JP2011006763A - さび止め油組成物 - Google Patents
さび止め油組成物 Download PDFInfo
- Publication number
- JP2011006763A JP2011006763A JP2009153902A JP2009153902A JP2011006763A JP 2011006763 A JP2011006763 A JP 2011006763A JP 2009153902 A JP2009153902 A JP 2009153902A JP 2009153902 A JP2009153902 A JP 2009153902A JP 2011006763 A JP2011006763 A JP 2011006763A
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- JP
- Japan
- Prior art keywords
- rust
- acid
- oil composition
- mass
- rust preventive
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000000203 mixture Substances 0.000 title claims abstract description 90
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims abstract description 140
- -1 fatty acid amine salt Chemical class 0.000 claims abstract description 90
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims abstract description 41
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 36
- 239000000194 fatty acid Substances 0.000 claims abstract description 36
- 229930195729 fatty acid Natural products 0.000 claims abstract description 36
- 150000002148 esters Chemical class 0.000 claims abstract description 33
- 239000001993 wax Substances 0.000 claims abstract description 30
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- 239000003921 oil Substances 0.000 claims description 85
- 125000004432 carbon atom Chemical group C* 0.000 claims description 64
- 230000003449 preventive effect Effects 0.000 claims description 50
- 125000000217 alkyl group Chemical group 0.000 claims description 48
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- FSYKKLYZXJSNPZ-UHFFFAOYSA-N sarcosine Chemical class C[NH2+]CC([O-])=O FSYKKLYZXJSNPZ-UHFFFAOYSA-N 0.000 claims description 19
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- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 11
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- 125000001183 hydrocarbyl group Chemical group 0.000 claims 1
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- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 8
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- 229920000768 polyamine Polymers 0.000 description 8
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- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 7
- 239000012298 atmosphere Substances 0.000 description 7
- 229910052788 barium Inorganic materials 0.000 description 7
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 7
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- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 6
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 6
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- 239000005642 Oleic acid Substances 0.000 description 6
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 6
- 239000000460 chlorine Substances 0.000 description 6
- 229910052801 chlorine Inorganic materials 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 239000003925 fat Substances 0.000 description 6
- 235000019197 fats Nutrition 0.000 description 6
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 6
- 229910052740 iodine Inorganic materials 0.000 description 6
- 239000011630 iodine Substances 0.000 description 6
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 6
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 6
- 235000021313 oleic acid Nutrition 0.000 description 6
- 229920006395 saturated elastomer Polymers 0.000 description 6
- 238000005406 washing Methods 0.000 description 6
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 5
- 229910052799 carbon Inorganic materials 0.000 description 5
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 5
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- 238000010998 test method Methods 0.000 description 5
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 4
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 4
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- 159000000007 calcium salts Chemical class 0.000 description 4
- 239000011248 coating agent Substances 0.000 description 4
- PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical compound NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 description 4
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 4
- 238000005238 degreasing Methods 0.000 description 4
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 4
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 4
- 239000003208 petroleum Substances 0.000 description 4
- 239000011591 potassium Substances 0.000 description 4
- 229910052700 potassium Inorganic materials 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 3
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- 108010077895 Sarcosine Proteins 0.000 description 3
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- 239000003963 antioxidant agent Substances 0.000 description 3
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Classifications
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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- C10M133/16—Amides; Imides
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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- C23F11/10—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent in other liquids using organic inhibitors
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- C23F11/14—Nitrogen-containing compounds
- C23F11/144—Aminocarboxylic acids
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- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
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- C23F11/16—Sulfur-containing compounds
- C23F11/163—Sulfonic acids
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- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
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- C23F11/00—Inhibiting corrosion of metallic material by applying inhibitors to the surface in danger of corrosion or adding them to the corrosive agent
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- C23F11/173—Macromolecular compounds
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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- C10M2205/0285—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers containing aliphatic monomers having more than four carbon atoms used as base material
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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Abstract
【解決手段】組成物全量基準で0.1〜10質量%の、親水親油指数が10〜12であるノニオン系界面活性剤と、ザルコシン型化合物、スルホン酸塩、エステル、アミン、カルボン酸、脂肪酸アミン塩、カルボン酸塩、パラフィンワックス、酸化ワックス塩、アルキル又はアルケニルコハク酸誘導体及びホウ素化合物から選ばれる少なくとも1種のさび止め添加剤と、を含有し、40℃における動粘度が1〜50mm2/sであることを特徴とするさび止め油組成物。
【選択図】なし
Description
親水親油指数=(親水基部分の分子量÷界面活性剤全体の分子量)×100÷5
Ra−N−〔(C2H4O)b−H〕c (1)
[式中、Rは炭素数1〜24の炭化水素基を表し、a及びcはそれぞれ1又は2であって、a+c=3を満たし、bは1〜7の整数を表す。]
Ra−N−〔(C2H4O)b−H〕c (1)
[式中、Rは炭素数1〜24の炭化水素基を表し、a及びcはそれぞれ1又は2であって、a+c=3を満たし、bは1〜7の整数を表す。]
R1−CO−NR2−(CH2)n−COOX (2)
[R1−CO−NR2−(CH2)n−COO]mY (3)
[R1−CO−NR2−(CH2)n−COO]m−Z−(OH)m’ (4)
(式中、R1は炭素数6〜30のアルキル基又は炭素数6〜30のアルケニル基;R2は炭素数1〜4のアルキル基;Xは水素原子、炭素数1〜30のアルキル基、又は炭素数1〜30のアルケニル基;Yはアルカリ金属又はアルカリ土類金属;Zは2価以上の多価アルコールの水酸基を除いた残基;mは1以上の整数で、Yがアルカリ金属の場合は1、アルカリ土類金属の場合は2;m’は0以上の整数;nは1〜4の整数;m+m’はZの価数、を示す。)
炭素数1〜13のアルケニル基を有するモノアルケニルアミン、炭素数2〜8のアルケニル基を2個有するジアルケニルアミン、炭素数2〜5のアルケニル基を3個有するトリアルケニルアミン;
メチル基2個と炭素数2〜13のアルケニル基1個を有するジメチルモノアルケニルアミン;
芳香族置換アルキルアミン、炭素数5〜16のシクロアルキルアミン、アルキル基およびシクロアルキル基を有するモノアミン、アルキルシクロアルキルアミンが挙げられ、これらモノアミンの全ての置換異性体も挙げられる。ここでいうモノアミンには、油脂から誘導される牛脂アミン等のモノアミンも含まれる。
炭素数1〜23のアルキル基を有するN−アルキルエチレンジアミン;
炭素数2〜23のアルケニル基を有するN−アルケニルエチレンジアミン;
N−アルキルまたはN−アルケニルアルキレンポリアミン及び、これらポリアミンの全ての置換異性体が挙げられる。また、ここでいうポリアミンには油脂から誘導されるポリアミン(牛脂ポリアミン等)も含まれる。
炭素数1〜16のアルコールのモノアルカノールモノアミン、
炭素数1〜7のアルコールのジアルカノールモノアミン、
炭素数1〜5のアルコールを3個有するトリアルカノールモノアミン、
炭素数2〜4のアルキル基1個と炭素数2〜5のアルコール2個を有するモノアルキルジアルカノールモノアミン、
炭素数2〜4のアルキル基2個と炭素数2〜5のアルコール1個を有するジアルキルモノアルカノールモノアミン、
シクロヘキシルと炭素数2または3のアルコールを1個有するモノシクロヘキシルモノアルカノールモノアミン、
シクロヘキシルと炭素数2または3のアルコールを2個有するモノシクロヘキシルジアルカノールモノアミン、
が挙げられ、これらアルカノールアミンの全ての置換異性体も挙げられる。
またはこれらの混合物が挙げられ、これら脂肪酸の全ての置換異性体も挙げられる。
また、基油に対する溶解性の観点からは不飽和カルボン酸が好ましく、例えばオレイン酸が挙げられる。また、耐ステイン性の観点からは飽和脂肪酸が好ましく、例えばイソステアリン酸が挙げられる。
ヒドロキシ脂肪酸としては、好ましくは炭素数6〜24のヒドロキシ脂肪酸が用いられる。また、ヒドロキシ脂肪酸が有するヒドロキシ基の個数は1個でも複数個でもよいが、1〜3個のヒドロキシ基を有するものが好ましく用いられる。このようなヒドロキシ脂肪酸としては、例えば、リシノール酸が挙げられる。
表1〜4の実施例1〜20に示す組成を有する各種の本発明に係るさび止め油組成物、及び表5〜6に示す比較例1〜9に示すさび止め油組成物をそれぞれ調製した。各組成物の調製に用いた成分は、以下のとおりである。
A1:ラウリルアミンのエチレンオキサイド付加物(EO付加モル数:3、親水親油指数:9.3)
A2:ステアリルアミンのエチレンオキサイド付加物(EO付加モル数:6、親水親油指数:10.5)
A3:モノシクロヘキシルアミンのエチレンオキサイド付加物(EO付加モル数:2、親水親油指数:11.1)
A4:ラウリルアミンのエチレンオキサイド付加物(EO付加モル数:5、親水親油指数:11.7)
A5:モノシクロヘキシルアミンのエチレンオキサイド付加物(EO付加モル数:4、親水親油指数:13.9)
A6:アラキン酸とソルビタンのエステル(親水親油指数:8.2)
A7:ラウリル酸とソルビタンのエステル(親水親油指数:10.9)
A8:カプリン酸とソルビタンのエステル(親水親油指数:11.9)
A9:カプロン酸とソルビタンのエステル(親水親油指数:14.5)
(B)成分
B1:オレオイルザルコシン(N−Methyloleamidoacetic acid)
B2−1:エチレンジアミンスルホネート
B2−2:Naジノニルナフタレンスルホネート
B2−3:中性Caスルホネート
B2−4:中性Baスルホネート
B3−1:ソルビタンモノイソステアレート
B3−2:コハク酸エステル(炭素数12のアルケニル基を有するアルケニルコハク酸とプロピレングリコールとのハーフエステル)
B4:ジシクロヘキシルアミン
B5: オレイン酸のダイマー酸
B6:オクタン酸とオクチルアミンの塩
B7:ラノリン脂肪酸のカルシウム塩
B8:融点46℃のパラフィンワックス
B9:酸化ワックスのカルシウム塩
(C)その他の添加剤
C1:酸化防止剤としてジ−t−ブチル−p−クレゾール
C2:金属不活性化剤としてのベンゾトリアゾール
(D)成分
D1:水(蒸留水)
(E)成分
E1:40℃における動粘度が0.75mm2/sの鉱油
E2:40℃における動粘度が22mm2/sの鉱油
E3:40℃における動粘度が480mm2/s鉱油
E4:合成油(ポリα―オレフィン:40℃における動粘度が21mm2/s)
<動粘度>
JIS K 2283に準拠して測定した。
<さび止め性試験−1(湿潤試験)>
JIS K 2246−2007「さび止め油」、6.34「湿潤試験方法」に準拠して評価した。さび発生度がA級(さび発生度が0%)を維持するまでの時間(h)を測定して評価した。
<さび止め性試験−2(中性塩水噴霧試験)>
JIS K2246−2007「さび止め油」、6.35「中性塩水噴霧試験」に準拠して評価した。さびが発生するまでの時間(h)を測定して評価し、評価は1時間ごとに行った。
<さび止め性試験−3(さび止め性試験)>
下記のステップで試験を実施した。
(1)清浄にした試験片(湿潤試験方法と同じもの)について、JIS K 2246−2007の6.31「指紋除去性試験」を準拠し、人工指紋液をプリントする。
(2)指紋をプリントした試験片を試料油中に浸漬塗布し、24h油切りする。
(3)湿潤試験と同じ要領で試験片を吊った状態とし、50℃、相対湿度95%に調整した高湿恒温槽内で2週間保持する。
上記の工程を終了後、さび発生の有無を評価した。さびが発生した場合を「有」、さびが発生しない場合を「無」とした。
<分離安定性>
さび止め油組成物を調製後、25℃に調整した恒温槽中に24h保持し、水の分離の有無を評価した。水が分離しない場合を、「無」、水が分離した場合を「有」とした。
<吸湿試験>
200mlのガラス容器に試料油を10g入れ、30℃,80%RHに調整した恒温槽に16h放置したときの水分量を測定した。
水分の測定方法:JIS K2275 カールフィッシャー式(水分気化装置を用いる)
上記試験の結果を表1〜6に示す。
Claims (7)
- 潤滑油基油と、
組成物全量基準で0.1〜10質量%の、親水親油指数が10〜12であるノニオン系界面活性剤と、
ザルコシン型化合物、スルホン酸塩、エステル、アミン、カルボン酸、脂肪酸アミン塩、カルボン酸塩、パラフィンワックス、酸化ワックス塩、アルキル又はアルケニルコハク酸誘導体及びホウ素化合物から選ばれる少なくとも1種のさび止め添加剤と、
を含有し、
40℃における動粘度が1〜50mm2/sであることを特徴とするさび止め油組成物。 - 前記さび止め添加剤のうちザルコシン型化合物を必須成分として含有することを特徴とする、請求項1に記載のさび止め油組成物。
- 前記潤滑油基油が、40℃における動粘度0.7〜40mm2/sの鉱油及び/又は合成油と、40℃における動粘度150〜700mm2/sの鉱油及び/又は合成油とからなることを特徴とする、請求項1又は2に記載のさび止め油組成物。
- 前記ノニオン系界面活性剤が、エチレングリコール型非イオン界面活性剤、ポリエチレングリコール型非イオン界面活性剤及び多価アルコール型非イオン界面活性剤から選ばれる少なくとも1種であることを特徴とする、請求項1〜3のいずれか1項に記載のさび止め油組成物。
- 前記ノニオン系界面活性剤が、ソルビタンの脂肪酸エステル又は下記一般式(1)で表されるオキシエチレンアルキルアミン及びポリオキシエチレンアルキルアミンから選ばれる少なくとも1種であることを特徴とする、請求項1〜4のいずれか1項に記載のさび止め油組成物。
Ra−N−〔(C2H4O)b−H〕c (1)
〔式中、Rは炭素数1〜24の炭化水素基を表し、a及びcはそれぞれ1又は2であって、a+c=3を満たし、bは1〜7の整数を表す。〕 - 前記さび止め添加剤としてスルホン酸塩を含有し、該スルホン酸塩がアミンスルホネート、ナトリウムスルホネート及びカルシウムスルホネートから選ばれる少なくとも1種であることを特徴とする、請求項1〜5のいずれか1項に記載のさび止め油組成物。
- 組成物全量基準で0.1〜10質量%の水を含有することを特徴とする、請求項1〜6のいずれか1項に記載のさび止め油組成物。
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