JP2008511645A - 最適化液相酸化 - Google Patents

最適化液相酸化 Download PDF

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Publication number
JP2008511645A
JP2008511645A JP2007530223A JP2007530223A JP2008511645A JP 2008511645 A JP2008511645 A JP 2008511645A JP 2007530223 A JP2007530223 A JP 2007530223A JP 2007530223 A JP2007530223 A JP 2007530223A JP 2008511645 A JP2008511645 A JP 2008511645A
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reaction medium
reaction zone
reactor
reaction
zone
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JP2007530223A
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Japanese (ja)
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JP2008511645A5 (enExample
Inventor
ジョージ ワンダース,アラン
ウッド,ジュニア ジェンキンス,ハワード
レイノルズ パーティン,リー
スコット ストラッサー,ウェイン
フレーデ,マルセル デ
グプタ,プニート
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Eastman Chemical Co
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Eastman Chemical Co
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Priority claimed from US11/154,116 external-priority patent/US7507857B2/en
Priority claimed from US11/153,993 external-priority patent/US7589231B2/en
Priority claimed from US11/154,253 external-priority patent/US7692037B2/en
Application filed by Eastman Chemical Co filed Critical Eastman Chemical Co
Publication of JP2008511645A publication Critical patent/JP2008511645A/ja
Publication of JP2008511645A5 publication Critical patent/JP2008511645A5/ja
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1862Stationary reactors having moving elements inside placed in series
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/002Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C63/00Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
    • C07C63/14Monocyclic dicarboxylic acids
    • C07C63/15Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
    • C07C63/261,4 - Benzenedicarboxylic acid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002Chemical plants
    • B01J2219/00004Scale aspects
    • B01J2219/00006Large-scale industrial plants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00121Controlling the temperature by direct heating or cooling
    • B01J2219/00123Controlling the temperature by direct heating or cooling adding a temperature modifying medium to the reactants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00121Controlling the temperature by direct heating or cooling
    • B01J2219/00128Controlling the temperature by direct heating or cooling by evaporation of reactants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00182Controlling or regulating processes controlling the level of reactants in the reactor vessel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00245Avoiding undesirable reactions or side-effects
    • B01J2219/0025Foam formation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00768Baffles attached to the reactor wall vertical
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/0077Baffles attached to the reactor wall inclined
    • B01J2219/00774Baffles attached to the reactor wall inclined in the form of cones
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00777Baffles attached to the reactor wall horizontal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/185Details relating to the spatial orientation of the reactor vertical

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2007530223A 2004-09-02 2005-08-29 最適化液相酸化 Pending JP2008511645A (ja)

Applications Claiming Priority (10)

Application Number Priority Date Filing Date Title
US60661804P 2004-09-02 2004-09-02
US60661404P 2004-09-02 2004-09-02
US60680904P 2004-09-02 2004-09-02
US63149004P 2004-11-29 2004-11-29
US63132604P 2004-11-29 2004-11-29
US63138804P 2004-11-29 2004-11-29
US11/154,116 US7507857B2 (en) 2004-09-02 2005-06-16 Optimized liquid-phase oxidation
US11/153,993 US7589231B2 (en) 2004-09-02 2005-06-16 Optimized liquid-phase oxidation
US11/154,253 US7692037B2 (en) 2004-09-02 2005-06-16 Optimized liquid-phase oxidation
PCT/US2005/030649 WO2006028766A2 (en) 2004-09-02 2005-08-29 Optimized liquid-phase oxidation

Publications (2)

Publication Number Publication Date
JP2008511645A true JP2008511645A (ja) 2008-04-17
JP2008511645A5 JP2008511645A5 (enExample) 2008-10-16

Family

ID=35504394

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2007530223A Pending JP2008511645A (ja) 2004-09-02 2005-08-29 最適化液相酸化

Country Status (8)

Country Link
EP (1) EP1786746A2 (enExample)
JP (1) JP2008511645A (enExample)
KR (1) KR20070048251A (enExample)
CN (2) CN101010267B (enExample)
BR (1) BRPI0514773A (enExample)
CA (1) CA2576246A1 (enExample)
MX (1) MX2007002283A (enExample)
WO (1) WO2006028766A2 (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008511649A (ja) * 2004-09-02 2008-04-17 イーストマン ケミカル カンパニー 最適化液相酸化
JP2016026232A (ja) * 2010-01-29 2016-02-12 グルーポ ペトロテメックス,ソシエダ アノニマ デ カピタル バリアブレ 側方取り出し式の第2の反応器を備える酸化システム

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8790601B2 (en) * 2010-01-29 2014-07-29 Grupo Petrotemex, S.A. De C.V. Oxidation system with sidedraw secondary reactor

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3240803A (en) * 1961-08-14 1966-03-15 Eastman Kodak Co Preparation of benzenecarboxylic acid
JPS56113346A (en) * 1980-01-23 1981-09-07 Montedison Spa Method of recovering catalyst for synthesizing terephthalic acid in active form
JPH07278048A (ja) * 1994-04-01 1995-10-24 Mitsui Petrochem Ind Ltd 芳香族カルボン酸の製造方法および装置
JPH10330292A (ja) * 1996-12-12 1998-12-15 Praxair Technol Inc 気泡塔反応器への直接的酸素注入法
JP2002526251A (ja) * 1998-09-23 2002-08-20 デグサ アクチエンゲゼルシャフト 気泡塔及びその使用
JP2004531573A (ja) * 2001-06-04 2004-10-14 イーストマン ケミカル カンパニー 精製テレフタル酸の製造方法
JP2004533410A (ja) * 2001-01-10 2004-11-04 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー カルボン酸を製造するための改善された方法
JP2006509044A (ja) * 2002-12-09 2006-03-16 イーストマン ケミカル カンパニー 粗製カルボン酸スラリーの精製方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6949673B2 (en) * 2000-01-12 2005-09-27 E.I. Du Pont De Nemours And Company Process for producing carboxylic acids

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3240803A (en) * 1961-08-14 1966-03-15 Eastman Kodak Co Preparation of benzenecarboxylic acid
JPS56113346A (en) * 1980-01-23 1981-09-07 Montedison Spa Method of recovering catalyst for synthesizing terephthalic acid in active form
JPH07278048A (ja) * 1994-04-01 1995-10-24 Mitsui Petrochem Ind Ltd 芳香族カルボン酸の製造方法および装置
JPH10330292A (ja) * 1996-12-12 1998-12-15 Praxair Technol Inc 気泡塔反応器への直接的酸素注入法
JP2002526251A (ja) * 1998-09-23 2002-08-20 デグサ アクチエンゲゼルシャフト 気泡塔及びその使用
JP2004533410A (ja) * 2001-01-10 2004-11-04 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー カルボン酸を製造するための改善された方法
JP2004531573A (ja) * 2001-06-04 2004-10-14 イーストマン ケミカル カンパニー 精製テレフタル酸の製造方法
JP2006509044A (ja) * 2002-12-09 2006-03-16 イーストマン ケミカル カンパニー 粗製カルボン酸スラリーの精製方法

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008511649A (ja) * 2004-09-02 2008-04-17 イーストマン ケミカル カンパニー 最適化液相酸化
JP2016026232A (ja) * 2010-01-29 2016-02-12 グルーポ ペトロテメックス,ソシエダ アノニマ デ カピタル バリアブレ 側方取り出し式の第2の反応器を備える酸化システム
JP2017190350A (ja) * 2010-01-29 2017-10-19 グルーポ ペトロテメックス,ソシエダ アノニマ デ カピタル バリアブレ 側方取り出し式の第2の反応器を備える酸化システム

Also Published As

Publication number Publication date
MX2007002283A (es) 2007-04-23
EP1786746A2 (en) 2007-05-23
CN101010267B (zh) 2013-05-29
CA2576246A1 (en) 2006-03-16
WO2006028766A2 (en) 2006-03-16
WO2006028766A3 (en) 2006-07-20
WO2006028766A8 (en) 2006-06-08
BRPI0514773A (pt) 2008-06-24
CN101010267A (zh) 2007-08-01
KR20070048251A (ko) 2007-05-08
CN101768034A (zh) 2010-07-07

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