproduction of acetic acid and acetic anhydride |
| US8637699B2 (en) | 2011-04-15 | 2014-01-28 | Lyondell Chemical Technology, L.P. | Process for the manufacture of acetic acid |
| US9415366B2 (en) * | 2012-12-31 | 2016-08-16 | Eastman Chemical Company | Systems and methods for processing variable acetyl streams |
| US10988432B2 (en) * | 2013-03-07 | 2021-04-27 | Ineos Acetyls Uk Limited | Process for the co-production of acetic acid and acetic anhydride |
| US9908835B2 (en) | 2015-11-13 | 2018-03-06 | Celanese International Corporation | Processes for purifying acetic and hydrating anhydride |
| US9907305B2 (en) | 2016-03-22 | 2018-03-06 | Solvay Sa | Production of disinfecting solutions |
| CN114031492B (zh) * | 2021-12-13 | 2023-08-29 | 上海簇睿低碳能源技术有限公司 | 一种采用微通道反应器合成醋酸或醋酐的工艺系统及制备方法 |
Family Cites Families (48)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SE364254B (enExample) | 1967-04-05 | 1974-02-18 | Monsanto Co | |
| US3772380A (en) | 1970-03-12 | 1973-11-13 | Monsanto Co | Production of carboxylic acids and esters |
| US3927078A (en) | 1972-08-21 | 1975-12-16 | Chevron Res | Methylene and oxymethylene bis-ester production |
| US4559183A (en) | 1973-09-04 | 1985-12-17 | The Halcon Sd Group, Inc. | Preparation of carboxylic acid anhydrides |
| DE2450965C2 (de) | 1974-10-26 | 1983-06-09 | Hoechst Ag, 6230 Frankfurt | Verfahren zur Herstellung von Essigsäureanhydrid |
| US4115444A (en) | 1975-03-10 | 1978-09-19 | Halcon International, Inc. | Process for preparing carboxylic acid anhydrides |
| DE2836084A1 (de) | 1978-08-17 | 1980-03-06 | Hoechst Ag | Verfahren zur herstellung von essigsaeureanhydrid |
| JPS5538369A (en) | 1978-09-01 | 1980-03-17 | Texaco Development Corp | Manufacture of carboxylic acids and their esters |
| US4252741A (en) | 1978-10-06 | 1981-02-24 | Halcon Research & Development Corp. | Carbonylation with Group VIII noble metal catalysts |
| US4358411A (en) | 1979-06-29 | 1982-11-09 | The Halcon Sd Group, Inc. | Preparation of carbonylation products |
| DE2939839A1 (de) | 1979-10-02 | 1981-04-23 | Hoechst Ag, 6000 Frankfurt | Verfahren zur herstellung von essigsaeureanhydrid |
| US4417077A (en) | 1980-10-01 | 1983-11-22 | University Of Illinois Foundation | Heterogeneous anionic transition metal catalysts |
| US4374070A (en) * | 1980-11-21 | 1983-02-15 | Eastman Kodak Company | Preparation of acetic anhydride |
| US4366259A (en) | 1981-10-29 | 1982-12-28 | Texaco, Inc. | Production of acetic acid and propionic acid and their esters |
| DE3148006A1 (de) | 1981-12-04 | 1983-06-09 | Hoechst Ag, 6230 Frankfurt | Verfahren zur herstellung von essigsaeureanhydrid und/oder essigsaeure und/oder ethylidendiacetat |
| NZ203225A (en) | 1982-02-13 | 1985-01-31 | Bp Chem Int Ltd | Coproduction of monocarboxylic acids and anhydrides |
| NZ203226A (en) | 1982-02-13 | 1985-08-30 | Bp Chemical Ltd | Production of acetic anhydride from methanol and carbon monoxide |
| ZA833528B (en) | 1982-05-22 | 1984-12-24 | Bp Chem Int Ltd | Process for the production of one or more carboxylic acid anhydrides |
| EP0109212B1 (en) | 1982-11-04 | 1987-05-27 | BP Chemicals Limited | Process for the preparation of acids |
| US4629809A (en) | 1983-07-21 | 1986-12-16 | Texaco Inc. | Process for selectively preparing acetic acid by carbonylation of methanol in the presence of a novel iodide-free catalyst system |
| GB8404136D0 (en) | 1984-02-16 | 1984-03-21 | Bp Chem Int Ltd | Carbonylation process |
| US5144068A (en) | 1984-05-03 | 1992-09-01 | Hoechst Celanese Corporation | Methanol carbonylation process |
| US5003104A (en) | 1987-03-03 | 1991-03-26 | Bp Chemicals Limited | Carbonylation process and catalyst |
| GB8807284D0 (en) | 1988-03-26 | 1988-04-27 | Bp Chem Int Ltd | Chemical process |
| GB8809027D0 (en) | 1988-04-16 | 1988-05-18 | British Petroleum Co Plc | Carbonylation of allylic alcohols |
| DE3823645C1 (enExample) * | 1988-07-13 | 1989-11-30 | Hoechst Ag | |
| US5442107A (en) | 1989-04-06 | 1995-08-15 | Bp Chemicals Limited | Preparing carboxylic acids |
| JP2839367B2 (ja) | 1989-04-06 | 1998-12-16 | ビーピー ケミカルズ リミテッド | カルボン酸類の製造方法 |
| GB9021454D0 (en) | 1990-10-03 | 1990-11-14 | Bp Chem Int Ltd | Process |
| DE69108567T2 (de) | 1990-12-20 | 1995-08-03 | Eastman Chem Co | Kontinuierliches verfahren zur herstellung von essigsäureanhydrid oder einer mischung von essigsäureanhydrid und essigsäure. |
| GB9211671D0 (en) | 1992-06-02 | 1992-07-15 | Bp Chem Int Ltd | Process |
| US5488143A (en) | 1992-06-30 | 1996-01-30 | Korea Institute Of Science And Technology | Processes for the carbonylation of methanol to form acetic acid, methyl acetate and acetic anhydride |
| GB9218346D0 (en) | 1992-08-28 | 1992-10-14 | Bp Chem Int Ltd | Process |
| CN1040101C (zh) * | 1993-08-18 | 1998-10-07 | 大世吕化学工业株式会社 | 乙酸酐或乙酸酐和乙酸的制备方法 |
| US5510524A (en) | 1995-02-21 | 1996-04-23 | Bp Chemicals Limited | Process for the production of a carboxylic acid |
| US5696284A (en) | 1995-06-21 | 1997-12-09 | Bp Chemicals Limited | Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof |
| US5900505A (en) | 1997-02-04 | 1999-05-04 | Eastman Chemical Company | Heterogeneous vapor phase carbonylation process |
| GB9802027D0 (en) * | 1998-01-31 | 1998-03-25 | Bp Chem Int Ltd | Chemical process |
| EP1071647A1 (en) | 1998-04-17 | 2001-01-31 | BP Chemicals Limited | Process for the production of acetic acid and/or acetic anhydride |
| US5922911A (en) | 1998-04-24 | 1999-07-13 | Eastman Chemical Company | Process for the manufacture of acetic anhydride |
| GB9816385D0 (en) | 1998-07-29 | 1998-09-23 | Bp Chem Int Ltd | Process |
| US6211405B1 (en) | 1998-10-23 | 2001-04-03 | Celanese International Corporation | Addition of iridium to the rhodium/inorganic iodide catalyst system |
| US6452043B1 (en) | 2000-04-05 | 2002-09-17 | Eastman Chemical Company | Carbonylation of lower alkyl alcohols and their derivatives using metals supported on carbonized polysulfonated divinylbenzene-styrene copolymers |
| DE10138778A1 (de) * | 2001-08-07 | 2003-02-20 | Basf Ag | Flexibles Verfahren zur gemeinsamen Herstellung von Ameisensäure sowie einer Carbonsäure mit mindestens zwei Kohlenstoffatomen und/oder deren Derivaten |
| JP3660982B2 (ja) | 2001-11-08 | 2005-06-15 | 独立行政法人産業技術総合研究所 | カルボン酸塩の製造方法 |
| US6667418B2 (en) | 2002-04-16 | 2003-12-23 | Celanese International Corporation | Oxidation treatment of a recycle stream in production of acetic acid by methanol carbonylation |
| CN1315771C (zh) | 2002-05-06 | 2007-05-16 | 伊斯曼化学公司 | 连续羰基化工艺 |
| FR2839972B1 (fr) | 2002-05-23 | 2005-08-19 | Inst Francais Du Petrole | Procede de carbonylation des alcools utilisant un catalyseur a base de rhodium ou d'iridium dans un liquide ionique non-aqueux,avec un recyclage efficace du catalyseur |
-
2006
- 2006-06-09 US US11/423,383 patent/US7737298B2/en active Active
-
2007
- 2007-05-25 CN CN200780021487.XA patent/CN101466659B/zh active Active
- 2007-05-25 JP JP2009514302A patent/JP5281000B2/ja not_active Expired - Fee Related
- 2007-05-25 EP EP07777273.9A patent/EP2029514B1/en active Active
- 2007-05-25 WO PCT/US2007/012457 patent/WO2007145795A2/en not_active Ceased
- 2007-06-07 TW TW096120444A patent/TWI398435B/zh active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP2009539835A5 (enExample) | ||
| RU2072981C1 (ru) | Способ очистки уксусной кислоты и/или уксусного ангидрида от примесей иодидов | |
| JP4724341B2 (ja) | 酢酸エチルの製造方法及びその方法を実施するための装置 | |
| RU2008129374A (ru) | Способ карбонилирования | |
| TW200946493A (en) | Method and apparatus for carbonylating methanol with acetic acid enriched flash stream | |
| NZ602714A (en) | Carbonylation process and apparatus for making acetic acid with improved purification | |
| TWI403500B (zh) | 製備乙酸乙烯酯的方法 | |
| RU2016146558A (ru) | Способ получения диметилового эфира из газообразных смесей монооксида углерода, водорода и метилацетата | |
| US20150336868A1 (en) | Integrated process for making acetic acid | |
| JP5281000B2 (ja) | 酢酸および酢酸と無水酢酸との混合物の製造 | |
| JP2013538826A5 (enExample) | ||
| RU2013118697A (ru) | Циркуляционный реактор для получения уксусной кислоты | |
| CN101575269A (zh) | 一种芳香族甲醚化合物的制备方法 | |
| JP2000109441A (ja) | メタノールの製造方法 | |
| CN112794286A (zh) | 氯化溴的连续流法合成系统和合成工艺 | |
| CN103201246B (zh) | 用于纯化酸溶液的工艺 | |
| JP2014504278A5 (enExample) | ||
| RU2013127674A (ru) | Получение уксусной кислоты с увеличенной скоростью получения | |
| CN102807500A (zh) | 一种液相制备n,n-二甲基乙酰胺的方法 | |
| TWI508943B (zh) | 醋酸與醋酸酐之共同生產 | |
| JP2000063319A (ja) | Ｄｍｅ／メタノ―ルのカルボニル化に基づく酢酸反応性蒸留プロセス | |
| TWI742248B (zh) | 氧化生產芳族二羧酸之能量及環境整合方法 | |
| JP2013537549A5 (enExample) | ||
| TWI628163B (zh) | 處理可變乙醯流之系統及方法 | |
| KR20170015330A (ko) | (s)-2-아세틸옥시프로피온산 및 그것의 유도체의 제조 방법 |