JP2013524813A - タバコ種子由来成分および材料 - Google Patents
タバコ種子由来成分および材料 Download PDFInfo
- Publication number
- JP2013524813A JP2013524813A JP2013506263A JP2013506263A JP2013524813A JP 2013524813 A JP2013524813 A JP 2013524813A JP 2013506263 A JP2013506263 A JP 2013506263A JP 2013506263 A JP2013506263 A JP 2013506263A JP 2013524813 A JP2013524813 A JP 2013524813A
- Authority
- JP
- Japan
- Prior art keywords
- seed
- tobacco
- isolate
- tobacco composition
- harvested
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 200
- 239000000463 material Substances 0.000 title claims description 83
- 239000004615 ingredient Substances 0.000 title abstract description 21
- 244000061176 Nicotiana tabacum Species 0.000 title description 172
- 239000000203 mixture Substances 0.000 claims abstract description 94
- 241000208125 Nicotiana Species 0.000 claims abstract description 62
- 238000000034 method Methods 0.000 claims abstract description 45
- 102000004190 Enzymes Human genes 0.000 claims abstract description 28
- 108090000790 Enzymes Proteins 0.000 claims abstract description 28
- 238000006243 chemical reaction Methods 0.000 claims abstract description 26
- 230000000391 smoking effect Effects 0.000 claims abstract description 25
- 239000000126 substance Substances 0.000 claims abstract description 17
- 238000005984 hydrogenation reaction Methods 0.000 claims abstract description 8
- 239000002253 acid Substances 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 230000007062 hydrolysis Effects 0.000 claims abstract description 6
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 6
- 235000019505 tobacco product Nutrition 0.000 claims description 32
- 238000000638 solvent extraction Methods 0.000 claims description 26
- 239000002904 solvent Substances 0.000 claims description 23
- 150000002632 lipids Chemical class 0.000 claims description 22
- 238000012545 processing Methods 0.000 claims description 16
- 238000000926 separation method Methods 0.000 claims description 13
- 238000003306 harvesting Methods 0.000 claims description 11
- 238000002955 isolation Methods 0.000 claims description 11
- 239000002775 capsule Substances 0.000 claims description 9
- 230000008859 change Effects 0.000 claims description 8
- 238000004587 chromatography analysis Methods 0.000 claims description 8
- 238000004821 distillation Methods 0.000 claims description 8
- 238000009472 formulation Methods 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 7
- 230000008569 process Effects 0.000 claims description 7
- 238000001953 recrystallisation Methods 0.000 claims description 7
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 claims description 6
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 230000002255 enzymatic effect Effects 0.000 claims description 5
- 239000012530 fluid Substances 0.000 claims description 5
- 102000004366 Glucosidases Human genes 0.000 claims description 4
- 108010056771 Glucosidases Proteins 0.000 claims description 4
- 102000005744 Glycoside Hydrolases Human genes 0.000 claims description 4
- 108010031186 Glycoside Hydrolases Proteins 0.000 claims description 4
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 238000005056 compaction Methods 0.000 claims description 4
- 238000007906 compression Methods 0.000 claims description 4
- 230000006835 compression Effects 0.000 claims description 4
- 239000003960 organic solvent Substances 0.000 claims description 4
- 102000004867 Hydro-Lyases Human genes 0.000 claims description 3
- 108090001042 Hydro-Lyases Proteins 0.000 claims description 3
- 230000015556 catabolic process Effects 0.000 claims description 3
- 238000006731 degradation reaction Methods 0.000 claims description 3
- 230000032050 esterification Effects 0.000 claims description 3
- 238000005886 esterification reaction Methods 0.000 claims description 3
- 230000008014 freezing Effects 0.000 claims description 3
- 238000007710 freezing Methods 0.000 claims description 3
- 239000002798 polar solvent Substances 0.000 claims description 3
- 238000005809 transesterification reaction Methods 0.000 claims description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 241000196324 Embryophyta Species 0.000 description 26
- 235000019504 cigarettes Nutrition 0.000 description 22
- 238000000605 extraction Methods 0.000 description 12
- 238000004519 manufacturing process Methods 0.000 description 12
- 150000001875 compounds Chemical class 0.000 description 10
- 238000001035 drying Methods 0.000 description 9
- 230000001953 sensory effect Effects 0.000 description 9
- 239000000796 flavoring agent Substances 0.000 description 8
- 239000000779 smoke Substances 0.000 description 8
- 235000019634 flavors Nutrition 0.000 description 7
- 241000282836 Camelus dromedarius Species 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 6
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 4
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 4
- 238000003672 processing method Methods 0.000 description 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 239000003570 air Substances 0.000 description 3
- 235000014113 dietary fatty acids Nutrition 0.000 description 3
- ZQPPMHVWECSIRJ-MDZDMXLPSA-N elaidic acid Chemical compound CCCCCCCC\C=C\CCCCCCCC(O)=O ZQPPMHVWECSIRJ-MDZDMXLPSA-N 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000000194 fatty acid Substances 0.000 description 3
- 229930195729 fatty acid Natural products 0.000 description 3
- 150000004665 fatty acids Chemical class 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 238000010348 incorporation Methods 0.000 description 3
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- -1 pH adjusters Substances 0.000 description 3
- 230000000704 physical effect Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 241000894007 species Species 0.000 description 3
- 150000003626 triacylglycerols Chemical class 0.000 description 3
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 2
- HNSDLXPSAYFUHK-UHFFFAOYSA-N 1,4-bis(2-ethylhexyl) sulfosuccinate Chemical compound CCCCC(CC)COC(=O)CC(S(O)(=O)=O)C(=O)OCC(CC)CCCC HNSDLXPSAYFUHK-UHFFFAOYSA-N 0.000 description 2
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 2
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 241000207746 Nicotiana benthamiana Species 0.000 description 2
- 241000250373 Nicotiana cavicola Species 0.000 description 2
- 241001495644 Nicotiana glutinosa Species 0.000 description 2
- 241000250027 Nicotiana linearis Species 0.000 description 2
- 241001144488 Nicotiana occidentalis Species 0.000 description 2
- 241000249968 Nicotiana umbratica Species 0.000 description 2
- 239000005642 Oleic acid Substances 0.000 description 2
- 235000021314 Palmitic acid Nutrition 0.000 description 2
- KYQCOXFCLRTKLS-UHFFFAOYSA-N Pyrazine Chemical compound C1=CN=CC=N1 KYQCOXFCLRTKLS-UHFFFAOYSA-N 0.000 description 2
- 235000021355 Stearic acid Nutrition 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 238000007605 air drying Methods 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- YZXBAPSDXZZRGB-DOFZRALJSA-N arachidonic acid Chemical compound CCCCC\C=C/C\C=C/C\C=C/C\C=C/CCCC(O)=O YZXBAPSDXZZRGB-DOFZRALJSA-N 0.000 description 2
- 239000011324 bead Substances 0.000 description 2
- 230000006399 behavior Effects 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 239000000969 carrier Substances 0.000 description 2
- 238000007385 chemical modification Methods 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 239000003085 diluting agent Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 235000013355 food flavoring agent Nutrition 0.000 description 2
- 239000000499 gel Substances 0.000 description 2
- CKDDRHZIAZRDBW-UHFFFAOYSA-N henicosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCC(O)=O CKDDRHZIAZRDBW-UHFFFAOYSA-N 0.000 description 2
- KEMQGTRYUADPNZ-UHFFFAOYSA-N heptadecanoic acid Chemical compound CCCCCCCCCCCCCCCCC(O)=O KEMQGTRYUADPNZ-UHFFFAOYSA-N 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- VKOBVWXKNCXXDE-UHFFFAOYSA-N icosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCC(O)=O VKOBVWXKNCXXDE-UHFFFAOYSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 2
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 2
- 235000021313 oleic acid Nutrition 0.000 description 2
- SECPZKHBENQXJG-FPLPWBNLSA-N palmitoleic acid Chemical compound CCCCCC\C=C/CCCCCCCC(O)=O SECPZKHBENQXJG-FPLPWBNLSA-N 0.000 description 2
- 239000003495 polar organic solvent Substances 0.000 description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 description 2
- 235000013824 polyphenols Nutrition 0.000 description 2
- 238000000899 pressurised-fluid extraction Methods 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- 239000008117 stearic acid Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- PVNIQBQSYATKKL-UHFFFAOYSA-N tripalmitin Chemical compound CCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCC PVNIQBQSYATKKL-UHFFFAOYSA-N 0.000 description 2
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 2
- 239000000080 wetting agent Substances 0.000 description 2
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 1
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- BITHHVVYSMSWAG-KTKRTIGZSA-N (11Z)-icos-11-enoic acid Chemical compound CCCCCCCC\C=C/CCCCCCCCCC(O)=O BITHHVVYSMSWAG-KTKRTIGZSA-N 0.000 description 1
- GEHPRJRWZDWFBJ-FOCLMDBBSA-N (2E)-2-heptadecenoic acid Chemical compound CCCCCCCCCCCCCC\C=C\C(O)=O GEHPRJRWZDWFBJ-FOCLMDBBSA-N 0.000 description 1
- KSDMISMEMOGBFU-UHFFFAOYSA-N (all-Z)-7,10,13-Eicosatrienoic acid Natural products CCCCCCC=CCC=CCC=CCCCCCC(O)=O KSDMISMEMOGBFU-UHFFFAOYSA-N 0.000 description 1
- HBOQXIRUPVQLKX-BBWANDEASA-N 1,2,3-trilinoleoylglycerol Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/C\C=C/CCCCC)COC(=O)CCCCCCC\C=C/C\C=C/CCCCC HBOQXIRUPVQLKX-BBWANDEASA-N 0.000 description 1
- 239000005635 Caprylic acid (CAS 124-07-2) Substances 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 1
- 241000287828 Gallus gallus Species 0.000 description 1
- 240000001238 Gaultheria procumbens Species 0.000 description 1
- 235000007297 Gaultheria procumbens Nutrition 0.000 description 1
- 241000081543 Hesperis Species 0.000 description 1
- 235000015842 Hesperis Nutrition 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- 125000002066 L-histidyl group Chemical group [H]N1C([H])=NC(C([H])([H])[C@](C(=O)[*])([H])N([H])[H])=C1[H] 0.000 description 1
- 235000021353 Lignoceric acid Nutrition 0.000 description 1
- CQXMAMUUWHYSIY-UHFFFAOYSA-N Lignoceric acid Natural products CCCCCCCCCCCCCCCCCCCCCCCC(=O)OCCC1=CC=C(O)C=C1 CQXMAMUUWHYSIY-UHFFFAOYSA-N 0.000 description 1
- 241001503485 Mammuthus Species 0.000 description 1
- 241000250374 Nicotiana acaulis Species 0.000 description 1
- 241000208126 Nicotiana acuminata Species 0.000 description 1
- 241001144497 Nicotiana africana Species 0.000 description 1
- 241000250377 Nicotiana amplexicaulis Species 0.000 description 1
- 241000228653 Nicotiana attenuata Species 0.000 description 1
- 241000250376 Nicotiana bonariensis Species 0.000 description 1
- 241001244271 Nicotiana cordifolia Species 0.000 description 1
- 241001144496 Nicotiana corymbosa Species 0.000 description 1
- 241000862464 Nicotiana excelsior Species 0.000 description 1
- 244000006449 Nicotiana forgetiana Species 0.000 description 1
- 241000208128 Nicotiana glauca Species 0.000 description 1
- 241000250366 Nicotiana gossei Species 0.000 description 1
- 241000579278 Nicotiana kawakamii Species 0.000 description 1
- 241000250031 Nicotiana megalosiphon Species 0.000 description 1
- 241000250030 Nicotiana miersii Species 0.000 description 1
- 241001144493 Nicotiana obtusifolia Species 0.000 description 1
- 241000876839 Nicotiana paniculata Species 0.000 description 1
- 241000208133 Nicotiana plumbaginifolia Species 0.000 description 1
- 241001290303 Nicotiana repanda Species 0.000 description 1
- 241001144486 Nicotiana rotundifolia Species 0.000 description 1
- 241000250044 Nicotiana simulans Species 0.000 description 1
- 241000249970 Nicotiana solanifolia Species 0.000 description 1
- 241001144495 Nicotiana spegazzinii Species 0.000 description 1
- 241000249966 Nicotiana stocktonii Species 0.000 description 1
- 241000208136 Nicotiana sylvestris Species 0.000 description 1
- 241000208138 Nicotiana tomentosiformis Species 0.000 description 1
- 241000249967 Nicotiana undulata Species 0.000 description 1
- 241001144494 Nicotiana wigandioides Species 0.000 description 1
- 241001143906 Nicotiana x sanderae Species 0.000 description 1
- 235000021319 Palmitoleic acid Nutrition 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- PCNDJXKNXGMECE-UHFFFAOYSA-N Phenazine Natural products C1=CC=CC2=NC3=CC=CC=C3N=C21 PCNDJXKNXGMECE-UHFFFAOYSA-N 0.000 description 1
- 241000251736 Raja clavata Species 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 244000082946 Tarchonanthus camphoratus Species 0.000 description 1
- BAECOWNUKCLBPZ-HIUWNOOHSA-N Triolein Natural products O([C@H](OCC(=O)CCCCCCC/C=C\CCCCCCCC)COC(=O)CCCCCCC/C=C\CCCCCCCC)C(=O)CCCCCCC/C=C\CCCCCCCC BAECOWNUKCLBPZ-HIUWNOOHSA-N 0.000 description 1
- PHYFQTYBJUILEZ-UHFFFAOYSA-N Trioleoylglycerol Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC(OC(=O)CCCCCCCC=CCCCCCCCC)COC(=O)CCCCCCCC=CCCCCCCCC PHYFQTYBJUILEZ-UHFFFAOYSA-N 0.000 description 1
- 241000712689 Velutina Species 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- AHANXAKGNAKFSK-PDBXOOCHSA-N all-cis-icosa-11,14,17-trienoic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCCCC(O)=O AHANXAKGNAKFSK-PDBXOOCHSA-N 0.000 description 1
- 239000012080 ambient air Substances 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 239000003125 aqueous solvent Substances 0.000 description 1
- 229940114079 arachidonic acid Drugs 0.000 description 1
- 235000021342 arachidonic acid Nutrition 0.000 description 1
- 150000001491 aromatic compounds Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000000872 buffer Substances 0.000 description 1
- 244000309464 bull Species 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 229920002301 cellulose acetate Polymers 0.000 description 1
- 230000001055 chewing effect Effects 0.000 description 1
- SECPZKHBENQXJG-UHFFFAOYSA-N cis-palmitoleic acid Natural products CCCCCCC=CCCCCCCCC(O)=O SECPZKHBENQXJG-UHFFFAOYSA-N 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000009402 cross-breeding Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- HOBAELRKJCKHQD-QNEBEIHSSA-N dihomo-γ-linolenic acid Chemical compound CCCCC\C=C/C\C=C/C\C=C/CCCCCCC(O)=O HOBAELRKJCKHQD-QNEBEIHSSA-N 0.000 description 1
- 229940090949 docosahexaenoic acid Drugs 0.000 description 1
- BITHHVVYSMSWAG-UHFFFAOYSA-N eicosenoic acid Natural products CCCCCCCCC=CCCCCCCCCCC(O)=O BITHHVVYSMSWAG-UHFFFAOYSA-N 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- FARYTWBWLZAXNK-WAYWQWQTSA-N ethyl (z)-3-(methylamino)but-2-enoate Chemical compound CCOC(=O)\C=C(\C)NC FARYTWBWLZAXNK-WAYWQWQTSA-N 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 229940047127 fiore Drugs 0.000 description 1
- 229940098330 gamma linoleic acid Drugs 0.000 description 1
- VZCCETWTMQHEPK-UHFFFAOYSA-N gamma-Linolensaeure Natural products CCCCCC=CCC=CCC=CCCCCC(O)=O VZCCETWTMQHEPK-UHFFFAOYSA-N 0.000 description 1
- VZCCETWTMQHEPK-QNEBEIHSSA-N gamma-linolenic acid Chemical compound CCCCC\C=C/C\C=C/C\C=C/CCCCC(O)=O VZCCETWTMQHEPK-QNEBEIHSSA-N 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 150000002337 glycosamines Chemical class 0.000 description 1
- 235000021299 gondoic acid Nutrition 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000008241 heterogeneous mixture Substances 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 239000003501 hydroponics Substances 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- YAQXGBBDJYBXKL-UHFFFAOYSA-N iron(2+);1,10-phenanthroline;dicyanide Chemical compound [Fe+2].N#[C-].N#[C-].C1=CN=C2C3=NC=CC=C3C=CC2=C1.C1=CN=C2C3=NC=CC=C3C=CC2=C1 YAQXGBBDJYBXKL-UHFFFAOYSA-N 0.000 description 1
- 230000005087 leaf formation Effects 0.000 description 1
- HBOQXIRUPVQLKX-UHFFFAOYSA-N linoleic acid triglyceride Natural products CCCCCC=CCC=CCCCCCCCC(=O)OCC(OC(=O)CCCCCCCC=CCC=CCCCCC)COC(=O)CCCCCCCC=CCC=CCCCCC HBOQXIRUPVQLKX-UHFFFAOYSA-N 0.000 description 1
- 229940041616 menthol Drugs 0.000 description 1
- OSWPMRLSEDHDFF-UHFFFAOYSA-N methyl salicylate Chemical compound COC(=O)C1=CC=CC=C1O OSWPMRLSEDHDFF-UHFFFAOYSA-N 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229960002446 octanoic acid Drugs 0.000 description 1
- 239000006187 pill Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000002953 preparative HPLC Methods 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000037452 priming Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000006798 recombination Effects 0.000 description 1
- 238000003168 reconstitution method Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000001850 reproductive effect Effects 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 230000008117 seed development Effects 0.000 description 1
- 238000002470 solid-phase micro-extraction Methods 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- 230000009974 thixotropic effect Effects 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 229940081852 trilinolein Drugs 0.000 description 1
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 description 1
- 229940117972 triolein Drugs 0.000 description 1
- 229960001947 tripalmitin Drugs 0.000 description 1
- 230000017260 vegetative to reproductive phase transition of meristem Effects 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/305—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation
- A24B15/307—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances of undetermined constitution characterised by their preparation using microorganisms or enzymes as catalysts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P13/00—Preparation of nitrogen-containing organic compounds
- C12P13/04—Alpha- or beta- amino acids
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/02—Preparation of oxygen-containing organic compounds containing a hydroxy group
- C12P7/22—Preparation of oxygen-containing organic compounds containing a hydroxy group aromatic
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
- C12P7/6409—Fatty acids
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
- C12P7/6409—Fatty acids
- C12P7/6427—Polyunsaturated fatty acids [PUFA], i.e. having two or more double bonds in their backbone
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
- C12P7/6409—Fatty acids
- C12P7/6427—Polyunsaturated fatty acids [PUFA], i.e. having two or more double bonds in their backbone
- C12P7/6431—Linoleic acids [18:2[n-6]]
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/64—Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
- C12P7/6436—Fatty acid esters
- C12P7/6445—Glycerides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Zoology (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Microbiology (AREA)
- Genetics & Genomics (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Toxicology (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
【選択図】なし
Description
i)タバコ属の種の収穫した種子またはその一部を受け取るステップと;
ii)収穫した種子またはその一部を細分して粒子状種子材料を形成するステップ、あるいは収穫した種子またはその一部を、冷間圧縮、溶媒抽出、クロマトグラフィー、蒸留、濾過、再結晶、溶媒−溶媒分配またはこれらの組み合わせに供することにより、収穫した種子から種子単離物を分離するステップの少なくとも一方により、収穫した種子またはその一部を加工するステップと;
iii)ステップii)で製造した粒子状種子材料または種子単離物を、喫煙具または無煙タバコ組成物に使用するのに適したタバコ組成物に添加するステップと
を含む。
Claims (32)
- 喫煙具または無煙タバコ組成物に使用するためのタバコ組成物であって、
タバコ材料と、
タバコ属の種の種子に由来する種子成分と、
を含み、
前記種子成分は、
(i)タバコ属の種の種子もしくは粒子形態のその一部;または
(ii)タバコ属の種の種子に由来する種子単離物
である、タバコ組成物。 - 前記種子成分が、化学的に変換した種子単離物である、請求項1に記載のタバコ組成物。
- 前記化学的に変換した種子単離物が、水素付加、酸/塩基反応、加水分解、熱処理、酵素処理およびこれらの組み合わせからなる群から選択される処理に供した種子単離物である、請求項2に記載のタバコ組成物。
- 前記化学的に変換した種子単離物が、エステル化、エステル交換、異性体転換、アセタール形成、アセタール分解およびこれらの組み合わせからなる群から選択される工程に供した種子単離物である、請求項2に記載のタバコ組成物。
- 前記化学的に変換した種子単離物が、タバコ属の種の種子から単離した水素付加脂質組成物を含む、請求項2に記載のタバコ組成物。
- 前記化学的に変換した種子単離物が、酵素処理した種子材料からの抽出物の形態の種子単離物である、請求項2に記載のタバコ組成物。
- 前記種子成分が、酵素処理した種子成分である、請求項1に記載のタバコ組成物。
- 前記種子成分が、種子から搾り出した脂質を含む種子単離物である、請求項1に記載のタバコ組成物。
- 前記種子成分が、種子材料からの抽出物の形態の種子単離物である、請求項1に記載のタバコ組成物。
- 前記抽出物が、極性溶媒、非極性有機溶媒または超臨界流体を使用して溶媒抽出により形成される、請求項9に記載のタバコ組成物。
- 前記種子単離物が、酵素処理した種子単離物である、請求項9に記載のタバコ組成物。
- 前記種子成分が、溶媒抽出、クロマトグラフィー、蒸留、濾過、冷間圧縮、再結晶、溶媒−溶媒分配およびこれらの組み合わせからなる群から選択される分離工程を使用して形成される種子単離物である、請求項1に記載のタバコ組成物。
- 前記種子成分が、種子材料の溶媒抽出後に残っている種子材料の不溶性残渣の形態の種子単離物である、請求項1に記載のタバコ組成物。
- 前記種子成分が、種子材料を圧縮してそこから脂質を除去した後に残っている種子残渣の形態の種子単離物である、請求項1に記載のタバコ組成物。
- 内部ペイロードを含む1種または複数のカプセルをさらに含み、前記種子成分が、前記内部ペイロード中に含まれる種子単離物である、請求項1に記載のタバコ組成物。
- 前記種子成分が、ケーシング配合物またはトップドレッシングの形態で前記タバコ材料に適用される、請求項1〜15のいずれか一項に記載のタバコ組成物。
- 前記タバコ材料が、再構成タバコ材料である、請求項1〜15のいずれか一項に記載のタバコ組成物。
- 前記タバコ材料が、喫煙具に使用するのに適している、請求項1〜15のいずれか一項に記載のタバコ組成物。
- 請求項18に記載のタバコ組成物を含む喫煙具。
- 前記タバコ材料が、無煙タバコ製品に使用するのに適している、請求項1〜15のいずれか一項に記載のタバコ組成物。
- 請求項20に記載のタバコ組成物を含む無煙タバコ製品。
- 前記タバコ組成物中の種子成分の量が、約5ppmと前記タバコ材料の総乾燥重量基準で約5重量%との間である、請求項18または請求項20のいずれかに記載のタバコ組成物。
- タバコ組成物に添加するためのタバコ属の種の種子に由来する種子単離物を調製する方法であって、
収穫した種子またはその一部を、冷間圧縮、溶媒抽出、クロマトグラフィー、蒸留、濾過、再結晶、溶媒−溶媒分配またはこれらの組み合わせに供することにより、タバコ属の種の収穫した種子の成分を単離して、種子単離物を形成するステップと、
前記単離ステップの前に前記収穫した種子を化学的に変換するまたは前記単離ステップの後に前記種子単離物を化学的に変換するステップであって、前記化学的に変換するステップは、水素付加、酸/塩基反応、加水分解、熱処理、酵素処理またはこれらの組み合わせからなる群から選択される処理であるステップと
を含む、方法。 - 喫煙具または無煙タバコ組成物に使用するのに適したタバコ組成物に化学的に変換した種子単離物を添加するステップをさらに含む、請求項23に記載の方法。
- 前記単離ステップが、溶媒を使用した収穫した種子またはその一部の溶媒抽出を含む、請求項23に記載の方法。
- 前記化学的に変換するステップが、前記収穫した種子またはその一部を酵素処理に供して酵素処理した種子材料を形成するステップを含み、前記単離ステップが、前記酵素処理した種子材料を溶媒抽出に供して化学的に変換した種子単離物を形成するステップを含む、請求項23に記載の方法。
- 前記化学的に変換するステップが、収穫した種子またはその一部を凍結して凍結種子材料を形成するステップと、前記凍結種子を粒子形態に加工するステップと、前記粒子状種子材料を酵素処理に供して前記粒子状種子材料を化学的に変化させるステップとを含み、前記単離ステップが、溶媒で前記粒子状種子材料を抽出して化学的に変換した種子単離物を製造するステップを含む、請求項23に記載の方法。
- 前記化学的に変換するステップが、ヒドロリアーゼ、グリコシダーゼまたはグルコシダーゼによる、前記収穫した種子またはその一部の酵素処理を含む、請求項23に記載の方法。
- 前記単離ステップが、前記収穫した種子から脂質を搾り出して脂質含有種子単離物を形成するために、前記収穫した種子またはその一部を冷間圧縮するステップを含む、請求項23に記載の方法。
- 前記化学的に変換するステップが、前記脂質含有種子単離物中の脂質の飽和度を変えるために、前記脂質含有種子単離物を水素付加に供するステップを含む、請求項29に記載の方法。
- タバコ組成物に添加するためのタバコ属の種の種子に由来する種子単離物を調製する方法であって、
i)タバコ属の種の収穫した種子またはその一部を受け取るステップと;
ii)前記収穫した種子またはその一部を細分して粒子状種子材料を形成するステップ、あるいは前記収穫した種子またはその一部を、冷間圧縮、溶媒抽出、クロマトグラフィー、蒸留、濾過、再結晶、溶媒−溶媒分配またはこれらの組み合わせに供することにより、前記収穫した種子から種子単離物を分離するステップの少なくとも一方により、前記収穫した種子またはその一部を加工するステップと;
iii)ステップii)で製造した前記粒子状種子材料または種子単離物を、喫煙具または無煙タバコ組成物に使用するのに適したタバコ組成物に添加するステップと
を含む、方法。 - 前記分離ステップが、収穫した種子またはその一部を酵素処理に供して酵素処理した種子材料を形成するステップと、前記酵素処理した種子材料を溶媒抽出に供して前記種子単離物を形成するステップとを含む、請求項31に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US12/764,613 | 2010-04-21 | ||
US12/764,613 US9402415B2 (en) | 2010-04-21 | 2010-04-21 | Tobacco seed-derived components and materials |
PCT/US2011/033187 WO2011133633A1 (en) | 2010-04-21 | 2011-04-20 | Tobacco seed-derived components and materials |
Publications (3)
Publication Number | Publication Date |
---|---|
JP2013524813A true JP2013524813A (ja) | 2013-06-20 |
JP2013524813A5 JP2013524813A5 (ja) | 2014-06-05 |
JP6196151B2 JP6196151B2 (ja) | 2017-09-13 |
Family
ID=44315023
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2013506263A Active JP6196151B2 (ja) | 2010-04-21 | 2011-04-20 | タバコ種子由来成分および材料 |
Country Status (6)
Country | Link |
---|---|
US (2) | US9402415B2 (ja) |
EP (1) | EP2560509B1 (ja) |
JP (1) | JP6196151B2 (ja) |
CN (1) | CN102933103B (ja) |
ES (1) | ES2539016T3 (ja) |
WO (1) | WO2011133633A1 (ja) |
Families Citing this family (34)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9402415B2 (en) | 2010-04-21 | 2016-08-02 | R. J. Reynolds Tobacco Company | Tobacco seed-derived components and materials |
US9155321B2 (en) | 2010-08-11 | 2015-10-13 | R.J. Reynolds Tobacco Company | Meltable smokeless tobacco composition |
US9204667B2 (en) | 2010-12-01 | 2015-12-08 | R.J. Reynolds Tobacco Company | Smokeless tobacco pastille and injection molding process for forming smokeless tobacco products |
US9458476B2 (en) | 2011-04-18 | 2016-10-04 | R.J. Reynolds Tobacco Company | Method for producing glycerin from tobacco |
US9192193B2 (en) | 2011-05-19 | 2015-11-24 | R.J. Reynolds Tobacco Company | Molecularly imprinted polymers for treating tobacco material and filtering smoke from smoking articles |
US20130206150A1 (en) | 2012-02-10 | 2013-08-15 | R.J. Reynolds Tobacco Company | Multi-layer smokeless tobacco composition |
US9339058B2 (en) | 2012-04-19 | 2016-05-17 | R. J. Reynolds Tobacco Company | Method for producing microcrystalline cellulose from tobacco and related tobacco product |
US8800571B2 (en) | 2012-06-01 | 2014-08-12 | R.J. Reynolds Tobacco Company | Method and system for moist tobacco extract isolation |
US11412775B2 (en) | 2012-10-09 | 2022-08-16 | R.J. Reynolds Tobacco Company | Tobacco-derived composition |
US9289011B2 (en) | 2013-03-07 | 2016-03-22 | R.J. Reynolds Tobacco Company | Method for producing lutein from tobacco |
US9661876B2 (en) | 2013-03-14 | 2017-05-30 | R.J. Reynolds Tobacco Company | Sugar-enriched extract derived from tobacco |
US9301544B2 (en) | 2013-03-14 | 2016-04-05 | R.J. Reynolds Tobacco Company | Protein-enriched tobacco-derived composition |
US9175052B2 (en) | 2013-05-17 | 2015-11-03 | R.J. Reynolds Tobacco Company | Tobacco-derived protein compositions |
US20140356295A1 (en) | 2013-06-03 | 2014-12-04 | R.J. Reynolds Tobacco Company | Cosmetic compositions comprising tobacco seed-derived component |
US9629391B2 (en) | 2013-08-08 | 2017-04-25 | R.J. Reynolds Tobacco Company | Tobacco-derived pyrolysis oil |
US10357054B2 (en) | 2013-10-16 | 2019-07-23 | R.J. Reynolds Tobacco Company | Smokeless tobacco pastille |
US9265284B2 (en) | 2014-01-17 | 2016-02-23 | R.J. Reynolds Tobacco Company | Process for producing flavorants and related materials |
US9375033B2 (en) | 2014-02-14 | 2016-06-28 | R.J. Reynolds Tobacco Company | Tobacco-containing gel composition |
CN105212260A (zh) * | 2014-05-26 | 2016-01-06 | 何氪 | 一种烟草薄片及卷烟制品 |
US9896429B2 (en) | 2014-05-27 | 2018-02-20 | R.J. Reynolds Tobacco Company | Nicotine salts, co-crystals, and salt co-crystal complexes |
CN113754634A (zh) | 2014-05-27 | 2021-12-07 | R.J.雷诺兹烟草公司 | 烟碱盐、共晶体和盐共晶体络合物 |
US10508096B2 (en) | 2014-05-27 | 2019-12-17 | R.J. Reynolds Tobacco Company | Nicotine salts, co-crystals, and salt co-crystal complexes |
US20160128294A1 (en) * | 2014-11-10 | 2016-05-12 | R.J. Reynolds Tobacco Company | Infused plant seeds |
US10881133B2 (en) | 2015-04-16 | 2021-01-05 | R.J. Reynolds Tobacco Company | Tobacco-derived cellulosic sugar |
US10869497B2 (en) | 2015-09-08 | 2020-12-22 | R.J. Reynolds Tobacco Company | High-pressure cold pasteurization of tobacco material |
WO2017089931A1 (en) | 2015-11-25 | 2017-06-01 | R. J. Reynolds Tobacco Company | Nicotine salts, co-crystals, and salt co-crystal complexes |
US11612183B2 (en) | 2015-12-10 | 2023-03-28 | R.J. Reynolds Tobacco Company | Protein-enriched tobacco composition |
US10499684B2 (en) | 2016-01-28 | 2019-12-10 | R.J. Reynolds Tobacco Company | Tobacco-derived flavorants |
US9795162B2 (en) | 2016-02-08 | 2017-10-24 | R. J. Reynolds Tobacco Company | System for monitoring environmental conditions of a tobacco curing site |
US11091446B2 (en) | 2017-03-24 | 2021-08-17 | R.J. Reynolds Tobacco Company | Methods of selectively forming substituted pyrazines |
GB201707758D0 (en) | 2017-05-15 | 2017-06-28 | British American Tobacco Investments Ltd | Ground tobacco composition |
US10757964B2 (en) | 2017-07-20 | 2020-09-01 | R.J. Reynolds Tobacco Company | Purification of tobacco-derived protein compositions |
WO2019049049A1 (en) | 2017-09-05 | 2019-03-14 | R. J. Reynolds Tobacco Company | SALTS, CO-CRYSTALS, AND CO-CRYSTAL COMPLEXES OF NICOTINE SALTS |
US20190307082A1 (en) | 2018-04-05 | 2019-10-10 | R.J. Reynolds Tobacco Company | Oriental tobacco production methods |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2020538A (en) * | 1978-05-12 | 1979-11-21 | British American Tobacco Co | Improvements relating to smoking-material additives |
JPS5928465A (ja) * | 1982-08-07 | 1984-02-15 | 日本たばこ産業株式会社 | たばこの香喫味改良法 |
JPS5945865A (ja) * | 1982-09-06 | 1984-03-14 | 日本たばこ産業株式会社 | たばこの香喫味改良方法 |
JPS62148439A (ja) * | 1985-12-23 | 1987-07-02 | Japan Tobacco Inc | 新規ジテルペン化合物及び該化合物からなるたばこ用香喫味改良剤 |
US5301694A (en) * | 1991-11-12 | 1994-04-12 | Philip Morris Incorporated | Process for isolating plant extract fractions |
JPH06211885A (ja) * | 1993-01-18 | 1994-08-02 | Japan Tobacco Inc | 新規なジテルペン配糖体および該配糖体を有効成分として含有するたばこ用香喫味改良剤 |
JP2002520005A (ja) * | 1998-07-08 | 2002-07-09 | ノボザイムス アクティーゼルスカブ | タバコの処理におけるフェノール酸化酵素の利用 |
WO2009110775A1 (en) * | 2008-03-05 | 2009-09-11 | Abat Murzagaliyev | Method of medicinal tobacco oil production |
Family Cites Families (182)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1376586A (en) | 1918-04-06 | 1921-05-03 | Schwartz Francis | Tobacco-tablet |
DE1692938A1 (de) | 1966-03-05 | 1972-03-16 | Reemtsma H F & Ph | Verfahren zur Beeinflussung der geschmacklichen Eigenschaften des Tabakrauches |
US3424171A (en) | 1966-08-15 | 1969-01-28 | William A Rooker | Tobacco aromatics enriched nontobacco smokable product and method of making same |
US3696917A (en) | 1970-09-10 | 1972-10-10 | Elaine G Levi | Tobacco pouch closure |
US4045879A (en) | 1973-02-20 | 1977-09-06 | Stork Amsterdam B.V. | Process for treating oil containing vegetable raw materials |
US4009290A (en) | 1974-02-11 | 1977-02-22 | Nisshin Seiyu Kabushiki Kaisha | Method for preparing edible oil |
GB1489761A (en) | 1974-03-08 | 1977-10-26 | Amf Inc | Process of treating tobacco |
US3977415A (en) * | 1975-03-20 | 1976-08-31 | R. J. Reynolds Tobacco Company | Smoking compositions |
AR207144A1 (es) * | 1974-04-15 | 1976-09-15 | Reynolds Tobacco Co R | Material para fumar en forma semejante a relleno de cigarrillos o tabaco cortado para pipa |
US4008210A (en) | 1974-11-05 | 1977-02-15 | Gold Kist Inc. | Solvent extraction of oil from oil seeds |
NL7511125A (nl) | 1975-09-19 | 1977-03-22 | Stork Amsterdam | Werkwijze en installatie voor het winnen van olien uit oliehoudende grondstoffen. |
US4083372A (en) * | 1976-05-24 | 1978-04-11 | Robert Boden | Cigarette-simulating inhaler |
US4150677A (en) | 1977-01-24 | 1979-04-24 | Philip Morris Incorporated | Treatment of tobacco |
US4267847A (en) | 1978-05-12 | 1981-05-19 | British-American Tobacco Company Limited | Tobacco additives |
US4289147A (en) | 1979-11-15 | 1981-09-15 | Leaf Proteins, Inc. | Process for obtaining deproteinized tobacco freed of nicotine and green pigment, for use as a smoking product |
US4589428A (en) | 1980-02-21 | 1986-05-20 | Philip Morris Incorporated | Tobacco treatment |
DE3009031C2 (de) | 1980-03-08 | 1983-04-21 | B.A.T. Cigaretten-Fabriken Gmbh, 2000 Hamburg | Verfahren zur Herstellung von Aromastoffen für Rauchprodukte |
DE3009032C2 (de) | 1980-03-08 | 1983-11-24 | B.A.T. Cigaretten-Fabriken Gmbh, 2000 Hamburg | Verfahren zur Herstellung von Aromastoffen für Rauchprodukte |
US4298540A (en) | 1980-12-15 | 1981-11-03 | Shell Oil Company | Process for oilseed extraction with an isopropanol-based solvent |
US4359417A (en) | 1981-02-25 | 1982-11-16 | Dravo Corporation | Process for extracting oleaginous seed materials particularly cottonseed with aqueous alcohol |
IN158943B (ja) | 1981-12-07 | 1987-02-21 | Mueller Adam | |
US4466923A (en) | 1982-04-01 | 1984-08-21 | The United States Of America As Represented By The Secretary Of Agriculture | Supercritical CO2 extraction of lipids from lipid-containing materials |
US4456556A (en) | 1982-05-07 | 1984-06-26 | Shell Oil Company | Oilseed extraction process |
US4456557A (en) | 1982-05-07 | 1984-06-26 | Shell Oil Company | Oilseed extraction process |
US4528993A (en) | 1982-08-20 | 1985-07-16 | R. J. Reynolds Tobacco Company | Process for producing moist snuff |
US4660577A (en) | 1982-08-20 | 1987-04-28 | R.J. Reynolds Tobacco Company | Dry pre-mix for moist snuff |
US4513756A (en) | 1983-04-28 | 1985-04-30 | The Pinkerton Tobacco Company | Process of making tobacco pellets |
JPS6024172A (ja) | 1983-07-21 | 1985-02-06 | 日本たばこ産業株式会社 | たばこ用香料の製造方法 |
US5092352A (en) | 1983-12-14 | 1992-03-03 | American Brands, Inc. | Chewing tobacco product |
US4515726A (en) | 1984-06-28 | 1985-05-07 | Shell Oil Company | Oilseed extraction process |
US4793365A (en) | 1984-09-14 | 1988-12-27 | R. J. Reynolds Tobacco Company | Smoking article |
US4624269A (en) | 1984-09-17 | 1986-11-25 | The Pinkerton Tobacco Company | Chewable tobacco based product |
US4847106A (en) | 1985-09-30 | 1989-07-11 | Rme Research Associates | Method of pressing sesame seeds |
US5033483A (en) | 1985-10-28 | 1991-07-23 | R. J. Reynolds Tobacco Company | Smoking article with tobacco jacket |
US4917128A (en) | 1985-10-28 | 1990-04-17 | R. J. Reynolds Tobacco Co. | Cigarette |
US4716911A (en) | 1986-04-08 | 1988-01-05 | Genencor, Inc. | Method for protein removal from tobacco |
US4727889A (en) | 1986-12-22 | 1988-03-01 | R. J. Reynolds Tobacco Company | Tobacco processing |
US5018540A (en) | 1986-12-29 | 1991-05-28 | Philip Morris Incorporated | Process for removal of basic materials |
US4830028A (en) * | 1987-02-10 | 1989-05-16 | R. J. Reynolds Tobacco Company | Salts provided from nicotine and organic acid as cigarette additives |
US4819668A (en) | 1987-04-02 | 1989-04-11 | R. J. Reynolds Tobacco Company | Cigarette cut filler containing rare and specialty tobaccos |
US4924888A (en) | 1987-05-15 | 1990-05-15 | R. J. Reynolds Tobacco Company | Smoking article |
US4947974A (en) | 1988-01-15 | 1990-08-14 | Deere & Company | Fast fill hydraulic clutch |
US5005593A (en) | 1988-01-27 | 1991-04-09 | R. J. Reynolds Tobacco Company | Process for providing tobacco extracts |
US5435325A (en) | 1988-04-21 | 1995-07-25 | R. J. Reynolds Tobacco Company | Process for providing tobacco extracts using a solvent in a supercritical state |
US5360023A (en) | 1988-05-16 | 1994-11-01 | R. J. Reynolds Tobacco Company | Cigarette filter |
US5074321A (en) | 1989-09-29 | 1991-12-24 | R. J. Reynolds Tobacco Company | Cigarette |
US4887618A (en) | 1988-05-19 | 1989-12-19 | R. J. Reynolds Tobacco Company | Tobacco processing |
US4987907A (en) | 1988-06-29 | 1991-01-29 | Helme Tobacco Company | Chewing tobacco composition and process for producing same |
US4920990A (en) | 1988-11-23 | 1990-05-01 | R. J. Reynolds Tobacco Company | Cigarette |
US4967771A (en) | 1988-12-07 | 1990-11-06 | R. J. Reynolds Tobacco Company | Process for extracting tobacco |
US5211684A (en) | 1989-01-10 | 1993-05-18 | R. J. Reynolds Tobacco Company | Catalyst containing smoking articles for reducing carbon monoxide |
GB8901579D0 (en) | 1989-01-25 | 1989-03-15 | Imp Tobacco Co Ltd | Improvements to smoking articles |
US4961438A (en) | 1989-04-03 | 1990-10-09 | Brown & Williamson Tobacco Corporation | Smoking device |
US4986286A (en) | 1989-05-02 | 1991-01-22 | R. J. Reynolds Tobacco Company | Tobacco treatment process |
US4941484A (en) | 1989-05-30 | 1990-07-17 | R. J. Reynolds Tobacco Company | Tobacco processing |
DE69013092T2 (de) | 1989-07-20 | 1995-03-02 | Quest Int | Verfahren zur Isolation von Hydroxyfettsäurederivaten aus Convolvulaceae-Pflanzen. |
US5077071A (en) | 1989-09-06 | 1991-12-31 | Epe Incorporated | Oil extrusion process |
US5101839A (en) | 1990-08-15 | 1992-04-07 | R. J. Reynolds Tobacco Company | Cigarette and smokable filler material therefor |
US5056537A (en) | 1989-09-29 | 1991-10-15 | R. J. Reynolds Tobacco Company | Cigarette |
US5121757A (en) | 1989-12-18 | 1992-06-16 | R. J. Reynolds Tobacco Company | Tobacco treatment process |
US5060669A (en) | 1989-12-18 | 1991-10-29 | R. J. Reynolds Tobacco Company | Tobacco treatment process |
US5234008A (en) | 1990-02-23 | 1993-08-10 | R. J. Reynolds Tobacco Company | Tobacco processing |
US5065775A (en) | 1990-02-23 | 1991-11-19 | R. J. Reynolds Tobacco Company | Tobacco processing |
US5131414A (en) | 1990-02-23 | 1992-07-21 | R. J. Reynolds Tobacco Company | Tobacco processing |
US5027837A (en) * | 1990-02-27 | 1991-07-02 | R. J. Reynolds Tobacco Company | Cigarette |
US5183062A (en) | 1990-02-27 | 1993-02-02 | R. J. Reynolds Tobacco Company | Cigarette |
US5099862A (en) | 1990-04-05 | 1992-03-31 | R. J. Reynolds Tobacco Company | Tobacco extraction process |
US5074319A (en) | 1990-04-19 | 1991-12-24 | R. J. Reynolds Tobacco Company | Tobacco extraction process |
US5932095A (en) | 1990-07-13 | 1999-08-03 | Isco, Inc. | Multi-chambered supercritical fluid extraction cartridge |
US5668295A (en) | 1990-11-14 | 1997-09-16 | Philip Morris Incorporated | Protein involved in nicotine synthesis, DNA encoding, and use of sense and antisense DNAs corresponding thereto to affect nicotine content in transgenic tobacco cells and plants |
US5247949A (en) | 1991-01-09 | 1993-09-28 | Philip Morris Incorporated | Method for producing metal carbide heat sources |
US5143097A (en) | 1991-01-28 | 1992-09-01 | R. J. Reynolds Tobacco Company | Tobacco reconstitution process |
US5131415A (en) | 1991-04-04 | 1992-07-21 | R. J. Reynolds Tobacco Company | Tobacco extraction process |
US5197494A (en) | 1991-06-04 | 1993-03-30 | R.J. Reynolds Tobacco Company | Tobacco extraction process |
US5318050A (en) | 1991-06-04 | 1994-06-07 | R. J. Reynolds Tobacco Company | Tobacco treatment process |
US5159942A (en) | 1991-06-04 | 1992-11-03 | R. J. Reynolds Tobacco Company | Process for providing smokable material for a cigarette |
US5343879A (en) | 1991-06-21 | 1994-09-06 | R. J. Reynolds Tobacco Company | Tobacco treatment process |
CA2069687A1 (en) | 1991-06-28 | 1992-12-29 | Chandra Kumar Banerjee | Tobacco smoking article with electrochemical heat source |
US5235992A (en) | 1991-06-28 | 1993-08-17 | R. J. Reynolds Tobacco Company | Processes for producing flavor substances from tobacco and smoking articles made therewith |
US5285798A (en) | 1991-06-28 | 1994-02-15 | R. J. Reynolds Tobacco Company | Tobacco smoking article with electrochemical heat source |
US5178167A (en) | 1991-06-28 | 1993-01-12 | R. J. Reynolds Tobacco Company | Carbonaceous composition for fuel elements of smoking articles and method of modifying the burning characteristics thereof |
US5360022A (en) | 1991-07-22 | 1994-11-01 | R. J. Reynolds Tobacco Company | Tobacco processing |
US5148819A (en) | 1991-08-15 | 1992-09-22 | R. J. Reynolds Tobacco Company | Process for extracting tobacco |
US5243999A (en) | 1991-09-03 | 1993-09-14 | R. J. Reynolds Tobacco Company | Tobacco processing |
US5230354A (en) | 1991-09-03 | 1993-07-27 | R. J. Reynolds Tobacco Company | Tobacco processing |
US5547997A (en) | 1991-10-01 | 1996-08-20 | Chemisches Laboratorium Dr. Kurt Richter Gmbh | Plant-derived cosmetic composition and method of treatment of skin |
US5220930A (en) | 1992-02-26 | 1993-06-22 | R. J. Reynolds Tobacco Company | Cigarette with wrapper having additive package |
JP3681410B2 (ja) | 1992-04-09 | 2005-08-10 | フィリップ・モーリス・プロダクツ・インコーポレイテッド | 再構成タバコシート及びその製造法及び使用法 |
US5445169A (en) | 1992-08-17 | 1995-08-29 | R. J. Reynolds Tobacco Company | Process for providing a tobacco extract |
US5692525A (en) | 1992-09-11 | 1997-12-02 | Philip Morris Incorporated | Cigarette for electrical smoking system |
US5469871A (en) | 1992-09-17 | 1995-11-28 | R. J. Reynolds Tobacco Company | Cigarette and method of making same |
US5397571A (en) | 1993-03-25 | 1995-03-14 | W. R. Grace & Co.-Conn. | Co-extraction of azadirachtin and neem oil |
PH30299A (en) | 1993-04-07 | 1997-02-20 | Reynolds Tobacco Co R | Fuel element composition |
US5468266A (en) | 1993-06-02 | 1995-11-21 | Philip Morris Incorporated | Method for making a carbonaceous heat source containing metal oxide |
US5387416A (en) | 1993-07-23 | 1995-02-07 | R. J. Reynolds Tobacco Company | Tobacco composition |
US5539093A (en) | 1994-06-16 | 1996-07-23 | Fitzmaurice; Wayne P. | DNA sequences encoding enzymes useful in carotenoid biosynthesis |
US5533530A (en) | 1994-09-01 | 1996-07-09 | R. J. Reynolds Tobacco Company | Tobacco reconstitution process |
US5637785A (en) | 1994-12-21 | 1997-06-10 | The Salk Institute For Biological Studies | Genetically modified plants having modulated flower development |
US6083729A (en) | 1995-10-26 | 2000-07-04 | Metabolix, Inc. | Methods for isolating polyhydroxyalkanoates from plants |
US5705624A (en) | 1995-12-27 | 1998-01-06 | Fitzmaurice; Wayne Paul | DNA sequences encoding enzymes useful in phytoene biosynthesis |
US6089857A (en) | 1996-06-21 | 2000-07-18 | Japan Tobacco, Inc. | Heater for generating flavor and flavor generation appliance |
US6591841B1 (en) | 1996-08-01 | 2003-07-15 | Jackie Lee White | Method of providing flavorful and aromatic tobacco suspension |
DE69720508T2 (de) | 1996-10-15 | 2004-03-04 | Rothmans, Benson & Hedges Inc., North York | Vorrichtung zur kontrolle der seitenströmung und der freien brenngeschwindigkeit einer zigarette |
CA2281830C (en) | 1997-03-07 | 2007-06-19 | Prodigene, Inc. | Methods of commercial production and extraction of protein from seed |
EA003066B1 (ru) | 1998-01-06 | 2002-12-26 | Филип Моррис Продактс Инк. | Сигарета с уменьшенным потоком побочного дыма |
US6225483B1 (en) | 1998-06-01 | 2001-05-01 | Henry L Franke | Cold solvent extraction process for extracting oil from oil-bearing materials |
EP0965631B1 (en) | 1998-06-05 | 2013-04-17 | Consejo Superior De Investigaciones Cientificas | High stable vegetable oils |
US6095153A (en) | 1998-06-19 | 2000-08-01 | Kessler; Stephen B. | Vaporization of volatile materials |
US6298859B1 (en) | 1998-07-08 | 2001-10-09 | Novozymes A/S | Use of a phenol oxidizing enzyme in the treatment of tobacco |
US6298858B1 (en) | 1998-11-18 | 2001-10-09 | R. J. Reynolds Tobacco Company | Tobacco flavoring components of enhanced aromatic content and method of providing same |
US6428624B1 (en) | 1998-12-07 | 2002-08-06 | R. J. Reynolds Tobacco Co. | Method of providing flavorful and aromatic compounds |
GB2352724B (en) | 1999-08-05 | 2003-03-12 | Naturol Ltd | A novel process for preparing fine extracts and oils from plants and other matter |
US7156981B2 (en) | 1999-01-25 | 2007-01-02 | Bio Extraction Limited | ITFM extraction of oil seeds |
WO2000054608A1 (de) | 1999-03-17 | 2000-09-21 | Fraunhofer Gesellschaft zur Förderung der angewandten Forschung e.V. | Verfahren zur behandlung und verarbeitung alkaloid-, öl- und proteinhaltiger lupinensamen |
US6131584A (en) | 1999-04-15 | 2000-10-17 | Brown & Williamson Tobacco Corporation | Tobacco treatment process |
US6805134B2 (en) | 1999-04-26 | 2004-10-19 | R. J. Reynolds Tobacco Company | Tobacco processing |
US6403126B1 (en) | 1999-05-26 | 2002-06-11 | Websar Innovations Inc. | Cannabinoid extraction method |
US6216706B1 (en) | 1999-05-27 | 2001-04-17 | Philip Morris Incorporated | Method and apparatus for producing reconstituted tobacco sheets |
US6311694B1 (en) | 1999-07-02 | 2001-11-06 | Philip Morris Incorporated | Smoking article having reduced sidestream smoke |
US6214351B1 (en) | 1999-08-27 | 2001-04-10 | Morinda, Inc. | Morinda citrifolia oil |
US6547987B1 (en) | 2000-01-25 | 2003-04-15 | University Of Missouri Board Of Curators | Solvent and method for extraction of triglyceride rich oil |
IN192689B (ja) | 2000-02-14 | 2004-05-15 | Rao Gariimella Bhaskar Dr | |
US6325860B1 (en) | 2000-02-15 | 2001-12-04 | R. J. Reynolds Tobacco Company | Method of providing flavorful and aromatic compounds in absence of reducing sugars |
US6440223B1 (en) | 2000-02-15 | 2002-08-27 | R. J. Reynolds Tobacco Co. | Smoking article containing heat activatable flavorant-generating material |
US6861077B1 (en) | 2000-03-17 | 2005-03-01 | L'oreal S.A. | Use of plant extracts in a cosmetic composition to protect keratinous fibers |
AU2001261532A1 (en) | 2000-05-11 | 2001-11-20 | Phlip Morris Products, Inc. | Cigarette with smoke constituent attenuator |
US6499489B1 (en) | 2000-05-12 | 2002-12-31 | R. J. Reynolds Tobacco Company | Tobacco-based cooked casing formulation |
JP2004507250A (ja) | 2000-08-30 | 2004-03-11 | ノース・キャロライナ・ステイト・ユニヴァーシティ | タンパク質含量を変化させる分子デコイを含有するトランスジェニック植物 |
US20020155177A1 (en) | 2000-09-29 | 2002-10-24 | Krasutsky Pavel A. | Process for extracting compounds from plants |
WO2002037990A2 (en) | 2000-11-10 | 2002-05-16 | Vector Tobacco Ltd. | Method and product for removing carcinogens from tobacco smoke |
ES2380178T3 (es) | 2001-03-08 | 2012-05-09 | Michigan State University | Reguladores del metabolismo de lípidos en plantas |
AU2002308524B2 (en) | 2001-05-01 | 2006-10-12 | Regent Court Technologies, Llc | Smokeless tobacco product |
US6668839B2 (en) | 2001-05-01 | 2003-12-30 | Jonnie R. Williams | Smokeless tobacco product |
US20040020503A1 (en) | 2001-05-01 | 2004-02-05 | Williams Jonnie R. | Smokeless tobacco product |
US7208659B2 (en) | 2001-05-02 | 2007-04-24 | Conopco Inc. | Process for increasing the flavonoid content of a plant and plants obtainable thereby |
US6730832B1 (en) | 2001-09-10 | 2004-05-04 | Luis Mayan Dominguez | High threonine producing lines of Nicotiana tobacum and methods for producing |
US7032601B2 (en) | 2001-09-28 | 2006-04-25 | U.S. Smokeless Tobacco Company | Encapsulated materials |
US6953040B2 (en) | 2001-09-28 | 2005-10-11 | U.S. Smokeless Tobacco Company | Tobacco mint plant material product |
NZ516876A (en) | 2002-01-28 | 2004-05-28 | New Zealand Botan Oils Ltd | A method of producing an oil extract from the seeds of the plants meadowfoam, brassicas and crambe and its use in skin conditions e.g. eczema, psoriasis and burns |
US7105173B1 (en) | 2002-03-21 | 2006-09-12 | Rolling Kenneth J | Nicotine replacement applique |
US6772767B2 (en) | 2002-09-09 | 2004-08-10 | Brown & Williamson Tobacco Corporation | Process for reducing nitrogen containing compounds and lignin in tobacco |
US7025066B2 (en) | 2002-10-31 | 2006-04-11 | Jerry Wayne Lawson | Method of reducing the sucrose ester concentration of a tobacco mixture |
US20040173228A1 (en) | 2003-03-04 | 2004-09-09 | R. J. Reynolds Tobacco Company | Method for producing flavorful and aromatic compounds from tobacco |
AU2003252766A1 (en) | 2003-03-12 | 2004-09-30 | Gao Shen Sdn. Bhd. | Integrated process for separation of oil, protein, carbohydrates, shell and minor toxic components from seeds |
SE0301244D0 (sv) | 2003-04-29 | 2003-04-29 | Swedish Match North Europe Ab | Smokeless tobacco product user package |
US7836895B2 (en) | 2003-06-23 | 2010-11-23 | R. J. Reynolds Tobacco Company | Filtered cigarette incorporating a breakable capsule |
AR045076A1 (es) | 2003-07-24 | 2005-10-12 | Smithkline Beecham Plc | Composicion de pelicula que se disuelve oralmente, pelicula multicomponente que se disuelve oralmente, uso de la composicion de pelicula y de la pelicula que se disuelve oralmente para preparar un medicamento, forma de dosificacion oral y procedimiento para preparar la composicion de pelicula que se |
SE527350C8 (sv) | 2003-08-18 | 2006-03-21 | Gallaher Snus Ab | Lock till snusdosa |
US8066011B2 (en) | 2003-09-30 | 2011-11-29 | R. J. Reynolds Tobacco Company | Filtered cigarette incorporating an adsorbent material |
CN1878480A (zh) | 2003-11-03 | 2006-12-13 | 美国无烟烟草公司 | 加香的无烟烟草及制备方法 |
US8627828B2 (en) | 2003-11-07 | 2014-01-14 | U.S. Smokeless Tobacco Company Llc | Tobacco compositions |
EP1691631A4 (en) | 2003-11-07 | 2012-09-05 | Us Smokeless Tobacco Co | TOBACCO COMPOSITIONS |
WO2005063060A1 (en) | 2003-12-22 | 2005-07-14 | U.S. Smokeless Tobacco Company | Conditioning process for tobacco and/or snuff compositions |
ITRM20040177A1 (it) | 2004-04-07 | 2004-07-07 | Atika Soulimani | Miscela cosmetica per capelli. |
EP1765309B1 (en) | 2004-07-02 | 2009-08-05 | Radi Medical Biodegradable AB | Smokeless toabacco product |
US7337782B2 (en) | 2004-08-18 | 2008-03-04 | R.J. Reynolds Tobacco Company | Process to remove protein and other biomolecules from tobacco extract or slurry |
EP1781123A1 (en) | 2004-08-23 | 2007-05-09 | U.S. Smokeless Tobacco Company | Nicotiana compositions |
US7650891B1 (en) | 2004-09-03 | 2010-01-26 | Rosswil Llc Ltd. | Tobacco precursor product |
EP1827123B1 (en) | 2004-11-04 | 2015-07-22 | Monsanto Technology, LLC | High pufa oil compositions |
WO2007012980A1 (en) | 2005-06-01 | 2007-02-01 | Philip Morris Products S.A. | Tobacco with an increased level of natural tar dilutents |
WO2006136197A1 (en) | 2005-06-21 | 2006-12-28 | V. Mane Fils | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
US7861728B2 (en) * | 2006-02-10 | 2011-01-04 | R.J. Reynolds Tobacco Company | Smokeless tobacco composition having an outer and inner pouch |
US20070062549A1 (en) | 2005-09-22 | 2007-03-22 | Holton Darrell E Jr | Smokeless tobacco composition |
US7819124B2 (en) | 2006-01-31 | 2010-10-26 | U.S. Smokeless Tobacco Company | Tobacco articles and methods |
US7810507B2 (en) | 2006-02-10 | 2010-10-12 | R. J. Reynolds Tobacco Company | Smokeless tobacco composition |
CN101415808B (zh) | 2006-04-10 | 2011-10-05 | R.J.雷诺兹烟草公司 | 从肉豆蔻油选择性除去黄樟素的方法 |
US20080173317A1 (en) | 2006-08-01 | 2008-07-24 | John Howard Robinson | Smokeless tobacco |
US20080029116A1 (en) | 2006-08-01 | 2008-02-07 | John Howard Robinson | Smokeless tobacco |
US20080029117A1 (en) | 2006-08-01 | 2008-02-07 | John-Paul Mua | Smokeless Tobacco |
US7726320B2 (en) | 2006-10-18 | 2010-06-01 | R. J. Reynolds Tobacco Company | Tobacco-containing smoking article |
US20100040758A1 (en) | 2006-12-28 | 2010-02-18 | Chitra Vasant Savngikar | Integrated production of phytochemical rich plant products or isolates from green vegetation |
EP2129243A4 (en) | 2007-02-23 | 2010-08-04 | Us Smokeless Tobacco Co | NEW TOBACCO COMPOSITIONS AND MANUFACTURING METHOD THEREFOR |
ITRM20070129A1 (it) | 2007-03-14 | 2008-09-15 | Plantechno S R L | Piante di tabacco mutagenizzate come coltura da seme per la produzioe di olio da usare ai fini energetici industriali e alimentari |
WO2008119556A2 (en) | 2007-04-03 | 2008-10-09 | Medizinische Universität Wien | A process to activate extracts derived from living organisms using long wave uv irradiation and compositions comprising said activated extract |
US8186360B2 (en) | 2007-04-04 | 2012-05-29 | R.J. Reynolds Tobacco Company | Cigarette comprising dark air-cured tobacco |
US7972254B2 (en) | 2007-06-11 | 2011-07-05 | R.J. Reynolds Tobacco Company | Apparatus for inserting objects into a filter component of a smoking article, and associated method |
FR2922763B1 (fr) | 2007-10-31 | 2012-12-07 | Oreal | Composition cosmetique contenant un agent tenseur et un polymere acrylique. |
US8336557B2 (en) | 2007-11-28 | 2012-12-25 | Philip Morris Usa Inc. | Smokeless compressed tobacco product for oral consumption |
US20100037903A1 (en) | 2008-08-14 | 2010-02-18 | R. J. Reynolds Tobacco Company | Method for Preparing Flavorful and Aromatic Compounds |
CN101361590B (zh) * | 2008-09-28 | 2012-06-06 | 河南中烟工业有限责任公司 | 韭菜籽提取物在卷烟中的应用 |
EA200900693A1 (ru) | 2009-02-16 | 2009-12-30 | Олег Михайлович ЛИ | Способ получения табачного масла |
US9402415B2 (en) | 2010-04-21 | 2016-08-02 | R. J. Reynolds Tobacco Company | Tobacco seed-derived components and materials |
-
2010
- 2010-04-21 US US12/764,613 patent/US9402415B2/en active Active
-
2011
- 2011-04-20 ES ES11719113.0T patent/ES2539016T3/es active Active
- 2011-04-20 EP EP11719113.0A patent/EP2560509B1/en active Active
- 2011-04-20 JP JP2013506263A patent/JP6196151B2/ja active Active
- 2011-04-20 WO PCT/US2011/033187 patent/WO2011133633A1/en active Application Filing
- 2011-04-20 CN CN201180027662.2A patent/CN102933103B/zh active Active
-
2016
- 2016-07-14 US US15/209,981 patent/US10028522B2/en active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB2020538A (en) * | 1978-05-12 | 1979-11-21 | British American Tobacco Co | Improvements relating to smoking-material additives |
JPS5928465A (ja) * | 1982-08-07 | 1984-02-15 | 日本たばこ産業株式会社 | たばこの香喫味改良法 |
JPS5945865A (ja) * | 1982-09-06 | 1984-03-14 | 日本たばこ産業株式会社 | たばこの香喫味改良方法 |
JPS62148439A (ja) * | 1985-12-23 | 1987-07-02 | Japan Tobacco Inc | 新規ジテルペン化合物及び該化合物からなるたばこ用香喫味改良剤 |
US5301694A (en) * | 1991-11-12 | 1994-04-12 | Philip Morris Incorporated | Process for isolating plant extract fractions |
JPH06211885A (ja) * | 1993-01-18 | 1994-08-02 | Japan Tobacco Inc | 新規なジテルペン配糖体および該配糖体を有効成分として含有するたばこ用香喫味改良剤 |
JP2002520005A (ja) * | 1998-07-08 | 2002-07-09 | ノボザイムス アクティーゼルスカブ | タバコの処理におけるフェノール酸化酵素の利用 |
WO2009110775A1 (en) * | 2008-03-05 | 2009-09-11 | Abat Murzagaliyev | Method of medicinal tobacco oil production |
Also Published As
Publication number | Publication date |
---|---|
CN102933103A (zh) | 2013-02-13 |
US9402415B2 (en) | 2016-08-02 |
ES2539016T3 (es) | 2015-06-25 |
EP2560509A1 (en) | 2013-02-27 |
US20110259353A1 (en) | 2011-10-27 |
US10028522B2 (en) | 2018-07-24 |
CN102933103B (zh) | 2015-08-19 |
EP2560509B1 (en) | 2015-04-08 |
US20160316814A1 (en) | 2016-11-03 |
WO2011133633A1 (en) | 2011-10-27 |
JP6196151B2 (ja) | 2017-09-13 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JP6196151B2 (ja) | タバコ種子由来成分および材料 | |
US10561168B2 (en) | Tobacco-derived components and materials | |
JP6085478B2 (ja) | タバコ由来の成分および材料 | |
US20120211016A1 (en) | Plastic from tobacco biomass | |
US9458476B2 (en) | Method for producing glycerin from tobacco | |
US10188137B2 (en) | Process for producing flavorants and related materials | |
US9289011B2 (en) | Method for producing lutein from tobacco | |
EP2780314B1 (en) | Method for producing triethyl citrate from tobacco | |
US20150189911A1 (en) | Method for Producing Triacetin from Tobaccl |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20140416 |
|
A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20140416 |
|
A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20150529 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20150707 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20151005 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20160105 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20160705 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20160929 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20161226 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20170124 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20170418 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20170720 |
|
TRDD | Decision of grant or rejection written | ||
A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20170725 |
|
A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20170817 |
|
R150 | Certificate of patent or registration of utility model |
Ref document number: 6196151 Country of ref document: JP Free format text: JAPANESE INTERMEDIATE CODE: R150 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |