JP2012511505A5 - - Google Patents
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- Publication number
- JP2012511505A5 JP2012511505A5 JP2011538921A JP2011538921A JP2012511505A5 JP 2012511505 A5 JP2012511505 A5 JP 2012511505A5 JP 2011538921 A JP2011538921 A JP 2011538921A JP 2011538921 A JP2011538921 A JP 2011538921A JP 2012511505 A5 JP2012511505 A5 JP 2012511505A5
- Authority
- JP
- Japan
- Prior art keywords
- phase
- glycerin
- acrolein
- separation
- acrylic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 claims 72
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims 72
- 235000011187 glycerol Nutrition 0.000 claims 36
- 238000000034 method Methods 0.000 claims 29
- 238000006243 chemical reaction Methods 0.000 claims 15
- 238000001728 nano-filtration Methods 0.000 claims 12
- 238000000926 separation method Methods 0.000 claims 11
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims 9
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims 9
- 229920000642 polymer Polymers 0.000 claims 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 9
- 239000012528 membrane Substances 0.000 claims 7
- 238000004519 manufacturing process Methods 0.000 claims 6
- 238000004821 distillation Methods 0.000 claims 5
- 238000000746 purification Methods 0.000 claims 5
- 238000000909 electrodialysis Methods 0.000 claims 4
- 238000001914 filtration Methods 0.000 claims 4
- 150000003839 salts Chemical class 0.000 claims 4
- 239000004952 Polyamide Substances 0.000 claims 3
- 239000004695 Polyether sulfone Substances 0.000 claims 3
- 239000012530 fluid Substances 0.000 claims 3
- 238000005342 ion exchange Methods 0.000 claims 3
- 229920002647 polyamide Polymers 0.000 claims 3
- 229920006393 polyether sulfone Polymers 0.000 claims 3
- 238000003776 cleavage reaction Methods 0.000 claims 2
- 238000001471 micro-filtration Methods 0.000 claims 2
- 230000003204 osmotic effect Effects 0.000 claims 2
- 230000001590 oxidative effect Effects 0.000 claims 2
- 238000006116 polymerization reaction Methods 0.000 claims 2
- 238000001223 reverse osmosis Methods 0.000 claims 2
- 230000007017 scission Effects 0.000 claims 2
- 125000006850 spacer group Chemical group 0.000 claims 2
- 238000005809 transesterification reaction Methods 0.000 claims 2
- 150000003626 triacylglycerols Chemical class 0.000 claims 2
- 238000000108 ultra-filtration Methods 0.000 claims 2
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims 1
- PMKQSEYPLQIEAY-YWNRKNDBSA-N Phaseolic acid Chemical compound OC(=O)C[C@@H](C(O)=O)OC(=O)\C=C\C1=CC=C(O)C(O)=C1 PMKQSEYPLQIEAY-YWNRKNDBSA-N 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 239000007795 chemical reaction product Substances 0.000 claims 1
- 230000018044 dehydration Effects 0.000 claims 1
- 238000006297 dehydration reaction Methods 0.000 claims 1
- 238000000502 dialysis Methods 0.000 claims 1
- 235000014113 dietary fatty acids Nutrition 0.000 claims 1
- 230000005611 electricity Effects 0.000 claims 1
- 229930195729 fatty acid Natural products 0.000 claims 1
- 239000000194 fatty acid Substances 0.000 claims 1
- 150000004665 fatty acids Chemical class 0.000 claims 1
- 125000005456 glyceride group Chemical group 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 150000002736 metal compounds Chemical class 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 150000002894 organic compounds Chemical class 0.000 claims 1
- 230000003647 oxidation Effects 0.000 claims 1
- 238000007254 oxidation reaction Methods 0.000 claims 1
- 239000012466 permeate Substances 0.000 claims 1
- 230000000379 polymerizing effect Effects 0.000 claims 1
- 238000004064 recycling Methods 0.000 claims 1
- 239000000344 soap Substances 0.000 claims 1
- 230000002194 synthesizing effect Effects 0.000 claims 1
- PMKQSEYPLQIEAY-UHFFFAOYSA-N trans-caffeoyl-L-malic acid Natural products OC(=O)CC(C(O)=O)OC(=O)C=CC1=CC=C(O)C(O)=C1 PMKQSEYPLQIEAY-UHFFFAOYSA-N 0.000 claims 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102008060888.2 | 2008-12-09 | ||
| DE102008060888A DE102008060888A1 (de) | 2008-12-09 | 2008-12-09 | Verfahren zur Herstellung von Acrolein umfassend die Aufarbeitung einer Rohglycerin-Phase |
| PCT/EP2009/064500 WO2010066513A1 (de) | 2008-12-09 | 2009-11-03 | Verfahren zur herstellung von acrolein umfassend die aufarbeitung einer rohglycerin-phase |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2012511505A JP2012511505A (ja) | 2012-05-24 |
| JP2012511505A5 true JP2012511505A5 (enExample) | 2012-12-20 |
Family
ID=41668419
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011538921A Pending JP2012511505A (ja) | 2008-12-09 | 2009-11-03 | 粗製グリセリン相の処理を含むアクロレインの製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US8524945B2 (enExample) |
| EP (1) | EP2356088B1 (enExample) |
| JP (1) | JP2012511505A (enExample) |
| CN (1) | CN102245551A (enExample) |
| BR (1) | BRPI0919647B1 (enExample) |
| DE (1) | DE102008060888A1 (enExample) |
| WO (1) | WO2010066513A1 (enExample) |
| ZA (1) | ZA201102268B (enExample) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102006039203B4 (de) | 2006-08-22 | 2014-06-18 | Evonik Degussa Gmbh | Verfahren zur Herstellung von durch Kristallisation gereinigter Acrylsäure aus Hydroxypropionsäure sowie Vorrichtung dazu |
| FR2953829B1 (fr) | 2009-12-14 | 2011-12-09 | Arkema France | Procede de fabrication d'acroleine et/ou d'acide acrylique a partir de glycerol |
| US10676664B2 (en) * | 2012-03-29 | 2020-06-09 | Axel R. Johnson | Increased availability and reduced costs for viscoelastic surfactants used in hydrofracturing fluids |
| US9725641B2 (en) * | 2012-03-29 | 2017-08-08 | Axel R. Johnson | Methods fluids by producing and employing oil and gas well drilling and completion fluids as well as hydraulic fracturing fluids employing triglyceride processing by products and propylene glycol recovered from aircraft deicing operations |
| DE102013000602A1 (de) | 2013-01-16 | 2014-07-17 | Evonik Industries Ag | Verfahren zur Herstellung von Acrylsäure |
| DE102013217386A1 (de) | 2013-09-02 | 2015-03-05 | Evonik Industries Ag | Verfahren zur Herstellung von Acrylsäure |
| JP6228246B2 (ja) | 2015-03-03 | 2017-11-08 | エボニック デグサ ゲーエムベーハーＥｖｏｎｉｋ Ｄｅｇｕｓｓａ ＧｍｂＨ | エテンのオリゴマー化に使用される不均一系触媒の再生 |
| PL3255029T3 (pl) | 2016-06-10 | 2019-04-30 | Evonik Degussa Gmbh | Oligomeryzacja etenu w warunkach nadkrytycznych |
| EP3266757B1 (de) | 2016-07-08 | 2019-12-25 | Evonik Operations GmbH | Herstellung von zumindest 1-hexen und octen aus ethen |
| US10227279B2 (en) | 2016-09-12 | 2019-03-12 | Evonik Degussa Gmbh | Dehydrogenation of LPG or NGL and flexible utilization of the olefins thus obtained |
| US10882028B2 (en) | 2018-03-14 | 2021-01-05 | Evonik Operations Gmbh | Ni-containing catalyst for the oligomerization of olefins |
| US11253844B2 (en) | 2018-03-14 | 2022-02-22 | Evonik Operations Gmbh | Oligomerization catalyst and process for the production thereof |
| US10850261B2 (en) | 2018-03-14 | 2020-12-01 | Evonik Operations Gmbh | Oligomerization catalyst and process for the production thereof |
| US10882027B2 (en) | 2018-03-14 | 2021-01-05 | Evonik Operations Gmbh | Process for producing an oligomerization catalyst |
| CA3049521C (en) | 2018-07-25 | 2025-05-27 | Evonik Oxeno Gmbh & Co. Kg | PROCESS FOR OLIGOMERIZING BUTENE AND DETERMINING THE PROPORTION OF ACID CATALYSIS |
| US11186782B2 (en) | 2019-01-08 | 2021-11-30 | Evonik Operations Gmbh | Catalyst and process for removing mercaptans from hydrocarbon streams |
| ES2953108T3 (es) | 2019-01-08 | 2023-11-08 | Evonik Operations Gmbh | Procedimiento para eliminar hidrocarburos poliinsaturados de corrientes de hidrocarburos C4 en presencia de mercaptano, disulfuros e hidrocarburos C5 |
| CN110642674B (zh) * | 2019-10-15 | 2022-04-26 | 宁波环洋新材料股份有限公司 | 一种在生物柴油副产粗甘油的精制过程中联产丙烯醛的方法 |
Family Cites Families (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL86631C (enExample) * | 1954-07-13 | |||
| US3919306A (en) * | 1970-05-18 | 1975-11-11 | Atlantic Richfield Co | Purification of recirculated stream for isophthalic acid production |
| CA1329782C (en) * | 1988-08-09 | 1994-05-24 | Thomas Buenemann | Process for purifying crude glycerol |
| US5250182A (en) * | 1992-07-13 | 1993-10-05 | Zenon Environmental Inc. | Membrane-based process for the recovery of lactic acid and glycerol from a "corn thin stillage" stream |
| DE4238493C1 (de) * | 1992-11-14 | 1994-04-21 | Degussa | Verfahren zur Herstellung von Acrolein und dessen Verwendung |
| DE4328407C1 (de) | 1993-08-24 | 1994-09-01 | Sartorius Gmbh | Durch Einwirkung von Hitze sterilisierbarer Wickelmodul |
| DE19636767A1 (de) * | 1996-09-10 | 1998-03-12 | Basf Ag | Verfahren zur Herstellung von aliphatischen alpha, omega-Aminonitrilen |
| SG81982A1 (en) | 1998-05-18 | 2001-07-24 | Nippon Catalytic Chem Ind | Method for production of acrolein and acrylic acid |
| DE19829747A1 (de) | 1998-07-03 | 2000-01-05 | Huels Infracor Gmbh | Entaluminierter Katalysatorträger, Verfahren zur Herstellung des Katalysatorträgers und Verfahren zur Hydratisierung von C2- oder C3-Olefinen mit Wasser in Gegenwart eines Katalysators, der aus diesem mit Säure getränkten Katalysatorträger besteht |
| DE19838425A1 (de) * | 1998-08-24 | 2000-03-02 | Degussa | Verfahren zur Abtrennung mehrfunktioneller Alkohole von wasserlöslichen Salzen aus wäßrigen Systemen |
| JP3712903B2 (ja) * | 2000-01-28 | 2005-11-02 | 花王株式会社 | グリセリンの製造方法 |
| EP1199096A1 (en) | 2000-10-21 | 2002-04-24 | Degussa AG | Catalyst for destruction of CO, VOC, and halogenated organic emissions |
| DE10138150A1 (de) | 2001-08-03 | 2003-02-13 | Basf Ag | Verfahren zur Herstellung wasserabsorbierender Harze |
| DE10142620A1 (de) | 2001-08-31 | 2003-03-20 | Degussa | Ammoximation von Ketonen und Aufarbeitung durch Pervaporation/Dampfpermeation |
| DE10153546A1 (de) | 2001-10-30 | 2003-05-22 | Degussa | Direktsynthese von Wasserstoffperoxid und deren Integration in Oxidationsprozesse |
| ATE391116T1 (de) | 2001-12-14 | 2008-04-15 | Stockhausen Chem Fab Gmbh | Verfahren zur herstellung von acrylsäure |
| US7141683B2 (en) | 2002-05-02 | 2006-11-28 | Degussa Ag | Process for the epoxidation of olefins |
| DE10241762A1 (de) | 2002-09-10 | 2004-03-18 | Oxeno Olefinchemie Gmbh | Verfahren zur Herstellung von wasserfreiem tert.-Butanol |
| US7722847B2 (en) | 2002-09-30 | 2010-05-25 | Evonik Degussa Gmbh | Aqueous hydrogen peroxide solutions and method of making same |
| US6838572B2 (en) | 2002-09-30 | 2005-01-04 | Degussa Ag | Process for the epoxidation of olefins |
| US7169945B2 (en) | 2002-11-26 | 2007-01-30 | Degussa Ag | Process for the epoxidation of olefins |
| US6878836B2 (en) | 2003-06-18 | 2005-04-12 | Degussa Ag | Process for the epoxidation of propene |
| DE10335510A1 (de) | 2003-07-31 | 2005-03-10 | Stockhausen Chem Fab Gmbh | Beschichteter Katalysator-Trägerkörper |
| DE102004030943B4 (de) | 2004-06-26 | 2013-10-02 | Evonik Oxeno Gmbh | Verfahren zur Herstellung von tert.-Butanol aus Isobuten-haltigen Kohlenwasserstoffgemischen |
| JP4903716B2 (ja) | 2005-01-06 | 2012-03-28 | テリック，インコーポレイテッド | トリペプチドおよびテトラペプチドチオエーテル |
| US7501064B2 (en) | 2005-01-06 | 2009-03-10 | Eet | Integrated electro-pressure membrane deionization system |
| FR2882052B1 (fr) * | 2005-02-15 | 2007-03-23 | Arkema Sa | Procede de deshydratation du glycerol en acroleine |
| TWI529181B (zh) | 2005-02-28 | 2016-04-11 | 贏創德固賽有限責任公司 | 以可更新原料為基之吸水聚合物結構及其生產的方法 |
| TWI438187B (zh) * | 2005-02-28 | 2014-05-21 | Evonik Degussa Gmbh | 丙烯酸和基於可再生原料之吸水聚合物結構及二者之製備方法 |
| US20090068440A1 (en) | 2005-06-20 | 2009-03-12 | Gunther Bub | Production of acrolein, acrylic acid and water-absorbent polymer structures made from glycerine |
| DE102005046250B4 (de) | 2005-09-27 | 2020-10-08 | Evonik Operations Gmbh | Anlage zur Abtrennung von organischen Übergangsmetallkomplexkatalysatoren |
| DE102006003618A1 (de) | 2006-01-26 | 2007-08-02 | Oxeno Olefinchemie Gmbh | Verfahren zur Abtrennung von Metall-Komplexkatalysatoren aus Telomerisationsgemischen |
| GB2437516A (en) * | 2006-04-26 | 2007-10-31 | Bai Leng | Method and apparatus for purifying glycerine using filter membranes and a deionisation means |
| DE102006039205A1 (de) * | 2006-08-22 | 2008-03-20 | Stockhausen Gmbh | Auf nachwachsenden Rohstoffen basierende Acrylsäure und wasserabsorbierende Polymergebilde sowie Verfahren zu deren Herstellung mittels Dehydratisierung |
| DE102006054519A1 (de) * | 2006-11-20 | 2008-05-21 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Fettsäurealkylestern und Acrolein aus Triglyceriden |
| DE102007004351A1 (de) * | 2007-01-29 | 2008-07-31 | Evonik Degussa Gmbh | Neue Katalysatoren und Verfahren zur Dehydratisierung von Glycerin |
| DE102007004350A1 (de) | 2007-01-29 | 2008-07-31 | Evonik Degussa Gmbh | Verfahren zur Regenerierung eines Katalysators |
| DE102007019379A1 (de) | 2007-04-23 | 2008-10-30 | Bayer Technology Services Gmbh | Verfahren zur Aufreinigung von Produktgemischen aus Umesterungsreaktionen |
-
2008
- 2008-12-09 DE DE102008060888A patent/DE102008060888A1/de not_active Ceased
-
2009
- 2009-11-03 BR BRPI0919647A patent/BRPI0919647B1/pt not_active IP Right Cessation
- 2009-11-03 EP EP09745047.2A patent/EP2356088B1/de not_active Not-in-force
- 2009-11-03 US US13/128,538 patent/US8524945B2/en not_active Expired - Fee Related
- 2009-11-03 JP JP2011538921A patent/JP2012511505A/ja active Pending
- 2009-11-03 CN CN2009801492265A patent/CN102245551A/zh active Pending
- 2009-11-03 WO PCT/EP2009/064500 patent/WO2010066513A1/de not_active Ceased
-
2011
- 2011-03-28 ZA ZA2011/02268A patent/ZA201102268B/en unknown
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