JP2013033250A - ビアリールポリカーボネート中間転写部材 - Google Patents
ビアリールポリカーボネート中間転写部材 Download PDFInfo
- Publication number
- JP2013033250A JP2013033250A JP2012156550A JP2012156550A JP2013033250A JP 2013033250 A JP2013033250 A JP 2013033250A JP 2012156550 A JP2012156550 A JP 2012156550A JP 2012156550 A JP2012156550 A JP 2012156550A JP 2013033250 A JP2013033250 A JP 2013033250A
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- JP
- Japan
- Prior art keywords
- intermediate transfer
- transfer member
- biaryl
- mol
- biaryl polycarbonate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
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Images
Classifications
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- G—PHYSICS
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- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G15/00—Apparatus for electrographic processes using a charge pattern
- G03G15/14—Apparatus for electrographic processes using a charge pattern for transferring a pattern to a second base
- G03G15/16—Apparatus for electrographic processes using a charge pattern for transferring a pattern to a second base of a toner pattern, e.g. a powder pattern, e.g. magnetic transfer
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- G—PHYSICS
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- G03G15/00—Apparatus for electrographic processes using a charge pattern
- G03G15/14—Apparatus for electrographic processes using a charge pattern for transferring a pattern to a second base
- G03G15/16—Apparatus for electrographic processes using a charge pattern for transferring a pattern to a second base of a toner pattern, e.g. a powder pattern, e.g. magnetic transfer
- G03G15/1665—Apparatus for electrographic processes using a charge pattern for transferring a pattern to a second base of a toner pattern, e.g. a powder pattern, e.g. magnetic transfer by introducing the second base in the nip formed by the recording member and at least one transfer member, e.g. in combination with bias or heat
- G03G15/167—Apparatus for electrographic processes using a charge pattern for transferring a pattern to a second base of a toner pattern, e.g. a powder pattern, e.g. magnetic transfer by introducing the second base in the nip formed by the recording member and at least one transfer member, e.g. in combination with bias or heat at least one of the recording member or the transfer member being rotatable during the transfer
- G03G15/1685—Structure, details of the transfer member, e.g. chemical composition
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- G—PHYSICS
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- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G15/00—Apparatus for electrographic processes using a charge pattern
- G03G15/14—Apparatus for electrographic processes using a charge pattern for transferring a pattern to a second base
- G03G15/16—Apparatus for electrographic processes using a charge pattern for transferring a pattern to a second base of a toner pattern, e.g. a powder pattern, e.g. magnetic transfer
- G03G15/1605—Apparatus for electrographic processes using a charge pattern for transferring a pattern to a second base of a toner pattern, e.g. a powder pattern, e.g. magnetic transfer using at least one intermediate support
- G03G15/162—Apparatus for electrographic processes using a charge pattern for transferring a pattern to a second base of a toner pattern, e.g. a powder pattern, e.g. magnetic transfer using at least one intermediate support details of the the intermediate support, e.g. chemical composition
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
- G03G5/00—Recording members for original recording by exposure, e.g. to light, to heat, to electrons; Manufacture thereof; Selection of materials therefor
- G03G5/02—Charge-receiving layers
- G03G5/04—Photoconductive layers; Charge-generation layers or charge-transporting layers; Additives therefor; Binders therefor
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31507—Of polycarbonate
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/3154—Of fluorinated addition polymer from unsaturated monomers
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/3154—Of fluorinated addition polymer from unsaturated monomers
- Y10T428/31544—Addition polymer is perhalogenated
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31652—Of asbestos
- Y10T428/31663—As siloxane, silicone or silane
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31721—Of polyimide
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- General Physics & Mathematics (AREA)
- Electrostatic Charge, Transfer And Separation In Electrography (AREA)
- Polyesters Or Polycarbonates (AREA)
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- Compositions Of Macromolecular Compounds (AREA)
Abstract
【解決手段】ビアリールポリカーボネート、任意のポリシロキサン、および任意の伝導性フィラー構成成分を含む、中間転写部材。
【選択図】なし
Description
式中、mは約20モル%であり;nは約80モル%であり、数平均分子量は約38,000であり;次の式/構造
式中、mは約20モル%であり、nは約80モル%であり、数平均分子量は、約8,000であり、重量平均分子量は、約20,000であり、South Dakota School of Mines and Technologyから得られ;次の式/構造
中間転写部材はまた、一般に、ポリシロキサンポリマーを含むことができる。本明細書中で開示される中間転写部材のために選択されるポリシロキサンポリマーの例としては、既知の好適なポリシロキサン、例えば、BYK(登録商標)333、BYK(登録商標)330(メトキシプロピルアセタート中約51重量%)およびBYK(登録商標)344(キシレン/イソブタノール比80/20中約52.3重量%で存在する)としてBYK Chemicalから市販されるポリエーテルとポリジメチルシロキサンとのコポリマー;BYK(登録商標)−SILCLEAN3710およびBYK(登録商標)3720(メトキシプロパノール中約25重量%で存在する);BYK(登録商標)310(キシレン中約25重量%で存在する)およびBYK(登録商標)370(キシレン/アルキルベンゼン/シクロヘキサノン/モノフェニルグリコール、比75/11/7/7中約25重量%で存在する)としてBYK Chemicalから市販されるポリエステルとポリジメチルシロキサンとのコポリマー;BYK(登録商標)−SILCLEAN3700(メトキシプロピルアセタート中約25重量%)としてBYK Chemicalから市販されるポリアクリレートとポリジメチルシロキサンとのコポリマー;BYK(登録商標)375(ジ−プロピレングリコールモノメチルエーテル中約25重量%で存在する)としてBYK Chemicalから市販されるポリエステルポリエーテルとポリジメチルシロキサンとのコポリマーなど、並びにこれらの混合物が挙げられる。
場合により、本明細書に開示される中間転写部材は、例えば、中間転写部材の伝導性を変更するおよび調節するために、1種以上のフィラーを含有してもよい。中間転写部材が1層構造である場合、伝導性フィラーは、本明細書中で開示されるビアリールポリカーボネートの混合物中に含まれ得る。しかし、中間転写部材が多層構造である場合、伝導性フィラーは、1つ以上の部材層、例えば支持基材において、その上にコーティングされたビアリールポリカーボネート層またはこれらの混合物において、または支持基材およびビアリールポリカーボネート層の両方において、含まれることができる。
本開示の実施形態において、中間転写部材のビアリールポリカーボネート層は、さらに、任意のポリマーを含むことができ、これは、主にバインダーとして機能する。追加の好適なポリマーの例としては、ポリアミドイミド、ポリイミド、ポリエーテルイミド、ポリカーボネート、ポリフェニレンスルフィド、ポリアミド、ポリスルホン、ポリエーテルイミド、ポリエステル、ポリビニリデンフルオリド、ポリエチレン−co−ポリテトラフルオロエチレンなど、およびこれらの混合物が挙げられる。
所望される場合、支持基材が、中間転写部材中、例えば、ポリマー層の下に含まれ得る。支持基材は、中間転写部材の剛性または強度を増大するために含まれ得る。
所望される場合、任意の離型層が、中間転写部材中に、例えば、ビアリールカーボネート層の上の層の構成に含まれ得る。この離型層は、トナークリーニングを補助するためおよび感光体から中間転写部材への現像画像の転写効率をさらに向上させるために含まれ得る。
本明細書に例示される、ビアリールポリカーボネート、ポリシロキサンおよび任意の伝導性フィラー構成成分を含むビアリールポリカーボネート中間転写部材または混合物は、任意の好適な方法によって、中間転写部材に配合され得る。例えば、既知のミル加工プロセスによって、ビアリールポリカーボネートの均一な分散液または中間転写部材混合物を得ることができ、次いで、既知のドローバーコーティングプロセスまたはフローコーティング方法を用いて、個々の金属基材、例えばステンレス鋼基材などの上にコーティングされる。得られた個々のフィルムは、基材上に残しながら、例えば、約100℃〜約400℃、約160℃〜約320℃、または約125℃〜約190℃で、好適な期間、例えば約20〜約180分間、約40〜約120分間、または約25〜約35分間の加熱によって乾燥され得る。より具体的には、形成されたフィルムは、125℃で30分間、190℃で30分間の加熱によって硬化され得る。
コーティング組成物を、Degussa Chemicalsから入手したspecial carbon black 4、PYRE−M.L.(登録商標)RC−5019としてIndustrial Summit Technologyから入手可能なピロメリト酸二無水物/4,4’−オキシジアニリンのポリアミック酸のポリイミド、およびBYK(登録商標)333としてBYK Chemicalから入手可能なポリエステル改変ポリジメチルシロキサンの混合物を、約13重量の固形分のN−メチル−2−ピロリドン(NMP)中、混合物初期供給量に対して14/85.8/0.2の比で撹拌しながら混合し、ミル加工することによって、調製した。得られた中間転写部材分散液を、0.5ミリメートル厚のステンレス鋼基材上にコーティングし、次いで、この混合物を125℃で30分間、190℃で30分間、および320℃で60分間の加熱によって硬化した。上記の比で上記の構成成分を含む得られた中間転写部材は、ステンレス鋼基材から離型せず、むしろ基材上に付着していた。得られた中間転写部材フィルムは、水中に3ヶ月間浸漬した後、最終的に基材から離型した。
中間転写部材は、Degussa Chemicalsから得られる特定のカーボンブラック4、Mitsubishi Gas Chemical Companyから入手可能なポリカーボネートPCZ−400[ポリ(4,4’−ジヒドロキシ−ジフェニル−1−1−シクロヘキサン)カーボネート、Mw=40,000)]、およびBYK ChemicalからのBYK(登録商標)333として入手可能なポリエステル改質ポリジメチルシロキサンの混合物を、初期混合物の供給物量に基づき、THF/トルエン=70/30混合物中、約15重量部の固体にて、12.8/87/0.2比で撹拌しながら混合し、ミル加工することによって調製した。得られた中間転写部材分散液を、0.5ミリメートル厚のステンレス鋼基材上にコーティングし、次いで、混合物を65℃で20分間、および160℃で40分間の加熱によって乾燥させた。示された比で上記構成成分を含む得られた中間転写部材は、外側プロセスの補助なしで15秒以内でステンレス鋼基材から離型した。
中間転写部材は、PCZ−400を次の式/構造のビアリールポリカーボネートと、12.8/87/0.2カーボンブラック、ビアリールカーボネート/ポリジメチルシロキサンの比で置き換える以外、比較例2のプロセスを繰り返すことによって調製した。
South Dakota School of Mines and Technologyから得られるような次の式/構造のビアリールポリカーボネートが選択される以外、実施例1のプロセスを繰り返すことによって中間転写部材を調製するが、式中、mは約20モル%であり、nが約80モル%であり、数平均分子量はゲル浸透クロマトグラフィ(GPC)分析によって決定される場合に約8,000であり、重量平均分子量はゲル浸透クロマトグラフィ(GPC)分析によって決定される場合に約20,000であり、12.7/87/0.3のカーボンブラック、ビアリールカーボネート/ポリジメチルシロキサンである。
上記の実施例1並びに比較例1および比較例2の中間転写部材を、ヤング率について既知のASTM D882−97プロセスに従って測定した。各中間転写部材のサンプル(0.5インチ×12インチ)を、市販されているInstron Tensile Tester測定機中に置き、次いで、このサンプルを、一定の引張速度で破断するまで伸長した。この間、得られた負荷対サンプル伸長を記録した。このヤング率値を、記録した曲線結果の初期直線部分に対し正接するいずれかの点を取り、対応する歪みで引張応力を除算することによって計算した。引張応力を、負荷を各試験サンプルの平均断面積で除算することによって計算した。結果を、下の表に示す。
Claims (4)
- ビアリールポリカーボネートを含む中間転写部材。
- ビアリールポリカーボネート、ポリシロキサン、および伝導性フィラー構成成分の混合物を含む中間転写部材であって、ここでこの部材は、約2,500〜約5,000メガパスカルのヤング率、および約70〜約150メガパスカルの破断強度を有し、この混合物は金属基材から容易に離型可能である、中間転写部材。
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US13/196,141 US8617712B2 (en) | 2011-08-02 | 2011-08-02 | Biaryl polycarbonate intermediate transfer members |
US13/196,141 | 2011-08-02 |
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JP2013033250A5 JP2013033250A5 (ja) | 2015-09-03 |
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US9052645B2 (en) * | 2013-04-13 | 2015-06-09 | Xerox Corporation | Polyarylatecarbonate intermediate transfer members |
CN107187229A (zh) * | 2017-05-07 | 2017-09-22 | 库尔兹压烫科技(合肥)有限公司 | 一种防冲墨装饰转印箔 |
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KR101799605B1 (ko) | 2017-12-20 |
US8617712B2 (en) | 2013-12-31 |
KR20130019347A (ko) | 2013-02-26 |
CN102911489B (zh) | 2016-01-20 |
JP5860353B2 (ja) | 2016-02-16 |
US20130034733A1 (en) | 2013-02-07 |
US9618881B2 (en) | 2017-04-11 |
EP2555060A1 (en) | 2013-02-06 |
CA2783844C (en) | 2018-10-16 |
EP2555060B1 (en) | 2017-04-26 |
CA2783844A1 (en) | 2013-02-02 |
CN102911489A (zh) | 2013-02-06 |
RU2012133188A (ru) | 2014-02-10 |
US20140079446A1 (en) | 2014-03-20 |
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