JP2008511638A - 最適化液相酸化 - Google Patents

最適化液相酸化 Download PDF

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Publication number
JP2008511638A
JP2008511638A JP2007530196A JP2007530196A JP2008511638A JP 2008511638 A JP2008511638 A JP 2008511638A JP 2007530196 A JP2007530196 A JP 2007530196A JP 2007530196 A JP2007530196 A JP 2007530196A JP 2008511638 A JP2008511638 A JP 2008511638A
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JP
Japan
Prior art keywords
reaction medium
bubble column
reactor
reaction zone
oxidation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2007530196A
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English (en)
Japanese (ja)
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JP2008511638A5 (enExample
Inventor
ジョージ ワンダース,アラン
リン,ロバート
フレーデ,マルセル デ
レイノルズ パーティン,リー
スコット ストラッサー,ウェイン
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Eastman Chemical Co
Original Assignee
Eastman Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US11/154,202 external-priority patent/US7692036B2/en
Priority claimed from US11/154,218 external-priority patent/US7568361B2/en
Application filed by Eastman Chemical Co filed Critical Eastman Chemical Co
Publication of JP2008511638A publication Critical patent/JP2008511638A/ja
Publication of JP2008511638A5 publication Critical patent/JP2008511638A5/ja
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1872Details of the fluidised bed reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1836Heating and cooling the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/23Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
    • C07C51/235Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00106Controlling the temperature by indirect heat exchange
    • B01J2208/00115Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/0015Plates; Cylinders

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Combustion & Propulsion (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2007530196A 2004-09-02 2005-08-29 最適化液相酸化 Pending JP2008511638A (ja)

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
US60685604P 2004-09-02 2004-09-02
US63132004P 2004-11-29 2004-11-29
US63139904P 2004-11-29 2004-11-29
US11/154,202 US7692036B2 (en) 2004-11-29 2005-06-16 Optimized liquid-phase oxidation
US11/154,218 US7568361B2 (en) 2004-09-02 2005-06-16 Optimized liquid-phase oxidation
PCT/US2005/030546 WO2006028752A2 (en) 2004-09-02 2005-08-29 Optimized liquid-phase oxidation

Publications (2)

Publication Number Publication Date
JP2008511638A true JP2008511638A (ja) 2008-04-17
JP2008511638A5 JP2008511638A5 (enExample) 2008-10-16

Family

ID=35504618

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2007530196A Pending JP2008511638A (ja) 2004-09-02 2005-08-29 最適化液相酸化

Country Status (12)

Country Link
EP (1) EP1791800B1 (enExample)
JP (1) JP2008511638A (enExample)
KR (2) KR101281347B1 (enExample)
CN (2) CN101023046B (enExample)
BR (1) BRPI0514800B1 (enExample)
CA (1) CA2576632A1 (enExample)
ES (1) ES2655728T3 (enExample)
LT (1) LT1791800T (enExample)
MX (1) MX2007002565A (enExample)
PL (1) PL1791800T3 (enExample)
PT (1) PT1791800T (enExample)
WO (1) WO2006028752A2 (enExample)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016536109A (ja) * 2013-09-25 2016-11-24 リンデ アクチエンゲゼルシャフトLinde Aktiengesellschaft 角柱体から成る物質移動トレイと液体分配部とを備えた塔
JP2021502895A (ja) * 2017-11-14 2021-02-04 中国石油化工股▲ふん▼有限公司 流体分配器、反応装置及びその適用

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8066949B2 (en) 2008-09-26 2011-11-29 Exxonmobil Research & Engineering Company Scrubber for fluid coker unit
US8933265B2 (en) * 2010-06-30 2015-01-13 Uop Llc Process for oxidizing alkyl aromatic compounds
US8933266B2 (en) * 2010-06-30 2015-01-13 Uop Llc Process for producing terephthalic acid
KR102849255B1 (ko) * 2021-12-10 2025-08-21 주식회사 엘지화학 기포탑 반응기

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1062482A (en) * 1963-04-30 1967-03-22 Standard Oil Co High quality phthalic acids
JPS5257134A (en) * 1975-10-31 1977-05-11 Mitsubishi Chem Ind Ltd Process for preparation of aromatic polycarboxylic acids
JPS59104345A (ja) * 1982-12-03 1984-06-16 Kuraray Yuka Kk 直接重合用に適したテレフタル酸の製造方法
JPS6354403B2 (enExample) * 1982-04-13 1988-10-27 Jgc Corp
JPH06345699A (ja) * 1993-06-07 1994-12-20 Bayer Ag エチレングリコールカーボネート及びプロピレングリコールカーボネートを製造するための反応器及びその反応器で行う連続的方法
JPH0741456A (ja) * 1993-07-29 1995-02-10 Mitsubishi Gas Chem Co Inc 芳香族ジカルボン酸製造用酸化反応器
JPH09278709A (ja) * 1996-02-13 1997-10-28 Mitsubishi Chem Corp 芳香族カルボン酸の製造方法
JP2002526251A (ja) * 1998-09-23 2002-08-20 デグサ アクチエンゲゼルシャフト 気泡塔及びその使用
WO2004052821A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
WO2004052820A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the purification of a crude carboxylic acid slurry

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT236346B (de) * 1961-01-25 1964-10-12 Union Carbide Corp Boden zum Inberührungbringen von Flüssigkeit und Gas
GB1250222A (enExample) * 1968-10-25 1971-10-20
US3660476A (en) * 1968-10-30 1972-05-02 Teijin Ltd Method for the preparation of terephthalic acid
BE724040A (enExample) * 1968-11-18 1969-05-02
SI9500109A (en) * 1995-04-05 1996-10-31 Levec Janez Dipl Ing Prof Dr Apparatus and Process for Thermal Oxidative Treatment of Waste Waters
US5929274A (en) * 1995-06-07 1999-07-27 Hfm International, Inc. Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid
US6084125A (en) * 1996-02-27 2000-07-04 Praxair Technology, Inc. Process for producing aliphatic acids using a reactor system having a shell and a tube reactor configuration to force circulation of reaction liquid
ID19133A (id) * 1996-12-12 1998-06-18 Praxair Technology Inc Pengisian oksigen langsung kedalam reaktor-reaktor ruang gelembung
GB9701251D0 (en) * 1997-01-22 1997-03-12 Bp Chem Int Ltd Process
CA2396967A1 (en) * 2000-01-21 2001-07-26 Bp Corporation North America Inc. Production of high purity aromatic carboxylic acid by oxidation in benzoic acid and water solvent
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1062482A (en) * 1963-04-30 1967-03-22 Standard Oil Co High quality phthalic acids
JPS5257134A (en) * 1975-10-31 1977-05-11 Mitsubishi Chem Ind Ltd Process for preparation of aromatic polycarboxylic acids
JPS6354403B2 (enExample) * 1982-04-13 1988-10-27 Jgc Corp
JPS59104345A (ja) * 1982-12-03 1984-06-16 Kuraray Yuka Kk 直接重合用に適したテレフタル酸の製造方法
JPH06345699A (ja) * 1993-06-07 1994-12-20 Bayer Ag エチレングリコールカーボネート及びプロピレングリコールカーボネートを製造するための反応器及びその反応器で行う連続的方法
JPH0741456A (ja) * 1993-07-29 1995-02-10 Mitsubishi Gas Chem Co Inc 芳香族ジカルボン酸製造用酸化反応器
JPH09278709A (ja) * 1996-02-13 1997-10-28 Mitsubishi Chem Corp 芳香族カルボン酸の製造方法
JP2002526251A (ja) * 1998-09-23 2002-08-20 デグサ アクチエンゲゼルシャフト 気泡塔及びその使用
WO2004052821A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
WO2004052820A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the purification of a crude carboxylic acid slurry

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2016536109A (ja) * 2013-09-25 2016-11-24 リンデ アクチエンゲゼルシャフトLinde Aktiengesellschaft 角柱体から成る物質移動トレイと液体分配部とを備えた塔
JP2021502895A (ja) * 2017-11-14 2021-02-04 中国石油化工股▲ふん▼有限公司 流体分配器、反応装置及びその適用
JP7216087B2 (ja) 2017-11-14 2023-01-31 中国石油化工股▲ふん▼有限公司 流体分配器、反応装置及びその適用

Also Published As

Publication number Publication date
WO2006028752A3 (en) 2006-06-01
LT1791800T (lt) 2018-01-25
KR20130003039A (ko) 2013-01-08
EP1791800B1 (en) 2017-11-01
BRPI0514800A (pt) 2008-06-24
PL1791800T3 (pl) 2018-04-30
CN101766979A (zh) 2010-07-07
PT1791800T (pt) 2018-02-02
CN101766979B (zh) 2012-12-26
MX2007002565A (es) 2007-04-24
KR101281347B1 (ko) 2013-07-02
BRPI0514800B1 (pt) 2015-11-24
KR20070048256A (ko) 2007-05-08
EP1791800A2 (en) 2007-06-06
CN101023046A (zh) 2007-08-22
KR101363824B1 (ko) 2014-02-17
ES2655728T3 (es) 2018-02-21
CA2576632A1 (en) 2006-03-16
WO2006028752A2 (en) 2006-03-16
CN101023046B (zh) 2019-01-18

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