JP2010509444A5 - - Google Patents
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- JP2010509444A5 JP2010509444A5 JP2009536316A JP2009536316A JP2010509444A5 JP 2010509444 A5 JP2010509444 A5 JP 2010509444A5 JP 2009536316 A JP2009536316 A JP 2009536316A JP 2009536316 A JP2009536316 A JP 2009536316A JP 2010509444 A5 JP2010509444 A5 JP 2010509444A5
- Authority
- JP
- Japan
- Prior art keywords
- salt
- acid
- polymerization medium
- weight
- fluoropolymer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000000034 method Methods 0.000 claims description 32
- 239000002253 acid Substances 0.000 claims description 16
- 238000006116 polymerization reaction Methods 0.000 claims description 16
- 150000003839 salts Chemical class 0.000 claims description 15
- 229920002313 fluoropolymer Polymers 0.000 claims description 12
- 239000004811 fluoropolymer Substances 0.000 claims description 12
- 230000000379 polymerizing effect Effects 0.000 claims description 8
- 239000004215 Carbon black (E152) Substances 0.000 claims description 7
- 229930195733 hydrocarbon Natural products 0.000 claims description 7
- 150000002430 hydrocarbons Chemical class 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 7
- 239000004094 surface-active agent Substances 0.000 claims description 7
- 239000000178 monomer Substances 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 239000006185 dispersion Substances 0.000 claims description 5
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 3
- 125000001153 fluoro group Chemical group F* 0.000 claims description 2
- 239000003999 initiator Substances 0.000 claims description 2
- 229920000642 polymer Polymers 0.000 claims description 2
- 239000002609 medium Substances 0.000 description 11
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- BQCIDUSAKPWEOX-UHFFFAOYSA-N 1,1-Difluoroethene Chemical compound FC(F)=C BQCIDUSAKPWEOX-UHFFFAOYSA-N 0.000 description 2
- YSYRISKCBOPJRG-UHFFFAOYSA-N 4,5-difluoro-2,2-bis(trifluoromethyl)-1,3-dioxole Chemical compound FC1=C(F)OC(C(F)(F)F)(C(F)(F)F)O1 YSYRISKCBOPJRG-UHFFFAOYSA-N 0.000 description 2
- UUAGAQFQZIEFAH-UHFFFAOYSA-N chlorotrifluoroethylene Chemical group FC(F)=C(F)Cl UUAGAQFQZIEFAH-UHFFFAOYSA-N 0.000 description 2
- 229920001577 copolymer Polymers 0.000 description 2
- HCDGVLDPFQMKDK-UHFFFAOYSA-N hexafluoropropylene Chemical group FC(F)=C(F)C(F)(F)F HCDGVLDPFQMKDK-UHFFFAOYSA-N 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 239000010702 perfluoropolyether Substances 0.000 description 2
- MIZLGWKEZAPEFJ-UHFFFAOYSA-N 1,1,2-trifluoroethene Chemical group FC=C(F)F MIZLGWKEZAPEFJ-UHFFFAOYSA-N 0.000 description 1
- JMGNVALALWCTLC-UHFFFAOYSA-N 1-fluoro-2-(2-fluoroethenoxy)ethene Chemical compound FC=COC=CF JMGNVALALWCTLC-UHFFFAOYSA-N 0.000 description 1
- RFJVDJWCXSPUBY-UHFFFAOYSA-N 2-(difluoromethylidene)-4,4,5-trifluoro-5-(trifluoromethyl)-1,3-dioxolane Chemical compound FC(F)=C1OC(F)(F)C(F)(C(F)(F)F)O1 RFJVDJWCXSPUBY-UHFFFAOYSA-N 0.000 description 1
- QMIWYOZFFSLIAK-UHFFFAOYSA-N 3,3,3-trifluoro-2-(trifluoromethyl)prop-1-ene Chemical group FC(F)(F)C(=C)C(F)(F)F QMIWYOZFFSLIAK-UHFFFAOYSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- XUCNUKMRBVNAPB-UHFFFAOYSA-N fluoroethene Chemical compound FC=C XUCNUKMRBVNAPB-UHFFFAOYSA-N 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000012985 polymerization agent Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US85800806P | 2006-11-09 | 2006-11-09 | |
| US60/858,008 | 2006-11-09 | ||
| PCT/US2007/023642 WO2008060463A1 (en) | 2006-11-09 | 2007-11-09 | Aqueous polymerization of fluorinated monomers using polymerization agent comprising fluoropolyether acid or salt and hydrocarbon surfactant |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010509444A JP2010509444A (ja) | 2010-03-25 |
| JP2010509444A5 true JP2010509444A5 (OSRAM) | 2010-12-24 |
| JP5439186B2 JP5439186B2 (ja) | 2014-03-12 |
Family
ID=39110524
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009536316A Active JP5439186B2 (ja) | 2006-11-09 | 2007-11-09 | フルオロポリエーテル酸または塩および炭化水素系界面活性剤を含む重合剤を用いるフッ素化モノマーの水性重合 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US7897682B2 (OSRAM) |
| EP (1) | EP2084195B1 (OSRAM) |
| JP (1) | JP5439186B2 (OSRAM) |
| CN (1) | CN101605826B (OSRAM) |
| AT (1) | ATE512165T1 (OSRAM) |
| WO (1) | WO2008060463A1 (OSRAM) |
Families Citing this family (51)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8080621B2 (en) * | 2005-06-10 | 2011-12-20 | Arkema Inc. | Aqueous process for making fluoropolymers |
| ATE509960T1 (de) * | 2006-11-09 | 2011-06-15 | Du Pont | Wässrige polymerisation eines fluorinierten monomers mithilfe eines polymerisationsmittels mit einer fluorpolyethersäure oder einem salz daraus und einem fluorpolyethersäuretensid oder - salztensid von hohem molekulargewicht |
| US20090281241A1 (en) * | 2008-05-09 | 2009-11-12 | E. I. Du Pont De Nemours And Company | Aqueous Polymerization of Fluorinated Monomer Using a Mixture of Fluoropolyether Acids or Salts |
| US20100113691A1 (en) * | 2008-11-06 | 2010-05-06 | E. I. Du Pont De Nemours And Company | Fluoro olefin polymerization |
| US8153738B2 (en) | 2008-12-23 | 2012-04-10 | E I Du Pont De Nemours And Company | Fluoropolymer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer |
| US8436053B2 (en) * | 2008-12-23 | 2013-05-07 | E.I. Du Pont De Nemours And Company | Fluorinated ionomer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer |
| US8058376B2 (en) | 2008-12-23 | 2011-11-15 | E. I. Du Pont De Nemours And Company | Fluoropolymer produced by aqueous polymerization using dispersed particulate of fluorinated lonomer produced in situ |
| US8436054B2 (en) * | 2008-12-23 | 2013-05-07 | E I Du Pont De Nemours And Company | Fluorinated ionomer produced by aqueous polymerization using dispersed particulate of fluorinated ionomer produced in situ |
| US8835547B2 (en) * | 2008-12-23 | 2014-09-16 | E I Du Pont De Nemours And Company | Fluoropolymer particles having a nucleus of fluorinated ionomer |
| JP5746168B2 (ja) * | 2009-07-31 | 2015-07-08 | スリーエム イノベイティブ プロパティズ カンパニー | ポリオール化合物を含有するフルオロポリマー組成物及びその製造方法 |
| JP5684283B2 (ja) * | 2009-12-18 | 2015-03-11 | ソルヴェイ・スペシャルティ・ポリマーズ・イタリー・エッセ・ピ・ア | フルオロポリマーの製造方法 |
| WO2011073254A1 (en) * | 2009-12-18 | 2011-06-23 | Solvay Solexis S.P.A. | Process for manufacturing a dispersion of a vinylidene fluoride polymer |
| EP2638083B1 (en) | 2010-11-09 | 2019-04-10 | The Chemours Company FC, LLC | Reducing the telogenic behavior of hydrocarbon-containing surfactants in aqueous dispersion fluoromonomer polymerization |
| JP6109073B2 (ja) | 2010-11-09 | 2017-04-05 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーＥ．Ｉ．Ｄｕ Ｐｏｎｔ Ｄｅ Ｎｅｍｏｕｒｓ Ａｎｄ Ｃｏｍｐａｎｙ | 炭化水素界面活性剤を用いたフルオロモノマーの水性重合 |
| WO2012064846A1 (en) * | 2010-11-09 | 2012-05-18 | E. I. Du Pont De Nemours And Company | Nucleation in aqueous polymerization of fluoromonomer |
| JP5730093B2 (ja) * | 2011-03-28 | 2015-06-03 | 株式会社クレハ | フッ化ビニリデン系重合体の製造方法 |
| CN102585070B (zh) * | 2012-01-06 | 2015-12-09 | 石家庄市海森化工有限公司 | 三氟氯乙烯-乙烯共聚物的制备方法 |
| CN102627719B (zh) * | 2012-03-23 | 2014-05-07 | 上海三爱富新材料股份有限公司 | 一种高强度耐蠕变性的聚四氟乙烯制备方法 |
| EP3074430B1 (en) | 2013-11-26 | 2019-02-20 | The Chemours Company FC, LLC | Employing polyalkylene oxides for nucleation in aqueous polymerization of fluoromonomer |
| US10407588B2 (en) | 2015-03-13 | 2019-09-10 | Daikin Industries, Ltd. | Coating composition and coated article |
| CN108017746B (zh) * | 2016-10-28 | 2020-03-20 | 中昊晨光化工研究院有限公司 | 一种低压缩永久变形的过氧化物硫化氟橡胶及其制备方法 |
| JP6750729B2 (ja) | 2017-03-31 | 2020-09-02 | ダイキン工業株式会社 | フルオロポリマーの製造方法、重合用界面活性剤及び界面活性剤の使用 |
| CN117304372A (zh) | 2017-03-31 | 2023-12-29 | 大金工业株式会社 | 含氟聚合物的组合物和成型体 |
| EP3666802A4 (en) | 2017-08-10 | 2021-05-26 | Daikin Industries, Ltd. | PROCESS FOR THE PRODUCTION OF A LIQUID CONSISTING OF AN AQUEOUS DISPERSION OF PURIFIED POLYTETRAFLUORETHYLENE, PROCESS FOR THE PRODUCTION OF A MODIFIED POLYTETRAFLUORETHYLENE POWDER, PROCESS FOR THE PRODUCTION OF A MOLDED OBJECT IN POLYTETRAFLUORETHYLENE, ETHYLORETHYLENE COMPOSITION |
| US11401352B2 (en) * | 2017-09-08 | 2022-08-02 | Solvay Specialty Polymers Italy S.P.A. | Method for making fluoropolymers |
| WO2019065638A1 (ja) * | 2017-09-28 | 2019-04-04 | Ａｇｃ株式会社 | 変性ポリテトラフルオロエチレンの製造方法、変性ポリテトラフルオロエチレン粉末の製造方法、延伸多孔体の製造方法 |
| EP3750924A4 (en) | 2018-02-08 | 2021-10-27 | Daikin Industries, Ltd. | PROCESS FOR THE MANUFACTURE OF A FLUORINATED POLYMER, SURFACTANT FOR ITS POLYMERIZATION, USE OF THE SURFACTANT AND COMPOSITION |
| WO2019168183A1 (ja) | 2018-03-01 | 2019-09-06 | ダイキン工業株式会社 | フルオロポリマーの製造方法 |
| EP3763747B1 (en) * | 2018-03-07 | 2025-10-29 | Daikin Industries, Ltd. | Method for producing fluoropolymer |
| CN112154162B (zh) * | 2018-05-18 | 2022-07-26 | Ａｇｃ株式会社 | 含氟聚合物的制造方法及含氟离子交换聚合物的制造方法 |
| EP3862368A4 (en) * | 2018-10-03 | 2022-06-29 | Daikin Industries, Ltd. | Polytetrafluoroethylene production method |
| EP3960773B1 (en) | 2019-04-26 | 2025-07-16 | Daikin Industries, Ltd. | Method for producing aqueous fluoropolymer dispersion, drainage treatment method, and aqueous fluoropolymer dispersion |
| US20220251251A1 (en) | 2019-04-26 | 2022-08-11 | Daikin Industries, Ltd. | Fluoropolymer aqueous dispersion production method and fluoropolymer aqueous dispersion |
| WO2021015291A1 (ja) * | 2019-07-23 | 2021-01-28 | ダイキン工業株式会社 | フルオロポリマーの製造方法、ポリテトラフルオロエチレン組成物及びポリテトラフルオロエチレン粉末 |
| EP4041782A4 (en) * | 2019-10-11 | 2023-11-01 | Gujarat Fluorochemicals Limited | METHOD FOR PRODUCING FLUROPOLYMERS AND FLUOROELASTOMERS IN THE PRESENCE OF A NON-FLUORINATED SULFONATE TYPE CONTAINING SURFACTANT |
| CN114651019B (zh) | 2019-11-19 | 2024-11-08 | 大金工业株式会社 | 含氟聚合物的制造方法 |
| EP4063404A4 (en) | 2019-11-19 | 2023-12-06 | Daikin Industries, Ltd. | Method for producing fluoropolymer, method for producing polytetrafluoroethylene, method for producing perfluoroelastomer, and composition |
| JP6989792B2 (ja) | 2019-12-25 | 2022-01-12 | ダイキン工業株式会社 | フルオロポリマーの製造方法 |
| US12460020B2 (en) * | 2020-05-14 | 2025-11-04 | Gujarat Fluorochemicals Limited | Process for polymerizing fluoromonomers using a combination of fluorinated and nonfluorinated surfactant |
| WO2022072693A1 (en) | 2020-10-01 | 2022-04-07 | The Chemours Company Fc, Llc | Low reactivity hydrocarbon dispersing agents in the aqueous polymerization of fluoropolymers |
| WO2022107894A1 (ja) | 2020-11-19 | 2022-05-27 | ダイキン工業株式会社 | ポリテトラフルオロエチレンの製造方法およびポリテトラフルオロエチレンを含有する組成物 |
| EP4342921A4 (en) | 2021-05-19 | 2025-04-23 | Daikin Industries, Ltd. | Process for producing a fluoropolymer, process for producing polytetrafluoroethylene and composition |
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| JP7747987B2 (ja) | 2021-06-30 | 2025-10-02 | ダイキン工業株式会社 | フルオロポリマー組成物の製造方法およびフルオロポリマー組成物 |
| EP4497762A1 (en) | 2022-03-23 | 2025-01-29 | Daikin Industries, Ltd. | Method for producing fluoropolymer, and composition |
| WO2023210820A1 (ja) | 2022-04-28 | 2023-11-02 | ダイキン工業株式会社 | フッ素樹脂を含有する組成物の製造方法およびフッ素樹脂を含有する組成物 |
| WO2023210819A1 (ja) | 2022-04-28 | 2023-11-02 | ダイキン工業株式会社 | フルオロポリマーの製造方法 |
| WO2024154773A1 (ja) | 2023-01-18 | 2024-07-25 | ダイキン工業株式会社 | テトラフルオロエチレン系ポリマー組成物、電気化学デバイス用バインダー、電極合剤、電極、及び、二次電池 |
| JP7492186B1 (ja) | 2023-01-18 | 2024-05-29 | ダイキン工業株式会社 | 電気化学デバイス用合剤、電気化学デバイス用合剤シート、電極、及び、電気化学デバイス |
| CN116854841A (zh) * | 2023-07-31 | 2023-10-10 | 河南省氟基新材料科技有限公司 | 一种锂电级聚偏二氟乙烯粘结剂的制备方法 |
| TW202528491A (zh) | 2023-12-06 | 2025-07-16 | 美商科慕Ｆｃ有限責任公司 | 部分氟化芳基醚界面活性劑組成物及使用方法 |
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| ITMI20050007A1 (it) | 2005-01-05 | 2006-07-06 | Solvay Solexis Spa | Uso di dispersioni acquose di polimeri a base di vdf nella preparazione di vernici per rivestimenti di substrati architettonici |
| US20070015937A1 (en) | 2005-07-15 | 2007-01-18 | 3M Innovative Properties Company | Process for recovery of fluorinated carboxylic acid surfactants from exhaust gas |
| GB0514398D0 (en) | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant |
| GB0525978D0 (en) | 2005-12-21 | 2006-02-01 | 3M Innovative Properties Co | Fluorinated Surfactants For Making Fluoropolymers |
| GB0514387D0 (en) | 2005-07-15 | 2005-08-17 | 3M Innovative Properties Co | Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant |
| WO2007046345A1 (ja) | 2005-10-17 | 2007-04-26 | Asahi Glass Company, Limited | ポリテトラフルオロエチレン水性乳化液、それから得られるポリテトラフルオロエチレンファインパウダーおよび多孔体 |
| CN101291987B (zh) | 2005-10-20 | 2012-05-09 | 旭硝子株式会社 | 聚四氟乙烯水性分散液及其制品 |
| WO2007046377A1 (ja) | 2005-10-20 | 2007-04-26 | Asahi Glass Company, Limited | 溶融成形可能なフッ素樹脂の製造方法 |
| EP1942118B1 (en) | 2005-10-26 | 2013-09-11 | Asahi Glass Company, Limited | Fluororesin with low fluorine-containing emulsifier residual and method for producing same |
| ATE509960T1 (de) * | 2006-11-09 | 2011-06-15 | Du Pont | Wässrige polymerisation eines fluorinierten monomers mithilfe eines polymerisationsmittels mit einer fluorpolyethersäure oder einem salz daraus und einem fluorpolyethersäuretensid oder - salztensid von hohem molekulargewicht |
-
2007
- 2007-11-09 EP EP07840004A patent/EP2084195B1/en not_active Not-in-force
- 2007-11-09 US US11/937,536 patent/US7897682B2/en active Active
- 2007-11-09 JP JP2009536316A patent/JP5439186B2/ja active Active
- 2007-11-09 CN CN200780041364.2A patent/CN101605826B/zh not_active Expired - Fee Related
- 2007-11-09 WO PCT/US2007/023642 patent/WO2008060463A1/en not_active Ceased
- 2007-11-09 AT AT07840004T patent/ATE512165T1/de not_active IP Right Cessation
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