JP2013503924A - イソシアナート不含のシラン架橋性組成物 - Google Patents
イソシアナート不含のシラン架橋性組成物 Download PDFInfo
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- JP2013503924A JP2013503924A JP2012527251A JP2012527251A JP2013503924A JP 2013503924 A JP2013503924 A JP 2013503924A JP 2012527251 A JP2012527251 A JP 2012527251A JP 2012527251 A JP2012527251 A JP 2012527251A JP 2013503924 A JP2013503924 A JP 2013503924A
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- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 2
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- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 description 2
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- WUFHQGLVNNOXMP-UHFFFAOYSA-N n-(triethoxysilylmethyl)cyclohexanamine Chemical compound CCO[Si](OCC)(OCC)CNC1CCCCC1 WUFHQGLVNNOXMP-UHFFFAOYSA-N 0.000 description 2
- QRANWKHEGLJBQC-UHFFFAOYSA-N n-(trimethoxysilylmethyl)cyclohexanamine Chemical compound CO[Si](OC)(OC)CNC1CCCCC1 QRANWKHEGLJBQC-UHFFFAOYSA-N 0.000 description 2
- REODOQPOCJZARG-UHFFFAOYSA-N n-[[diethoxy(methyl)silyl]methyl]cyclohexanamine Chemical compound CCO[Si](C)(OCC)CNC1CCCCC1 REODOQPOCJZARG-UHFFFAOYSA-N 0.000 description 2
- COFBOACTGSWMJQ-UHFFFAOYSA-N n-[[dimethoxy(methyl)silyl]methyl]cyclohexanamine Chemical compound CO[Si](C)(OC)CNC1CCCCC1 COFBOACTGSWMJQ-UHFFFAOYSA-N 0.000 description 2
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- POILWHVDKZOXJZ-ARJAWSKDSA-M (z)-4-oxopent-2-en-2-olate Chemical compound C\C([O-])=C\C(C)=O POILWHVDKZOXJZ-ARJAWSKDSA-M 0.000 description 1
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- ARYZCSRUUPFYMY-UHFFFAOYSA-N methoxysilane Chemical compound CO[SiH3] ARYZCSRUUPFYMY-UHFFFAOYSA-N 0.000 description 1
- INJVFBCDVXYHGQ-UHFFFAOYSA-N n'-(3-triethoxysilylpropyl)ethane-1,2-diamine Chemical compound CCO[Si](OCC)(OCC)CCCNCCN INJVFBCDVXYHGQ-UHFFFAOYSA-N 0.000 description 1
- PHQOGHDTIVQXHL-UHFFFAOYSA-N n'-(3-trimethoxysilylpropyl)ethane-1,2-diamine Chemical compound CO[Si](OC)(OC)CCCNCCN PHQOGHDTIVQXHL-UHFFFAOYSA-N 0.000 description 1
- MQWFLKHKWJMCEN-UHFFFAOYSA-N n'-[3-[dimethoxy(methyl)silyl]propyl]ethane-1,2-diamine Chemical compound CO[Si](C)(OC)CCCNCCN MQWFLKHKWJMCEN-UHFFFAOYSA-N 0.000 description 1
- YFBFAHMPVMWKIM-UHFFFAOYSA-N n-(3-triethoxysilylpropyl)cyclohexanamine Chemical compound CCO[Si](OCC)(OCC)CCCNC1CCCCC1 YFBFAHMPVMWKIM-UHFFFAOYSA-N 0.000 description 1
- KGNDVXPHQJMHLX-UHFFFAOYSA-N n-(3-trimethoxysilylpropyl)cyclohexanamine Chemical compound CO[Si](OC)(OC)CCCNC1CCCCC1 KGNDVXPHQJMHLX-UHFFFAOYSA-N 0.000 description 1
- BNQFLOSSLHYGLQ-UHFFFAOYSA-N n-[[dimethoxy(methyl)silyl]methyl]aniline Chemical compound CO[Si](C)(OC)CNC1=CC=CC=C1 BNQFLOSSLHYGLQ-UHFFFAOYSA-N 0.000 description 1
- SLYCYWCVSGPDFR-UHFFFAOYSA-N octadecyltrimethoxysilane Chemical compound CCCCCCCCCCCCCCCCCC[Si](OC)(OC)OC SLYCYWCVSGPDFR-UHFFFAOYSA-N 0.000 description 1
- MSRJTTSHWYDFIU-UHFFFAOYSA-N octyltriethoxysilane Chemical compound CCCCCCCC[Si](OCC)(OCC)OCC MSRJTTSHWYDFIU-UHFFFAOYSA-N 0.000 description 1
- 229960003493 octyltriethoxysilane Drugs 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- UKODFQOELJFMII-UHFFFAOYSA-N pentamethyldiethylenetriamine Chemical compound CN(C)CCN(C)CCN(C)C UKODFQOELJFMII-UHFFFAOYSA-N 0.000 description 1
- 125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical class OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920002857 polybutadiene Polymers 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920002689 polyvinyl acetate Polymers 0.000 description 1
- 239000011118 polyvinyl acetate Substances 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- HKJYVRJHDIPMQB-UHFFFAOYSA-N propan-1-olate;titanium(4+) Chemical compound CCCO[Ti](OCCC)(OCCC)OCCC HKJYVRJHDIPMQB-UHFFFAOYSA-N 0.000 description 1
- RLJWTAURUFQFJP-UHFFFAOYSA-N propan-2-ol;titanium Chemical compound [Ti].CC(C)O.CC(C)O.CC(C)O.CC(C)O RLJWTAURUFQFJP-UHFFFAOYSA-N 0.000 description 1
- 230000001698 pyrogenic effect Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 230000001603 reducing effect Effects 0.000 description 1
- 230000001235 sensitizing effect Effects 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- VXUYXOFXAQZZMF-UHFFFAOYSA-N tetraisopropyl titanate Substances CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- IMFACGCPASFAPR-UHFFFAOYSA-N tributylamine Chemical compound CCCCN(CCCC)CCCC IMFACGCPASFAPR-UHFFFAOYSA-N 0.000 description 1
- JXUKBNICSRJFAP-UHFFFAOYSA-N triethoxy-[3-(oxiran-2-ylmethoxy)propyl]silane Chemical compound CCO[Si](OCC)(OCC)CCCOCC1CO1 JXUKBNICSRJFAP-UHFFFAOYSA-N 0.000 description 1
- QQQSFSZALRVCSZ-UHFFFAOYSA-N triethoxysilane Chemical compound CCO[SiH](OCC)OCC QQQSFSZALRVCSZ-UHFFFAOYSA-N 0.000 description 1
- IMNIMPAHZVJRPE-UHFFFAOYSA-N triethylenediamine Chemical compound C1CN2CCN1CC2 IMNIMPAHZVJRPE-UHFFFAOYSA-N 0.000 description 1
- 239000013638 trimer Substances 0.000 description 1
- PPUHSHGIVZSPFO-UHFFFAOYSA-N trimethoxy(nonadecyl)silane Chemical compound CCCCCCCCCCCCCCCCCCC[Si](OC)(OC)OC PPUHSHGIVZSPFO-UHFFFAOYSA-N 0.000 description 1
- JEPXSTGVAHHRBD-UHFFFAOYSA-N trimethoxy(nonyl)silane Chemical compound CCCCCCCCC[Si](OC)(OC)OC JEPXSTGVAHHRBD-UHFFFAOYSA-N 0.000 description 1
- NMEPHPOFYLLFTK-UHFFFAOYSA-N trimethoxy(octyl)silane Chemical compound CCCCCCCC[Si](OC)(OC)OC NMEPHPOFYLLFTK-UHFFFAOYSA-N 0.000 description 1
- LCXXOYOABWDYBF-UHFFFAOYSA-N trimethoxy(pentadecyl)silane Chemical compound CCCCCCCCCCCCCCC[Si](OC)(OC)OC LCXXOYOABWDYBF-UHFFFAOYSA-N 0.000 description 1
- AXNJHBYHBDPTQF-UHFFFAOYSA-N trimethoxy(tetradecyl)silane Chemical compound CCCCCCCCCCCCCC[Si](OC)(OC)OC AXNJHBYHBDPTQF-UHFFFAOYSA-N 0.000 description 1
- QSYYSIXGDAAPNN-UHFFFAOYSA-N trimethoxy(tridecyl)silane Chemical compound CCCCCCCCCCCCC[Si](OC)(OC)OC QSYYSIXGDAAPNN-UHFFFAOYSA-N 0.000 description 1
- LIJFLHYUSJKHKV-UHFFFAOYSA-N trimethoxy(undecyl)silane Chemical compound CCCCCCCCCCC[Si](OC)(OC)OC LIJFLHYUSJKHKV-UHFFFAOYSA-N 0.000 description 1
- YUYCVXFAYWRXLS-UHFFFAOYSA-N trimethoxysilane Chemical compound CO[SiH](OC)OC YUYCVXFAYWRXLS-UHFFFAOYSA-N 0.000 description 1
- UKRDPEFKFJNXQM-UHFFFAOYSA-N vinylsilane Chemical class [SiH3]C=C UKRDPEFKFJNXQM-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L101/00—Compositions of unspecified macromolecular compounds
- C08L101/02—Compositions of unspecified macromolecular compounds characterised by the presence of specified groups, e.g. terminal or pendant functional groups
- C08L101/10—Compositions of unspecified macromolecular compounds characterised by the presence of specified groups, e.g. terminal or pendant functional groups containing hydrolysable silane groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/32—Polymers modified by chemical after-treatment
- C08G65/329—Polymers modified by chemical after-treatment with organic compounds
- C08G65/336—Polymers modified by chemical after-treatment with organic compounds containing silicon
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/24—Crosslinking, e.g. vulcanising, of macromolecules
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J201/00—Adhesives based on unspecified macromolecular compounds
- C09J201/02—Adhesives based on unspecified macromolecular compounds characterised by the presence of specified groups, e.g. terminal or pendant functional groups
- C09J201/10—Adhesives based on unspecified macromolecular compounds characterised by the presence of specified groups, e.g. terminal or pendant functional groups containing hydrolysable silane groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- General Chemical & Material Sciences (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Polyurethanes Or Polyureas (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Silicon Polymers (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102009029200A DE102009029200A1 (de) | 2009-09-04 | 2009-09-04 | Isocyanatfreie silanvernetzende Zusammensetzungen |
| DE102009029200.4 | 2009-09-04 | ||
| PCT/EP2010/054811 WO2011026658A1 (de) | 2009-09-04 | 2010-04-13 | Isocyanatfreie silanvernetzende zusammensetzungen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2013503924A true JP2013503924A (ja) | 2013-02-04 |
| JP2013503924A5 JP2013503924A5 (enExample) | 2013-12-19 |
Family
ID=42335064
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012527251A Pending JP2013503924A (ja) | 2009-09-04 | 2010-04-13 | イソシアナート不含のシラン架橋性組成物 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20120165493A1 (enExample) |
| EP (1) | EP2473545B3 (enExample) |
| JP (1) | JP2013503924A (enExample) |
| KR (1) | KR20120061960A (enExample) |
| CN (1) | CN102482408A (enExample) |
| DE (1) | DE102009029200A1 (enExample) |
| WO (1) | WO2011026658A1 (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102010028143A1 (de) | 2010-04-23 | 2011-10-27 | Wacker Chemie Ag | Beschichtungszusammensetzung zum Abdichten von Oberflächen |
| DE102011006128A1 (de) * | 2011-03-25 | 2012-09-27 | Wacker Chemie Ag | Vernetzbare Massen auf Basis von Organyloxysilanterminierten Polymeren |
| DE102011081264A1 (de) | 2011-08-19 | 2013-02-21 | Wacker Chemie Ag | Vernetzbare Massen auf Basis von organyloxysilanterminierten Polymeren |
| DE102011087603A1 (de) | 2011-12-01 | 2013-06-06 | Wacker Chemie Ag | Vernetzbare Massen auf Basis von organyloxysilanterminierten Polyurethanen |
| DE102011087604A1 (de) | 2011-12-01 | 2013-06-06 | Wacker Chemie Ag | Vernetzbare Massen auf Basis von organyloxysilanterminierten Polyurethanen |
| DE102012201734A1 (de) | 2012-02-06 | 2013-08-08 | Wacker Chemie Ag | Massen auf Basis von organyloxysilanterminierten Polymeren |
| DE102012214427A1 (de) | 2012-08-14 | 2014-02-20 | Wacker Chemie Ag | Mehrkomponentige vernetzbare Massen auf Basis von organyloxy-silanterminierten Polymeren |
| DE102013216787A1 (de) | 2013-08-23 | 2015-02-26 | Evonik Degussa Gmbh | Guanidingruppen aufweisende semi-organische Siliciumgruppen enthaltende Verbindungen |
| US9856345B2 (en) * | 2014-03-19 | 2018-01-02 | Vladimyr Wolan | Low viscosity dimethoxy amino silane polyurethane with triethoxy silyl groups for sealants and adhesives with easy processing, high tensile strength and low methanol emissions on curing |
| DE102016200704A1 (de) * | 2016-01-20 | 2017-07-20 | Bona Gmbh Deutschland | Verfahren zur Erhöhung der Anwendungssicherheit und der Alterungsbeständigkeit von Klebstoffen und anderen Produkten, enthaltend silanfunktionalisierte Präpolymere |
| WO2019094414A1 (en) | 2017-11-07 | 2019-05-16 | Henkel IP & Holding GmbH | Silane modified polymers and use of the same in adhesive compositions |
| US12441832B2 (en) | 2019-07-15 | 2025-10-14 | Arkema France | Isocyanate-free laminating adhesive |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005501146A (ja) * | 2001-08-28 | 2005-01-13 | コンゾルテイウム フユール エレクトロケミツシエ インヅストリー ゲゼルシヤフト ミツト ベシユレンクテル ハフツング | アルコキシシラン末端のポリマーを含有する速硬性１成分混合物 |
| JP2005139452A (ja) * | 2003-11-06 | 2005-06-02 | Wacker Chemie Gmbh | 湿分硬化エラストマーの弾性を上昇させる方法 |
| JP2009508989A (ja) * | 2005-09-16 | 2009-03-05 | モーメンティブ・パフォーマンス・マテリアルズ・インク | シラン含有接着促進組成物、並びにそれを含有するシーラント、接着剤及びコーティング |
| JP2009513734A (ja) * | 2003-07-04 | 2009-04-02 | ワッカー ケミー アクチエンゲゼルシャフト | アルコキシシラン末端基を有するプレポリマー |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1998040439A1 (en) * | 1997-03-14 | 1998-09-17 | Minnesota Mining And Manufacturing Company | Cure-on-demand, moisture-curable compositions having reactive silane functionality |
| US5990257A (en) * | 1998-01-22 | 1999-11-23 | Witco Corporation | Process for producing prepolymers which cure to improved sealants, and products formed thereby |
| DE19923300A1 (de) * | 1999-05-21 | 2000-11-23 | Bayer Ag | Phosphatstabilisierte, kondensationsvernetzende Polyurethanmassen, ein Verfahren zu ihrer Herstellung sowie ihre Verwendung |
| US6310170B1 (en) * | 1999-08-17 | 2001-10-30 | Ck Witco Corporation | Compositions of silylated polymer and aminosilane adhesion promoters |
| US6279632B1 (en) * | 1999-11-24 | 2001-08-28 | Bridgestone Corporation | Method to control increase in viscosity during aging of siloxane modified polymers |
| WO2002066532A1 (de) * | 2001-02-20 | 2002-08-29 | Consortium für elektrochemische Industrie GmbH | Isocyanatfrie schäumbare mischungen mit hoher härtungsgeschwindigkeit |
| DE10139132A1 (de) | 2001-08-09 | 2003-02-27 | Consortium Elektrochem Ind | Alkoxyvernetzende einkomponentige feuchtigkeitshärtende Massen |
| DE10328844A1 (de) * | 2003-06-26 | 2005-02-03 | Consortium für elektrochemische Industrie GmbH | Alkoxysilanterminierte Prepolymere |
| BRPI0707252A2 (pt) * | 2006-01-26 | 2011-04-26 | Sika Technology Ag | composições endurecìveis por umidade contendo polìmeros silano funcionais com boa aderência |
| DE102007056524A1 (de) * | 2007-11-22 | 2009-05-28 | Henkel Ag & Co. Kgaa | Härtbare Zusammensetzungen aus Trimethoxysilanen |
| DE102007058483A1 (de) * | 2007-12-04 | 2009-06-10 | Henkel Ag & Co. Kgaa | Härtbare Zusammensetzungen enthaltend silylierte Polyurethane |
| KR101443951B1 (ko) * | 2007-12-12 | 2014-09-23 | 라이온 가부시키가이샤 | 살균 청정제 조성물 |
-
2009
- 2009-09-04 DE DE102009029200A patent/DE102009029200A1/de not_active Withdrawn
-
2010
- 2010-04-13 KR KR1020127008778A patent/KR20120061960A/ko not_active Abandoned
- 2010-04-13 JP JP2012527251A patent/JP2013503924A/ja active Pending
- 2010-04-13 US US13/394,161 patent/US20120165493A1/en not_active Abandoned
- 2010-04-13 EP EP10717083.9A patent/EP2473545B3/de active Active
- 2010-04-13 WO PCT/EP2010/054811 patent/WO2011026658A1/de not_active Ceased
- 2010-04-13 CN CN201080039292XA patent/CN102482408A/zh active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005501146A (ja) * | 2001-08-28 | 2005-01-13 | コンゾルテイウム フユール エレクトロケミツシエ インヅストリー ゲゼルシヤフト ミツト ベシユレンクテル ハフツング | アルコキシシラン末端のポリマーを含有する速硬性１成分混合物 |
| JP2009513734A (ja) * | 2003-07-04 | 2009-04-02 | ワッカー ケミー アクチエンゲゼルシャフト | アルコキシシラン末端基を有するプレポリマー |
| JP2005139452A (ja) * | 2003-11-06 | 2005-06-02 | Wacker Chemie Gmbh | 湿分硬化エラストマーの弾性を上昇させる方法 |
| JP2009508989A (ja) * | 2005-09-16 | 2009-03-05 | モーメンティブ・パフォーマンス・マテリアルズ・インク | シラン含有接着促進組成物、並びにそれを含有するシーラント、接着剤及びコーティング |
Also Published As
| Publication number | Publication date |
|---|---|
| DE102009029200A1 (de) | 2011-03-17 |
| EP2473545B3 (de) | 2016-08-31 |
| CN102482408A (zh) | 2012-05-30 |
| EP2473545A1 (de) | 2012-07-11 |
| KR20120061960A (ko) | 2012-06-13 |
| EP2473545B1 (de) | 2013-07-03 |
| US20120165493A1 (en) | 2012-06-28 |
| WO2011026658A1 (de) | 2011-03-10 |
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