JP2011506528A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2011506528A5 JP2011506528A5 JP2010538577A JP2010538577A JP2011506528A5 JP 2011506528 A5 JP2011506528 A5 JP 2011506528A5 JP 2010538577 A JP2010538577 A JP 2010538577A JP 2010538577 A JP2010538577 A JP 2010538577A JP 2011506528 A5 JP2011506528 A5 JP 2011506528A5
- Authority
- JP
- Japan
- Prior art keywords
- solvent
- iiia
- reaction product
- mixture
- propanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- BKMMTJMQCTUHRP-VKHMYHEASA-N (S)-2-aminopropan-1-ol Chemical compound C[C@H](N)CO BKMMTJMQCTUHRP-VKHMYHEASA-N 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 239000003960 organic solvent Substances 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000007795 chemical reaction product Substances 0.000 claims 3
- 238000000034 method Methods 0.000 claims 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- 238000009835 boiling Methods 0.000 claims 2
- 239000000706 filtrate Substances 0.000 claims 2
- 239000002904 solvent Substances 0.000 claims 2
- NXMXETCTWNXSFG-BYPYZUCNSA-N (2s)-1-methoxypropan-2-amine Chemical compound COC[C@H](C)N NXMXETCTWNXSFG-BYPYZUCNSA-N 0.000 claims 1
- 239000003125 aqueous solvent Substances 0.000 claims 1
- 238000010533 azeotropic distillation Methods 0.000 claims 1
- 239000003085 diluting agent Substances 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 150000007529 inorganic bases Chemical class 0.000 claims 1
- 239000000047 product Substances 0.000 claims 1
- 238000010992 reflux Methods 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP07150226.4 | 2007-12-20 | ||
| EP07150226 | 2007-12-20 | ||
| PCT/EP2008/067181 WO2009080505A1 (de) | 2007-12-20 | 2008-12-10 | Verfahren zur herstellung von (s)-2-amino-1-propanol (l-alaninol) aus (s)-1-methoxy-2-propylamin |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011506528A JP2011506528A (ja) | 2011-03-03 |
| JP2011506528A5 true JP2011506528A5 (OSRAM) | 2012-02-02 |
| JP5361904B2 JP5361904B2 (ja) | 2013-12-04 |
Family
ID=40344507
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010538577A Expired - Fee Related JP5361904B2 (ja) | 2007-12-20 | 2008-12-10 | （ｓ）−１−メトキシ−２−プロピルアミンからの（ｓ）−２−アミノ−１−プロパノール（ｌ−アラニノール）の製造方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US8344182B2 (OSRAM) |
| EP (1) | EP2234962B1 (OSRAM) |
| JP (1) | JP5361904B2 (OSRAM) |
| KR (1) | KR20100098447A (OSRAM) |
| CN (1) | CN101903331A (OSRAM) |
| CA (1) | CA2706463A1 (OSRAM) |
| WO (1) | WO2009080505A1 (OSRAM) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2478098B1 (en) | 2009-09-15 | 2017-03-15 | Basf Se | Preparation of beta-amino acids |
| CN102229536B (zh) * | 2011-04-25 | 2013-11-13 | 上虞市众昌化工有限公司 | 一种膜法电渗析分离氨基烷基醇的方法 |
| CN106680392A (zh) * | 2016-12-27 | 2017-05-17 | 中蓝连海设计研究院 | 一种采用气相色谱法测定三正辛胺纯度的方法 |
| CN116874381A (zh) * | 2023-06-19 | 2023-10-13 | 万华化学集团股份有限公司 | 一种3-氨基丙醇的制备方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06199747A (ja) | 1992-12-28 | 1994-07-19 | Sumika Fine Kemu Kk | Ｌ−アラニノールの製造方法 |
| AU9434798A (en) | 1997-08-08 | 1999-03-01 | Lonza A.G. | Process for the production of l-alaminol and gamma-glutamyl isopropylamide and amicroorganism strain fo the genus psendomonas |
| WO2001073038A2 (de) | 2000-03-31 | 2001-10-04 | Lonza Ag | Verfahren zur biotechnologischen herstellung von l-alaninol |
| DE102004007499A1 (de) | 2004-02-13 | 2005-09-01 | Basf Ag | Verfahren zur Herstellung optisch aktiver Alkohole oder Carbonsäuren |
| CN101033193A (zh) * | 2007-04-11 | 2007-09-12 | 浙江大学 | 一种2－氨基丙醇的合成方法 |
-
2008
- 2008-12-10 KR KR1020107016006A patent/KR20100098447A/ko not_active Withdrawn
- 2008-12-10 CA CA2706463A patent/CA2706463A1/en not_active Abandoned
- 2008-12-10 US US12/745,836 patent/US8344182B2/en not_active Expired - Fee Related
- 2008-12-10 EP EP08864439.8A patent/EP2234962B1/de not_active Not-in-force
- 2008-12-10 JP JP2010538577A patent/JP5361904B2/ja not_active Expired - Fee Related
- 2008-12-10 CN CN2008801223226A patent/CN101903331A/zh active Pending
- 2008-12-10 WO PCT/EP2008/067181 patent/WO2009080505A1/de not_active Ceased
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP6216073B2 (ja) | １ｈ−［１，２，３］トリアゾール及びその中間体１−ベンジル−１ｈ−［１，２，３］トリアゾールの大規模な製造方法 | |
| CN107986944B (zh) | 一种以2,2-二氟-1-氯乙烷为原料合成二氟乙醇的方法 | |
| CN104470880A (zh) | 通过薄膜蒸馏制备高纯度无水糖醇的方法 | |
| JP2014507414A5 (OSRAM) | ||
| JP2013508368A5 (OSRAM) | ||
| JP2011506528A5 (OSRAM) | ||
| WO2013097629A1 (zh) | 一种盐酸阿莫罗芬的制备方法 | |
| CN102924386A (zh) | 一种4-溴哒嗪的工业化制备方法 | |
| CN102311394B (zh) | 一种5-乙基-5-苯基巴比妥酸的制备方法 | |
| CN104292122A (zh) | 在n-乙酰乙酰苯胺的生产中减少副产物3-(苯基氨基)-2-丁烯酸乙酯生成的方法 | |
| CN104262397B (zh) | 一种高纯度替诺福韦的制备方法 | |
| JP2010510253A5 (OSRAM) | ||
| CN103664805B (zh) | 一种制备阿昔莫司的方法 | |
| JP2001278858A (ja) | Ｎ−メチル−２−ピロリドンの製造方法 | |
| CN102260156A (zh) | 一种医药中间体对甲氧基苯丙酮的制备方法 | |
| CN101863791B (zh) | 对二甲氨基苯甲酸异辛酯(eha)的合成方法 | |
| TW201718510A (zh) | 製備1-甲基-3-(三氟甲基)-1h-吡唑-5-醇的方法 | |
| JP2006028066A5 (OSRAM) | ||
| US20120253051A1 (en) | Process for the preparation of ropinirole and salts thereof | |
| KR100881890B1 (ko) | 사포그렐레이트 염산염의 제조방법 | |
| WO2013149364A1 (zh) | 一种1-羟甲基环丙基乙腈合成方法 | |
| CN107162920A (zh) | 一种r-1-氨基-2-丙醇的制备方法 | |
| CN116063178A (zh) | 一种三氟乙酰乙酸乙酯的合成方法 | |
| CN100494162C (zh) | 一种非等比例顺式舍曲林盐酸盐混合物的分离方法 | |
| CN106632347B (zh) | 一种吡咯并吡嗪化合物及其盐的制备方法 |