JP2014141410A - 電解質を添加した移動相を用いた原子内包フラーレン塩の分離・精製方法 - Google Patents

電解質を添加した移動相を用いた原子内包フラーレン塩の分離・精製方法 Download PDF

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JP2014141410A
JP2014141410A JP2014094444A JP2014094444A JP2014141410A JP 2014141410 A JP2014141410 A JP 2014141410A JP 2014094444 A JP2014094444 A JP 2014094444A JP 2014094444 A JP2014094444 A JP 2014094444A JP 2014141410 A JP2014141410 A JP 2014141410A
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fullerene
solvent
salt
electrolyte
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JP2014141410A5 (enExample
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Hiroshi Okada
洋史 岡田
Ken Sakai
建 酒井
Yoshihiro Ono
吉弘 小野
Yasuhiko Kasama
泰彦 笠間
Kenji Omote
研次 表
Takashi Komuro
貴士 小室
Hiromi Hida
博実 飛田
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JP2014094444A 2009-09-01 2014-05-01 電解質を添加した移動相を用いた原子内包フラーレン塩の分離・精製方法 Pending JP2014141410A (ja)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018034258A1 (ja) * 2016-08-19 2018-02-22 国立研究開発法人産業技術総合研究所 内包フラーレン生成装置及び生成方法

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05180818A (ja) * 1992-01-08 1993-07-23 Daicel Chem Ind Ltd 液体クロマトグラフィー分離法
JPH06317575A (ja) * 1993-03-12 1994-11-15 Showa Denko Kk 高分子ポリマーの分子量分布の測定方法
JP2003036841A (ja) * 2001-05-29 2003-02-07 Itt Mfg Enterp Inc フラーレンベースの2次電池用電極
JP2004171921A (ja) * 2002-11-20 2004-06-17 Toyota Motor Corp 燃料電池から触媒金属及びスルホン酸基を有する含フッ素ポリマーを回収する方法
JP2005272159A (ja) * 2004-03-23 2005-10-06 Sony Corp 内包フラーレンの製造方法及び製造装置
WO2005095494A1 (ja) * 2004-03-31 2005-10-13 Nippon Kayaku Kabushiki Kaisha 新規水溶性フラーレン、その製造方法およびそれを含む活性酸素発生剤
JP2006036569A (ja) * 2004-07-26 2006-02-09 Takeshi Kodama 金属内包フラーレンの効率的かつ選択的抽出法
WO2006051989A1 (ja) * 2004-11-15 2006-05-18 Ideal Star Inc. アルカリ金属内包フラーレン類の分離剤、フラーレン類からのアルカリ金属とその化合物の除去方法、アルカリ金属内包フラーレン類の精製方法及び製造方法並びにそれらのシステム
JP3926331B2 (ja) * 2001-10-01 2007-06-06 ティーディーエイ リサーチ インコーポレイテッド 金属内包フラーレン類及びその他のフラーレン類の化学的精製方法
US20080085234A1 (en) * 2005-01-03 2008-04-10 Luna Innovations Chemical separation method for fullerenes
JP2011073887A (ja) * 2009-09-01 2011-04-14 Ideal Star Inc 電解質を添加した移動相を用いた原子内包フラーレン塩の分離・精製方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6303016B1 (en) * 1998-04-14 2001-10-16 Tda Research, Inc. Isolation of small-bandgap fullerenes and endohedral metallofullerenes
JP5065597B2 (ja) * 2005-01-14 2012-11-07 金子 博之 フラーレンベース材料の製造装置、及び、製造方法
JP5149787B2 (ja) * 2006-04-20 2013-02-20 金子 博之 フラーレンベース材料、及びフラーレンベース材料の製造方法

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05180818A (ja) * 1992-01-08 1993-07-23 Daicel Chem Ind Ltd 液体クロマトグラフィー分離法
JPH06317575A (ja) * 1993-03-12 1994-11-15 Showa Denko Kk 高分子ポリマーの分子量分布の測定方法
JP2003036841A (ja) * 2001-05-29 2003-02-07 Itt Mfg Enterp Inc フラーレンベースの2次電池用電極
JP3926331B2 (ja) * 2001-10-01 2007-06-06 ティーディーエイ リサーチ インコーポレイテッド 金属内包フラーレン類及びその他のフラーレン類の化学的精製方法
JP2004171921A (ja) * 2002-11-20 2004-06-17 Toyota Motor Corp 燃料電池から触媒金属及びスルホン酸基を有する含フッ素ポリマーを回収する方法
JP2005272159A (ja) * 2004-03-23 2005-10-06 Sony Corp 内包フラーレンの製造方法及び製造装置
WO2005095494A1 (ja) * 2004-03-31 2005-10-13 Nippon Kayaku Kabushiki Kaisha 新規水溶性フラーレン、その製造方法およびそれを含む活性酸素発生剤
JP2006036569A (ja) * 2004-07-26 2006-02-09 Takeshi Kodama 金属内包フラーレンの効率的かつ選択的抽出法
WO2006051989A1 (ja) * 2004-11-15 2006-05-18 Ideal Star Inc. アルカリ金属内包フラーレン類の分離剤、フラーレン類からのアルカリ金属とその化合物の除去方法、アルカリ金属内包フラーレン類の精製方法及び製造方法並びにそれらのシステム
US20080085234A1 (en) * 2005-01-03 2008-04-10 Luna Innovations Chemical separation method for fullerenes
JP2011073887A (ja) * 2009-09-01 2011-04-14 Ideal Star Inc 電解質を添加した移動相を用いた原子内包フラーレン塩の分離・精製方法

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
JPN6015008400; H. OKADA et al.: 'Preparation of endohedral fullerene containing lithium (Li@C60) and isolation as pure hexafluorophos' RSC Advances , 2012, 2, 10624-10631. *
JPN6015008401; B. ELLIOTT et al.: 'A Simple Isomeric Separation of D5h and Ih Sc3N@C80 by Selective Chemical Oxidation' J. Am. Chem. Soc. , 2005, 127, 10885-10888. *
JPN6015008403; 荒川力ら: '溶媒によるクロマトグラフィーの制御' 生化学 , 2008, 第80巻、第1号、45〜51ページ *
JPN6015008405; 'フラーレン関連カラム' ナカライテスクホームページ *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2018034258A1 (ja) * 2016-08-19 2018-02-22 国立研究開発法人産業技術総合研究所 内包フラーレン生成装置及び生成方法
JPWO2018034258A1 (ja) * 2016-08-19 2019-06-20 国立研究開発法人産業技術総合研究所 内包フラーレン生成装置及び生成方法

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