CN101023046B - 优化的液相氧化 - Google Patents

优化的液相氧化 Download PDF

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Publication number
CN101023046B
CN101023046B CN200580029558.1A CN200580029558A CN101023046B CN 101023046 B CN101023046 B CN 101023046B CN 200580029558 A CN200580029558 A CN 200580029558A CN 101023046 B CN101023046 B CN 101023046B
Authority
CN
China
Prior art keywords
reaction medium
reaction
reaction zone
oxidation
reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN200580029558.1A
Other languages
English (en)
Chinese (zh)
Other versions
CN101023046A (zh
Inventor
A·G·万德斯
林鑫
M·德弗里德
L·R·帕丁
W·S·施特拉泽
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Grupo Petrotemex SA de CV
Original Assignee
Grupo Petrotemex SA de CV
Eastman Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US11/154,202 external-priority patent/US7692036B2/en
Priority claimed from US11/154,218 external-priority patent/US7568361B2/en
Application filed by Grupo Petrotemex SA de CV, Eastman Chemical Co filed Critical Grupo Petrotemex SA de CV
Publication of CN101023046A publication Critical patent/CN101023046A/zh
Application granted granted Critical
Publication of CN101023046B publication Critical patent/CN101023046B/zh
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1872—Details of the fluidised bed reactor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1836—Heating and cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/23—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
    • C07C51/235—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/0015—Plates; Cylinders

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Combustion & Propulsion (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN200580029558.1A 2004-09-02 2005-08-29 优化的液相氧化 Expired - Lifetime CN101023046B (zh)

Applications Claiming Priority (11)

Application Number Priority Date Filing Date Title
US60685604P 2004-09-02 2004-09-02
US60/606,856 2004-09-02
US63132004P 2004-11-29 2004-11-29
US63139904P 2004-11-29 2004-11-29
US60/631,399 2004-11-29
US60/631,320 2004-11-29
US11/154,218 2005-06-16
US11/154,202 US7692036B2 (en) 2004-11-29 2005-06-16 Optimized liquid-phase oxidation
US11/154,218 US7568361B2 (en) 2004-09-02 2005-06-16 Optimized liquid-phase oxidation
US11/154,202 2005-06-16
PCT/US2005/030546 WO2006028752A2 (en) 2004-09-02 2005-08-29 Optimized liquid-phase oxidation

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN2010101169790A Division CN101766979B (zh) 2004-09-02 2005-08-29 优化的液相氧化

Publications (2)

Publication Number Publication Date
CN101023046A CN101023046A (zh) 2007-08-22
CN101023046B true CN101023046B (zh) 2019-01-18

Family

ID=35504618

Family Applications (2)

Application Number Title Priority Date Filing Date
CN200580029558.1A Expired - Lifetime CN101023046B (zh) 2004-09-02 2005-08-29 优化的液相氧化
CN2010101169790A Expired - Lifetime CN101766979B (zh) 2004-09-02 2005-08-29 优化的液相氧化

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN2010101169790A Expired - Lifetime CN101766979B (zh) 2004-09-02 2005-08-29 优化的液相氧化

Country Status (12)

Country Link
EP (1) EP1791800B1 (enExample)
JP (1) JP2008511638A (enExample)
KR (2) KR101281347B1 (enExample)
CN (2) CN101023046B (enExample)
BR (1) BRPI0514800B1 (enExample)
CA (1) CA2576632A1 (enExample)
ES (1) ES2655728T3 (enExample)
LT (1) LT1791800T (enExample)
MX (1) MX2007002565A (enExample)
PL (1) PL1791800T3 (enExample)
PT (1) PT1791800T (enExample)
WO (1) WO2006028752A2 (enExample)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8066949B2 (en) 2008-09-26 2011-11-29 Exxonmobil Research & Engineering Company Scrubber for fluid coker unit
US8933265B2 (en) * 2010-06-30 2015-01-13 Uop Llc Process for oxidizing alkyl aromatic compounds
US8933266B2 (en) * 2010-06-30 2015-01-13 Uop Llc Process for producing terephthalic acid
US10201765B2 (en) * 2013-09-25 2019-02-12 Linde Aktiengesellschaft Column with angular profiles
CN109772236B (zh) * 2017-11-14 2022-08-12 中国石油化工股份有限公司 一种流体分布器、反应装置及其应用
KR102849255B1 (ko) * 2021-12-10 2025-08-21 주식회사 엘지화학 기포탑 반응기

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004052820A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the purification of a crude carboxylic acid slurry

Family Cites Families (20)

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Publication number Priority date Publication date Assignee Title
AT236346B (de) * 1961-01-25 1964-10-12 Union Carbide Corp Boden zum Inberührungbringen von Flüssigkeit und Gas
GB1062482A (en) * 1963-04-30 1967-03-22 Standard Oil Co High quality phthalic acids
GB1250222A (enExample) * 1968-10-25 1971-10-20
US3660476A (en) * 1968-10-30 1972-05-02 Teijin Ltd Method for the preparation of terephthalic acid
BE724040A (enExample) * 1968-11-18 1969-05-02
JPS5912096B2 (ja) * 1975-10-31 1984-03-21 三菱化学株式会社 ホウコウゾクポリカルボンサンノセイゾウホウ
JPS58177106A (ja) * 1982-04-13 1983-10-17 Jgc Corp 多段式高流速気液接触装置
JPS59104345A (ja) * 1982-12-03 1984-06-16 Kuraray Yuka Kk 直接重合用に適したテレフタル酸の製造方法
DE4318893A1 (de) * 1993-06-07 1994-12-08 Bayer Ag Reaktor und damit durchzuführendes kontinuierliches Verfahren zur Herstellung von Ethylenglykolcarbonat bzw. Propylenglykolcarbonat
JP3719448B2 (ja) * 1993-07-29 2005-11-24 三菱瓦斯化学株式会社 芳香族ジカルボン酸製造用酸化反応器
SI9500109A (en) * 1995-04-05 1996-10-31 Levec Janez Dipl Ing Prof Dr Apparatus and Process for Thermal Oxidative Treatment of Waste Waters
US5929274A (en) * 1995-06-07 1999-07-27 Hfm International, Inc. Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid
JPH09278709A (ja) * 1996-02-13 1997-10-28 Mitsubishi Chem Corp 芳香族カルボン酸の製造方法
US6084125A (en) * 1996-02-27 2000-07-04 Praxair Technology, Inc. Process for producing aliphatic acids using a reactor system having a shell and a tube reactor configuration to force circulation of reaction liquid
ID19133A (id) * 1996-12-12 1998-06-18 Praxair Technology Inc Pengisian oksigen langsung kedalam reaktor-reaktor ruang gelembung
GB9701251D0 (en) * 1997-01-22 1997-03-12 Bp Chem Int Ltd Process
DE19843573A1 (de) * 1998-09-23 2000-03-30 Degussa Blasensäule und deren Verwendung
CA2396967A1 (en) * 2000-01-21 2001-07-26 Bp Corporation North America Inc. Production of high purity aromatic carboxylic acid by oxidation in benzoic acid and water solvent
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
RU2005121568A (ru) * 2002-12-09 2006-01-20 Истман Кемикал Компани (US) Способ окислительной очистки терефталевой кислоты

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004052820A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the purification of a crude carboxylic acid slurry

Also Published As

Publication number Publication date
WO2006028752A3 (en) 2006-06-01
LT1791800T (lt) 2018-01-25
KR20130003039A (ko) 2013-01-08
EP1791800B1 (en) 2017-11-01
BRPI0514800A (pt) 2008-06-24
PL1791800T3 (pl) 2018-04-30
CN101766979A (zh) 2010-07-07
PT1791800T (pt) 2018-02-02
CN101766979B (zh) 2012-12-26
MX2007002565A (es) 2007-04-24
KR101281347B1 (ko) 2013-07-02
BRPI0514800B1 (pt) 2015-11-24
KR20070048256A (ko) 2007-05-08
EP1791800A2 (en) 2007-06-06
CN101023046A (zh) 2007-08-22
KR101363824B1 (ko) 2014-02-17
ES2655728T3 (es) 2018-02-21
CA2576632A1 (en) 2006-03-16
WO2006028752A2 (en) 2006-03-16
JP2008511638A (ja) 2008-04-17

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Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
ASS Succession or assignment of patent right

Owner name: PEMEX GROUP LLC

Free format text: FORMER OWNER: EASTMAN CHEM CO.

Effective date: 20110906

C41 Transfer of patent application or patent right or utility model
TA01 Transfer of patent application right

Effective date of registration: 20110906

Address after: Nuevo Leon, Mexico

Applicant after: GRUPO PETROTEMEX, S.A. de C.V.

Address before: Tennessee

Applicant before: EASTMAN CHEMICAL Co.

EE01 Entry into force of recordation of patent licensing contract

Assignee: JIAXING PETROCHEMICAL Co.,Ltd.

Assignor: GRUPO PETROTEMEX, S.A. de C.V.

Contract record no.: 2012990000015

Denomination of invention: Optimized liquid-phase oxidation

License type: Common License

Open date: 20070822

Record date: 20120113

GR01 Patent grant
GR01 Patent grant
CX01 Expiry of patent term
CX01 Expiry of patent term

Granted publication date: 20190118